Effect of the addition of YAG (Y 3Al 5O 12) nanopowder on the mechanical properties of lanthanum zirconate
La 2Zr 2O 7 (LZ) is a promising thermal barrier coating material for the high-temperature applications, which could be significantly toughened by the YAG nanopowder incorporated into the matrix. The composites of xYAG/(1 − x)LZ ( x = 10, 15, 20 vol.%, LZ- x-YAG) were densified by means of high-press...
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Veröffentlicht in: | Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 2007-07, Vol.460, p.504-508 |
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Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | La
2Zr
2O
7 (LZ) is a promising thermal barrier coating material for the high-temperature applications, which could be significantly toughened by the YAG nanopowder incorporated into the matrix. The composites of
xYAG/(1
−
x)LZ (
x
=
10, 15, 20
vol.%, LZ-
x-YAG) were densified by means of high-pressure sintering (HPS) under a pressure of 4.5
GPa at 1650
°C for 5
min, by which a high-relative density above 93% could be obtained. The morphologies of the fractured surfaces were investigated by the scanning electron microscope, and the fracture toughness and Vicker's-hardness of the composites were evaluated by the microindentation. The grain size of the LZ matrix drops significantly with the addition of YAG nanoparticles and the fracture type changes from the intergranular to a mixture type of the transgranular and intergranular in the nanocomposites. The LZ-20-YAG nanocomposite has a fracture toughness of 1.93
MPa
m
1/2, which is obviously higher than that of the pure LZ (1.57
MPa
m
1/2), and the toughening mechanism is discussed in this paper. |
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ISSN: | 0921-5093 1873-4936 |
DOI: | 10.1016/j.msea.2007.02.003 |