Controlled synthesis and characterization of nickel phosphide nanocrystal
Ni 2 P nanocrystal with dendritic morphologies was synthesized via a solvothermal reaction between nickel sulfate (Ni-source) and yellow phosphorous (P-source) in a mixture solution of glycol and water. X-ray powder diffraction (XRD), electron diffraction pattern (ED) and transmission electronic mic...
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| Veröffentlicht in: | Journal of crystal growth 2007-06, Vol.304 (2), p.430-434 |
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| container_end_page | 434 |
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| container_issue | 2 |
| container_start_page | 430 |
| container_title | Journal of crystal growth |
| container_volume | 304 |
| creator | Liu, Shuling Liu, Xinzheng Xu, Liqiang Qian, Yitai Ma, Xicheng |
| description | Ni
2
P
nanocrystal with dendritic morphologies was synthesized via a solvothermal reaction between nickel sulfate (Ni-source) and yellow phosphorous (P-source) in a mixture solution of glycol and water. X-ray powder diffraction (XRD), electron diffraction pattern (ED) and transmission electronic microscopy (TEM) studies show that the as-synthesized nanocrystals is pure
Ni
2
P
with a hexagonal phase and a dendritic morphology. The growth mechanism of
Ni
2
P
dendrites involves a special solid–solution–solid transformation as well as an Ostwald ripening process. Moreover the growth of
Ni
2
P
nanodendrites occurs at the expense of
Ni
2
P
nanospheres. The effects of experimental conditions such as the volume ratio of glycol to water and solvothermal temperature on the final products were also discussed. |
| doi_str_mv | 10.1016/j.jcrysgro.2007.03.002 |
| format | Article |
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2
P
nanocrystal with dendritic morphologies was synthesized via a solvothermal reaction between nickel sulfate (Ni-source) and yellow phosphorous (P-source) in a mixture solution of glycol and water. X-ray powder diffraction (XRD), electron diffraction pattern (ED) and transmission electronic microscopy (TEM) studies show that the as-synthesized nanocrystals is pure
Ni
2
P
with a hexagonal phase and a dendritic morphology. The growth mechanism of
Ni
2
P
dendrites involves a special solid–solution–solid transformation as well as an Ostwald ripening process. Moreover the growth of
Ni
2
P
nanodendrites occurs at the expense of
Ni
2
P
nanospheres. The effects of experimental conditions such as the volume ratio of glycol to water and solvothermal temperature on the final products were also discussed.</description><identifier>ISSN: 0022-0248</identifier><identifier>EISSN: 1873-5002</identifier><identifier>DOI: 10.1016/j.jcrysgro.2007.03.002</identifier><identifier>CODEN: JCRGAE</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>A1. Characterization ; A1. Crystal morphology ; A1. Solvent ; A1. X-ray diffraction ; B1. Nanomaterials ; B1. Phosphides ; Condensed matter: structure, mechanical and thermal properties ; Cross-disciplinary physics: materials science; rheology ; Exact sciences and technology ; Materials science ; Methods of deposition of films and coatings; film growth and epitaxy ; Nanoscale materials and structures: fabrication and characterization ; Other topics in nanoscale materials and structures ; Physics ; Single-crystal and powder diffraction ; Structure of solids and liquids; crystallography ; Theory and models of film growth ; X-ray diffraction and scattering</subject><ispartof>Journal of crystal growth, 2007-06, Vol.304 (2), p.430-434</ispartof><rights>2007 Elsevier B.V.</rights><rights>2007 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c373t-184b3b0f914c1688257871a6dd29ce66717bb03bee852a4dcaf9c9d984d8eec93</citedby><cites>FETCH-LOGICAL-c373t-184b3b0f914c1688257871a6dd29ce66717bb03bee852a4dcaf9c9d984d8eec93</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.jcrysgro.2007.03.002$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,777,781,3537,27905,27906,45976</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=18829657$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Liu, Shuling</creatorcontrib><creatorcontrib>Liu, Xinzheng</creatorcontrib><creatorcontrib>Xu, Liqiang</creatorcontrib><creatorcontrib>Qian, Yitai</creatorcontrib><creatorcontrib>Ma, Xicheng</creatorcontrib><title>Controlled synthesis and characterization of nickel phosphide nanocrystal</title><title>Journal of crystal growth</title><description>Ni
2
P
nanocrystal with dendritic morphologies was synthesized via a solvothermal reaction between nickel sulfate (Ni-source) and yellow phosphorous (P-source) in a mixture solution of glycol and water. X-ray powder diffraction (XRD), electron diffraction pattern (ED) and transmission electronic microscopy (TEM) studies show that the as-synthesized nanocrystals is pure
Ni
2
P
with a hexagonal phase and a dendritic morphology. The growth mechanism of
Ni
2
P
dendrites involves a special solid–solution–solid transformation as well as an Ostwald ripening process. Moreover the growth of
Ni
2
P
nanodendrites occurs at the expense of
Ni
2
P
nanospheres. The effects of experimental conditions such as the volume ratio of glycol to water and solvothermal temperature on the final products were also discussed.</description><subject>A1. Characterization</subject><subject>A1. Crystal morphology</subject><subject>A1. Solvent</subject><subject>A1. X-ray diffraction</subject><subject>B1. Nanomaterials</subject><subject>B1. Phosphides</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Exact sciences and technology</subject><subject>Materials science</subject><subject>Methods of deposition of films and coatings; film growth and epitaxy</subject><subject>Nanoscale materials and structures: fabrication and characterization</subject><subject>Other topics in nanoscale materials and structures</subject><subject>Physics</subject><subject>Single-crystal and powder diffraction</subject><subject>Structure of solids and liquids; crystallography</subject><subject>Theory and models of film growth</subject><subject>X-ray diffraction and scattering</subject><issn>0022-0248</issn><issn>1873-5002</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2007</creationdate><recordtype>article</recordtype><recordid>eNqFkMtOwzAQRS0EEqXwCygb2CXYzsPODlTxqITEBtaWM55Ql9QudopUvh5XLWLJZmYW586duYRcMlowypqbZbGEsI3vwRecUlHQsqCUH5EJk6LM6zQfk0mqPKe8kqfkLMYlpUnJ6ITMZ96NwQ8Dmixu3bjAaGOmnclgoYOGEYP91qP1LvN95ix84JCtFz6uF9Zg5rTzO_NRD-fkpNdDxItDn5K3h_vX2VP-_PI4n90951CKcsyZrLqyo33LKmCNlLwWUjDdGMNbwKYRTHQdLTtEWXNdGdB9C61pZWUkIrTllFzv966D_9xgHNXKRsBh0A79JireCtlwWiew2YMQfIwBe7UOdqXDVjGqdsmppfpNTu2SU7RUKackvDo46Ah66IN2YOOfOh3dNrVI3O2ew_Tul8WgIlh0gMYGhFEZb_-z-gErYomI</recordid><startdate>20070615</startdate><enddate>20070615</enddate><creator>Liu, Shuling</creator><creator>Liu, Xinzheng</creator><creator>Xu, Liqiang</creator><creator>Qian, Yitai</creator><creator>Ma, Xicheng</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20070615</creationdate><title>Controlled synthesis and characterization of nickel phosphide nanocrystal</title><author>Liu, Shuling ; Liu, Xinzheng ; Xu, Liqiang ; Qian, Yitai ; Ma, Xicheng</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c373t-184b3b0f914c1688257871a6dd29ce66717bb03bee852a4dcaf9c9d984d8eec93</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2007</creationdate><topic>A1. Characterization</topic><topic>A1. Crystal morphology</topic><topic>A1. Solvent</topic><topic>A1. X-ray diffraction</topic><topic>B1. Nanomaterials</topic><topic>B1. Phosphides</topic><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Exact sciences and technology</topic><topic>Materials science</topic><topic>Methods of deposition of films and coatings; film growth and epitaxy</topic><topic>Nanoscale materials and structures: fabrication and characterization</topic><topic>Other topics in nanoscale materials and structures</topic><topic>Physics</topic><topic>Single-crystal and powder diffraction</topic><topic>Structure of solids and liquids; crystallography</topic><topic>Theory and models of film growth</topic><topic>X-ray diffraction and scattering</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Liu, Shuling</creatorcontrib><creatorcontrib>Liu, Xinzheng</creatorcontrib><creatorcontrib>Xu, Liqiang</creatorcontrib><creatorcontrib>Qian, Yitai</creatorcontrib><creatorcontrib>Ma, Xicheng</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of crystal growth</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Liu, Shuling</au><au>Liu, Xinzheng</au><au>Xu, Liqiang</au><au>Qian, Yitai</au><au>Ma, Xicheng</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Controlled synthesis and characterization of nickel phosphide nanocrystal</atitle><jtitle>Journal of crystal growth</jtitle><date>2007-06-15</date><risdate>2007</risdate><volume>304</volume><issue>2</issue><spage>430</spage><epage>434</epage><pages>430-434</pages><issn>0022-0248</issn><eissn>1873-5002</eissn><coden>JCRGAE</coden><abstract>Ni
2
P
nanocrystal with dendritic morphologies was synthesized via a solvothermal reaction between nickel sulfate (Ni-source) and yellow phosphorous (P-source) in a mixture solution of glycol and water. X-ray powder diffraction (XRD), electron diffraction pattern (ED) and transmission electronic microscopy (TEM) studies show that the as-synthesized nanocrystals is pure
Ni
2
P
with a hexagonal phase and a dendritic morphology. The growth mechanism of
Ni
2
P
dendrites involves a special solid–solution–solid transformation as well as an Ostwald ripening process. Moreover the growth of
Ni
2
P
nanodendrites occurs at the expense of
Ni
2
P
nanospheres. The effects of experimental conditions such as the volume ratio of glycol to water and solvothermal temperature on the final products were also discussed.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.jcrysgro.2007.03.002</doi><tpages>5</tpages></addata></record> |
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| source | Elsevier ScienceDirect Journals |
| subjects | A1. Characterization A1. Crystal morphology A1. Solvent A1. X-ray diffraction B1. Nanomaterials B1. Phosphides Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science rheology Exact sciences and technology Materials science Methods of deposition of films and coatings film growth and epitaxy Nanoscale materials and structures: fabrication and characterization Other topics in nanoscale materials and structures Physics Single-crystal and powder diffraction Structure of solids and liquids crystallography Theory and models of film growth X-ray diffraction and scattering |
| title | Controlled synthesis and characterization of nickel phosphide nanocrystal |
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