Synthesis of nickel-zinc ferrite nanoparticles in polyol: morphological, structural and magnetic studies
Nickel–zinc ferrite monodisperse nanoparticles are synthesized by forced hydrolysis in diethylenglycol. FC and ZFC susceptibility curves suggest that they present superparmagnetic behaviour with a blocking temperature between 63 and 15 K depending on the zinc content. The saturation magnetization of...
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| Veröffentlicht in: | Physica status solidi. A, Applications and materials science Applications and materials science, 2006-02, Vol.203 (3), p.504-512 |
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| container_title | Physica status solidi. A, Applications and materials science |
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| creator | Beji, Z. Ben Chaabane, T. Smiri, L. S. Ammar, S. Fiévet, F. Jouini, N. Grenèche, J. M. |
| description | Nickel–zinc ferrite monodisperse nanoparticles are synthesized by forced hydrolysis in diethylenglycol. FC and ZFC susceptibility curves suggest that they present superparmagnetic behaviour with a blocking temperature between 63 and 15 K depending on the zinc content. The saturation magnetization of the nanocrystals at 5 K is very close to that of bulk materials, and very high compared to that of similar particles prepared by other chemical routes. High Resolution Transmission Electron Microscopy and In‐field Mössbauer studies show clearly that these relatively high values are mainly due to: (i) the high crystalline quality of the particles and (ii) a cation distribution different from the classical distribution encountered in the bulk material. (© 2006 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim) |
| doi_str_mv | 10.1002/pssa.200521454 |
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High Resolution Transmission Electron Microscopy and In‐field Mössbauer studies show clearly that these relatively high values are mainly due to: (i) the high crystalline quality of the particles and (ii) a cation distribution different from the classical distribution encountered in the bulk material. (© 2006 WILEY‐VCH Verlag GmbH & Co. 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M.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of nickel-zinc ferrite nanoparticles in polyol: morphological, structural and magnetic studies</atitle><jtitle>Physica status solidi. A, Applications and materials science</jtitle><addtitle>phys. stat. sol. (a)</addtitle><date>2006-02</date><risdate>2006</risdate><volume>203</volume><issue>3</issue><spage>504</spage><epage>512</epage><pages>504-512</pages><issn>1862-6300</issn><issn>0031-8965</issn><eissn>1862-6319</eissn><abstract>Nickel–zinc ferrite monodisperse nanoparticles are synthesized by forced hydrolysis in diethylenglycol. FC and ZFC susceptibility curves suggest that they present superparmagnetic behaviour with a blocking temperature between 63 and 15 K depending on the zinc content. The saturation magnetization of the nanocrystals at 5 K is very close to that of bulk materials, and very high compared to that of similar particles prepared by other chemical routes. 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| source | Wiley Online Library Journals Frontfile Complete |
| subjects | 61.46.+w 68.37.Lp 75.50.Ee 75.60.Ej 75.75.+a 76.80.+y Condensed matter: electronic structure, electrical, magnetic, and optical properties Diamagnetism, paramagnetism and superparamagnetism Exact sciences and technology Magnetic properties and materials Magnetic properties of nanostructures Magnetic resonances and relaxations in condensed matter, mössbauer effect Mössbauer effect other γ-ray spectroscopy Physics |
| title | Synthesis of nickel-zinc ferrite nanoparticles in polyol: morphological, structural and magnetic studies |
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