High-yield solvothermal synthesis of single-crystalline tin oxide tetragonal prism nanorods

The tetragonal prism SnO 2 nanorods with the rutile structure have been successfully synthesized by a simple solvothermal method from high concentration precursors without any surfactant. Their sizes, morphologies and structure were studied by X-ray diffraction (XRD), field-emission scanning electro...

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Veröffentlicht in:Materials letters 2007-02, Vol.61 (4), p.1214-1217
Hauptverfasser: Xia, Linsheng, Yang, Beifang, Fu, Zhengping, Yang, Yingling, Yan, Hongwei, Xu, Yuandong, Fu, Shengquan, Li, Gongpu
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container_end_page 1217
container_issue 4
container_start_page 1214
container_title Materials letters
container_volume 61
creator Xia, Linsheng
Yang, Beifang
Fu, Zhengping
Yang, Yingling
Yan, Hongwei
Xu, Yuandong
Fu, Shengquan
Li, Gongpu
description The tetragonal prism SnO 2 nanorods with the rutile structure have been successfully synthesized by a simple solvothermal method from high concentration precursors without any surfactant. Their sizes, morphologies and structure were studied by X-ray diffraction (XRD), field-emission scanning electron microscopy (FESEM), select-area electron diffraction (SAED) and high-resolution transmission electron microscopy (HRTEM). The SnO 2 nanorods obtained by the solvothermal method exhibit higher crystalline quality and better dispersion compared with the samples prepared by the hydrothermal method. Our results suggest that the solvent plays an important role to obtain high-yield SnO 2 nanorods with high quality.
doi_str_mv 10.1016/j.matlet.2006.07.001
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subjects Nanomaterials
Semiconductors
Single-crystalline
SnO 2 nanorods
Solvothermal synthesis
title High-yield solvothermal synthesis of single-crystalline tin oxide tetragonal prism nanorods
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