High-yield solvothermal synthesis of single-crystalline tin oxide tetragonal prism nanorods
The tetragonal prism SnO 2 nanorods with the rutile structure have been successfully synthesized by a simple solvothermal method from high concentration precursors without any surfactant. Their sizes, morphologies and structure were studied by X-ray diffraction (XRD), field-emission scanning electro...
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Veröffentlicht in: | Materials letters 2007-02, Vol.61 (4), p.1214-1217 |
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creator | Xia, Linsheng Yang, Beifang Fu, Zhengping Yang, Yingling Yan, Hongwei Xu, Yuandong Fu, Shengquan Li, Gongpu |
description | The tetragonal prism SnO
2 nanorods with the rutile structure have been successfully synthesized by a simple solvothermal method from high concentration precursors without any surfactant. Their sizes, morphologies and structure were studied by X-ray diffraction (XRD), field-emission scanning electron microscopy (FESEM), select-area electron diffraction (SAED) and high-resolution transmission electron microscopy (HRTEM). The SnO
2 nanorods obtained by the solvothermal method exhibit higher crystalline quality and better dispersion compared with the samples prepared by the hydrothermal method. Our results suggest that the solvent plays an important role to obtain high-yield SnO
2 nanorods with high quality. |
doi_str_mv | 10.1016/j.matlet.2006.07.001 |
format | Article |
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2 nanorods with the rutile structure have been successfully synthesized by a simple solvothermal method from high concentration precursors without any surfactant. Their sizes, morphologies and structure were studied by X-ray diffraction (XRD), field-emission scanning electron microscopy (FESEM), select-area electron diffraction (SAED) and high-resolution transmission electron microscopy (HRTEM). The SnO
2 nanorods obtained by the solvothermal method exhibit higher crystalline quality and better dispersion compared with the samples prepared by the hydrothermal method. Our results suggest that the solvent plays an important role to obtain high-yield SnO
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2 nanorods with the rutile structure have been successfully synthesized by a simple solvothermal method from high concentration precursors without any surfactant. Their sizes, morphologies and structure were studied by X-ray diffraction (XRD), field-emission scanning electron microscopy (FESEM), select-area electron diffraction (SAED) and high-resolution transmission electron microscopy (HRTEM). The SnO
2 nanorods obtained by the solvothermal method exhibit higher crystalline quality and better dispersion compared with the samples prepared by the hydrothermal method. Our results suggest that the solvent plays an important role to obtain high-yield SnO
2 nanorods with high quality.</description><subject>Nanomaterials</subject><subject>Semiconductors</subject><subject>Single-crystalline</subject><subject>SnO 2 nanorods</subject><subject>Solvothermal synthesis</subject><issn>0167-577X</issn><issn>1873-4979</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2007</creationdate><recordtype>article</recordtype><recordid>eNqNkDFrHDEQhYVJwBcn_yDFVu52M1rpVqvGEExiBwxuHAikEDpp9qxDKzka2eT-fWQudUg1r_i-B_MY-8hh4MCnT4dhtTViHUaAaQA1APAztuGzEr3USr9hm4apfqvUj3P2jugAAFKD3LCft2H_2B8DRt9Rji-5PmJZbezomFqkQF1eOgppH7F35UjVxhgSdjWkLv8OviWsxe5zatJTCbR2yaZcsqf37O1iI-GHv_eCff_65eH6tr-7v_l2_fmud2Kaaz9PI9h5nPlO7HDxwu80t2oCobwTjiu506NfgC9ScYdaohRaKOm2zXbjjOKCXZ56n0r-9YxUzRrIYYw2YX4mM-pJTdO8_Q9QgNASGihPoCuZqOBi2merLUfDwbxObg7mNLl5ndyAMm3ypl2dNGzfvgQshlzA5NCHgq4an8O_C_4AeOGN4g</recordid><startdate>20070201</startdate><enddate>20070201</enddate><creator>Xia, Linsheng</creator><creator>Yang, Beifang</creator><creator>Fu, Zhengping</creator><creator>Yang, Yingling</creator><creator>Yan, Hongwei</creator><creator>Xu, Yuandong</creator><creator>Fu, Shengquan</creator><creator>Li, Gongpu</creator><general>Elsevier B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20070201</creationdate><title>High-yield solvothermal synthesis of single-crystalline tin oxide tetragonal prism nanorods</title><author>Xia, Linsheng ; Yang, Beifang ; Fu, Zhengping ; Yang, Yingling ; Yan, Hongwei ; Xu, Yuandong ; Fu, Shengquan ; Li, Gongpu</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c368t-8620a8281b3befd3db91a76037dc3c174b92df01f471ce94e439374c5368c28e3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2007</creationdate><topic>Nanomaterials</topic><topic>Semiconductors</topic><topic>Single-crystalline</topic><topic>SnO 2 nanorods</topic><topic>Solvothermal synthesis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Xia, Linsheng</creatorcontrib><creatorcontrib>Yang, Beifang</creatorcontrib><creatorcontrib>Fu, Zhengping</creatorcontrib><creatorcontrib>Yang, Yingling</creatorcontrib><creatorcontrib>Yan, Hongwei</creatorcontrib><creatorcontrib>Xu, Yuandong</creatorcontrib><creatorcontrib>Fu, Shengquan</creatorcontrib><creatorcontrib>Li, Gongpu</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Materials letters</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Xia, Linsheng</au><au>Yang, Beifang</au><au>Fu, Zhengping</au><au>Yang, Yingling</au><au>Yan, Hongwei</au><au>Xu, Yuandong</au><au>Fu, Shengquan</au><au>Li, Gongpu</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>High-yield solvothermal synthesis of single-crystalline tin oxide tetragonal prism nanorods</atitle><jtitle>Materials letters</jtitle><date>2007-02-01</date><risdate>2007</risdate><volume>61</volume><issue>4</issue><spage>1214</spage><epage>1217</epage><pages>1214-1217</pages><issn>0167-577X</issn><eissn>1873-4979</eissn><abstract>The tetragonal prism SnO
2 nanorods with the rutile structure have been successfully synthesized by a simple solvothermal method from high concentration precursors without any surfactant. Their sizes, morphologies and structure were studied by X-ray diffraction (XRD), field-emission scanning electron microscopy (FESEM), select-area electron diffraction (SAED) and high-resolution transmission electron microscopy (HRTEM). The SnO
2 nanorods obtained by the solvothermal method exhibit higher crystalline quality and better dispersion compared with the samples prepared by the hydrothermal method. Our results suggest that the solvent plays an important role to obtain high-yield SnO
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subjects | Nanomaterials Semiconductors Single-crystalline SnO 2 nanorods Solvothermal synthesis |
title | High-yield solvothermal synthesis of single-crystalline tin oxide tetragonal prism nanorods |
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