Spark-plasma-sintering (SPS) of nanostructured titanium carbonitride powders
Spark-plasma-sintering (SPS) compaction experiments of nanostructured titanium carbonitride powders have been performed at 1600 °C and 1800 °C (sintering time = 1 min). The as-received nanostructured powders have been synthesized through rapid condensation from the gas-phase (high frequency plasma)....
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Veröffentlicht in: | Journal of the European Ceramic Society 2005-07, Vol.25 (11), p.1919-1927 |
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container_end_page | 1927 |
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container_issue | 11 |
container_start_page | 1919 |
container_title | Journal of the European Ceramic Society |
container_volume | 25 |
creator | Angerer, P. Yu, L.G. Khor, K.A. Korb, G. Zalite, I. |
description | Spark-plasma-sintering (SPS) compaction experiments of nanostructured titanium carbonitride powders have been performed at 1600
°C and 1800
°C (sintering time = 1
min). The as-received nanostructured powders have been synthesized through rapid condensation from the gas-phase (high frequency plasma). The sintering results were compared with data obtained by various conventional sintering techniques such as pressureless sintering, gas pressure sintering, and hot pressing. The phase composition and the crystallite size were investigated by X-ray diffraction (XRD). The fracture surfaces of the sintered samples were inspected with scanning electron microscopy (SEM). The experiments show that the SPS method is capable of obtaining high densities (∼94% of theoretical density) combined with small grain-size quotient
d/
d
0 of 5.4–6.5. |
doi_str_mv | 10.1016/j.jeurceramsoc.2004.06.008 |
format | Article |
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°C and 1800
°C (sintering time = 1
min). The as-received nanostructured powders have been synthesized through rapid condensation from the gas-phase (high frequency plasma). The sintering results were compared with data obtained by various conventional sintering techniques such as pressureless sintering, gas pressure sintering, and hot pressing. The phase composition and the crystallite size were investigated by X-ray diffraction (XRD). The fracture surfaces of the sintered samples were inspected with scanning electron microscopy (SEM). The experiments show that the SPS method is capable of obtaining high densities (∼94% of theoretical density) combined with small grain-size quotient
d/
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0 of 5.4–6.5.</description><identifier>ISSN: 0955-2219</identifier><identifier>EISSN: 1873-619X</identifier><identifier>DOI: 10.1016/j.jeurceramsoc.2004.06.008</identifier><language>eng</language><publisher>Oxford: Elsevier Ltd</publisher><subject>Applied sciences ; Building materials. Ceramics. Glasses ; Carbonitride ; Ceramic industries ; Chemical industry and chemicals ; Exact sciences and technology ; Grain-size ; Microstructure ; Miscellaneous ; Spark-plasma-sintering ; Technical ceramics ; TiCN</subject><ispartof>Journal of the European Ceramic Society, 2005-07, Vol.25 (11), p.1919-1927</ispartof><rights>2004 Elsevier Ltd</rights><rights>2005 INIST-CNRS</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c627t-529770bae906b78ddb57225b560015fcc64369275bb4fa451d339a70b389418e3</citedby><cites>FETCH-LOGICAL-c627t-529770bae906b78ddb57225b560015fcc64369275bb4fa451d339a70b389418e3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0955221904002791$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65534</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=16860657$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Angerer, P.</creatorcontrib><creatorcontrib>Yu, L.G.</creatorcontrib><creatorcontrib>Khor, K.A.</creatorcontrib><creatorcontrib>Korb, G.</creatorcontrib><creatorcontrib>Zalite, I.</creatorcontrib><title>Spark-plasma-sintering (SPS) of nanostructured titanium carbonitride powders</title><title>Journal of the European Ceramic Society</title><description>Spark-plasma-sintering (SPS) compaction experiments of nanostructured titanium carbonitride powders have been performed at 1600
°C and 1800
°C (sintering time = 1
min). The as-received nanostructured powders have been synthesized through rapid condensation from the gas-phase (high frequency plasma). The sintering results were compared with data obtained by various conventional sintering techniques such as pressureless sintering, gas pressure sintering, and hot pressing. The phase composition and the crystallite size were investigated by X-ray diffraction (XRD). The fracture surfaces of the sintered samples were inspected with scanning electron microscopy (SEM). The experiments show that the SPS method is capable of obtaining high densities (∼94% of theoretical density) combined with small grain-size quotient
d/
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0 of 5.4–6.5.</description><subject>Applied sciences</subject><subject>Building materials. Ceramics. Glasses</subject><subject>Carbonitride</subject><subject>Ceramic industries</subject><subject>Chemical industry and chemicals</subject><subject>Exact sciences and technology</subject><subject>Grain-size</subject><subject>Microstructure</subject><subject>Miscellaneous</subject><subject>Spark-plasma-sintering</subject><subject>Technical ceramics</subject><subject>TiCN</subject><issn>0955-2219</issn><issn>1873-619X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2005</creationdate><recordtype>article</recordtype><recordid>eNqNkV2L1DAUhsOi4Lj6H8qCohetJ2mTNN7Juh_CgMKs4F1I01PJ2CY1SZX999thFtY75-rcPOd9D-ch5IJCRYGKD_tqj0u0GM2Ugq0YQFOBqADaM7KhraxLQdWPZ2QDivOSMapekJcp7QGoBKU2ZLubTfxVzqNJkymT8xmj8z-Ld7tvu_dFGApvfEg5LjYvEfsiu2y8W6bCmtgF73J0PRZz-NtjTK_I88GMCV8_znPy_frq7vK23H69-XL5aVtawWQuOVNSQmdQgehk2_cdl4zxjov1LD5YK5paKCZ51zWDaTjt61qZdaNuVUNbrM_J22PuHMPvBVPWk0sWx9F4DEvSTAkGUsoTwQb-D7aiUYKfBDLVspNAYJLyFfx4BG0MKUUc9BzdZOK9pqAPkvVe_ytZHyRrEHqVvC6_eWwxyZpxiMZbl54SxNoi-OERn48crlr-OIw6WYfeYu8i2qz74E6pewDQeMMs</recordid><startdate>20050701</startdate><enddate>20050701</enddate><creator>Angerer, P.</creator><creator>Yu, L.G.</creator><creator>Khor, K.A.</creator><creator>Korb, G.</creator><creator>Zalite, I.</creator><general>Elsevier Ltd</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>7U5</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope><scope>7TB</scope><scope>FR3</scope></search><sort><creationdate>20050701</creationdate><title>Spark-plasma-sintering (SPS) of nanostructured titanium carbonitride powders</title><author>Angerer, P. ; Yu, L.G. ; Khor, K.A. ; Korb, G. ; Zalite, I.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c627t-529770bae906b78ddb57225b560015fcc64369275bb4fa451d339a70b389418e3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2005</creationdate><topic>Applied sciences</topic><topic>Building materials. Ceramics. Glasses</topic><topic>Carbonitride</topic><topic>Ceramic industries</topic><topic>Chemical industry and chemicals</topic><topic>Exact sciences and technology</topic><topic>Grain-size</topic><topic>Microstructure</topic><topic>Miscellaneous</topic><topic>Spark-plasma-sintering</topic><topic>Technical ceramics</topic><topic>TiCN</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Angerer, P.</creatorcontrib><creatorcontrib>Yu, L.G.</creatorcontrib><creatorcontrib>Khor, K.A.</creatorcontrib><creatorcontrib>Korb, G.</creatorcontrib><creatorcontrib>Zalite, I.</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Mechanical & Transportation Engineering Abstracts</collection><collection>Engineering Research Database</collection><jtitle>Journal of the European Ceramic Society</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Angerer, P.</au><au>Yu, L.G.</au><au>Khor, K.A.</au><au>Korb, G.</au><au>Zalite, I.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Spark-plasma-sintering (SPS) of nanostructured titanium carbonitride powders</atitle><jtitle>Journal of the European Ceramic Society</jtitle><date>2005-07-01</date><risdate>2005</risdate><volume>25</volume><issue>11</issue><spage>1919</spage><epage>1927</epage><pages>1919-1927</pages><issn>0955-2219</issn><eissn>1873-619X</eissn><abstract>Spark-plasma-sintering (SPS) compaction experiments of nanostructured titanium carbonitride powders have been performed at 1600
°C and 1800
°C (sintering time = 1
min). The as-received nanostructured powders have been synthesized through rapid condensation from the gas-phase (high frequency plasma). The sintering results were compared with data obtained by various conventional sintering techniques such as pressureless sintering, gas pressure sintering, and hot pressing. The phase composition and the crystallite size were investigated by X-ray diffraction (XRD). The fracture surfaces of the sintered samples were inspected with scanning electron microscopy (SEM). The experiments show that the SPS method is capable of obtaining high densities (∼94% of theoretical density) combined with small grain-size quotient
d/
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source | Elsevier ScienceDirect Journals Complete |
subjects | Applied sciences Building materials. Ceramics. Glasses Carbonitride Ceramic industries Chemical industry and chemicals Exact sciences and technology Grain-size Microstructure Miscellaneous Spark-plasma-sintering Technical ceramics TiCN |
title | Spark-plasma-sintering (SPS) of nanostructured titanium carbonitride powders |
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