Spark-plasma-sintering (SPS) of nanostructured titanium carbonitride powders

Spark-plasma-sintering (SPS) compaction experiments of nanostructured titanium carbonitride powders have been performed at 1600 °C and 1800 °C (sintering time = 1 min). The as-received nanostructured powders have been synthesized through rapid condensation from the gas-phase (high frequency plasma)....

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Veröffentlicht in:Journal of the European Ceramic Society 2005-07, Vol.25 (11), p.1919-1927
Hauptverfasser: Angerer, P., Yu, L.G., Khor, K.A., Korb, G., Zalite, I.
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container_end_page 1927
container_issue 11
container_start_page 1919
container_title Journal of the European Ceramic Society
container_volume 25
creator Angerer, P.
Yu, L.G.
Khor, K.A.
Korb, G.
Zalite, I.
description Spark-plasma-sintering (SPS) compaction experiments of nanostructured titanium carbonitride powders have been performed at 1600 °C and 1800 °C (sintering time = 1 min). The as-received nanostructured powders have been synthesized through rapid condensation from the gas-phase (high frequency plasma). The sintering results were compared with data obtained by various conventional sintering techniques such as pressureless sintering, gas pressure sintering, and hot pressing. The phase composition and the crystallite size were investigated by X-ray diffraction (XRD). The fracture surfaces of the sintered samples were inspected with scanning electron microscopy (SEM). The experiments show that the SPS method is capable of obtaining high densities (∼94% of theoretical density) combined with small grain-size quotient d/ d 0 of 5.4–6.5.
doi_str_mv 10.1016/j.jeurceramsoc.2004.06.008
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subjects Applied sciences
Building materials. Ceramics. Glasses
Carbonitride
Ceramic industries
Chemical industry and chemicals
Exact sciences and technology
Grain-size
Microstructure
Miscellaneous
Spark-plasma-sintering
Technical ceramics
TiCN
title Spark-plasma-sintering (SPS) of nanostructured titanium carbonitride powders
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