Sulfonation of (glycidyl methacrylate) chains grafted onto nonwoven polypropylene fabric

Sulfonation of (glycidyl methacrylate) chains grafted onto nonwoven polypropylene fabric

Sulfonation of polyglycidyl methacrylate (PGMA) chains grafted onto nonwoven polypropylene fabric is investigated in detail. Sulfonation reaction consists in implantation of sulfonate groups via epoxy ring‐opening of PGMA chains grafted onto nonwoven polypropylene fabric by reaction between the GMA‐...

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Veröffentlicht in:Journal of applied polymer science 2007-06, Vol.104 (5), p.3256-3260
Hauptverfasser: Bondar, Yuliya V., Kim, Hong Je, Lim, Yong Jin
Format: Artikel
Sprache:eng
Schlagworte:
Applied sciences
electron beam irradiation
Exact sciences and technology
fibers
Fibers and threads
Forms of application and semi-finished materials
functionalization of polymers
Polymer industry, paints, wood
polypropylene (PP)
synthesis
Technology of polymers
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creator Bondar, Yuliya V.
Kim, Hong Je
Lim, Yong Jin
description Sulfonation of polyglycidyl methacrylate (PGMA) chains grafted onto nonwoven polypropylene fabric is investigated in detail. Sulfonation reaction consists in implantation of sulfonate groups via epoxy ring‐opening of PGMA chains grafted onto nonwoven polypropylene fabric by reaction between the GMA‐grafted sample and sodium hydrogensulfite in water–dimethylformamide solution. On the basis of analyses of IR spectra of the appropriate samples and data of backward titration, two simultaneous processes are demonstrated to take place during the sulfonation reaction. These processes are the implantation of sulfonate groups via opening of the GMA epoxy rings and hydrolysis of the GMA epoxy rings with α‐glycol groups formation. The main peculiarities of the sulfonation reaction in depending on the GMA grafting degree are reported. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci, 2007
doi_str_mv 10.1002/app.25887
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Sulfonation reaction consists in implantation of sulfonate groups via epoxy ring‐opening of PGMA chains grafted onto nonwoven polypropylene fabric by reaction between the GMA‐grafted sample and sodium hydrogensulfite in water–dimethylformamide solution. On the basis of analyses of IR spectra of the appropriate samples and data of backward titration, two simultaneous processes are demonstrated to take place during the sulfonation reaction. These processes are the implantation of sulfonate groups via opening of the GMA epoxy rings and hydrolysis of the GMA epoxy rings with α‐glycol groups formation. The main peculiarities of the sulfonation reaction in depending on the GMA grafting degree are reported. © 2007 Wiley Periodicals, Inc. 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subjects Applied sciences
electron beam irradiation
Exact sciences and technology
fibers
Fibers and threads
Forms of application and semi-finished materials
functionalization of polymers
Polymer industry, paints, wood
polypropylene (PP)
synthesis
Technology of polymers
title Sulfonation of (glycidyl methacrylate) chains grafted onto nonwoven polypropylene fabric
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