The suitability of XRF analysis for compositional classification of archaeological ceramic fabric: A comparison with a previous NAA study
The main drawbacks of EDXRF techniques, restricting its more frequent use for the specific purpose of compositional analysis of archaeological ceramic fabric, have been the insufficient sensitivity to determine some important elements (like Cr, REE, among others), a somewhat worse precision and the...
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| Veröffentlicht in: | Analytica chimica acta 2006-02, Vol.558 (1), p.283-289 |
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| creator | Padilla, R. Espen, P. Van Torres, P.P. Godo |
| description | The main drawbacks of EDXRF techniques, restricting its more frequent use for the specific purpose of compositional analysis of archaeological ceramic fabric, have been the insufficient sensitivity to determine some important elements (like Cr, REE, among others), a somewhat worse precision and the inability to perform standard-less quantitative procedures in the absence of suitable certified reference materials (CRM) for ceramic fabric. This paper presents the advantages of combining two energy dispersive X-ray fluorescence methods for fast and non-destructive analysis of ceramic fabric with increased sensitivity. Selective polarized excitation using secondary targets (EDPXRF) and radioisotope excitation (R-XRF) using a
241Am source. The analytical performance of the methods was evaluated by analyzing several CRM of sediment type, and the fitness for the purpose of compositional classification was compared with that obtained by using Instrumental Neutron Activation Analysis in a previous study of Cuban aborigine pottery. |
| doi_str_mv | 10.1016/j.aca.2005.10.077 |
| format | Article |
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241Am source. The analytical performance of the methods was evaluated by analyzing several CRM of sediment type, and the fitness for the purpose of compositional classification was compared with that obtained by using Instrumental Neutron Activation Analysis in a previous study of Cuban aborigine pottery.</description><subject>Analytical chemistry</subject><subject>Archaeological pottery</subject><subject>Chemistry</subject><subject>Compositional classification</subject><subject>Energy dispersive X-ray fluorescence analysis</subject><subject>Exact sciences and technology</subject><subject>Radiochemical methods</subject><subject>Spectrometric and optical methods</subject><issn>0003-2670</issn><issn>1873-4324</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2006</creationdate><recordtype>article</recordtype><recordid>eNp9kEGP0zAQhS0EEmXhB3DzBW4pduI0CZyqFbuLtAIJ7UrcrMlkTKdK6-JJF_Un7L_GoStx42Jrnr73xn5KvbVmaY1dfdguAWFZGlPneWma5pla2LapCleV7rlaGGOqolw15qV6JbLNY2mNW6jHuw1pOfIEPY88nXQM-sf3Kw17GE_CokNMGuPuEIUnjlnVOIIIB0aYhdkACTdAcYw_s5gBSrBj1AH6xPhRr_8GQGLJ-G-eNhr0IdEDx6Por-u1luk4nF6rFwFGoTdP94W6v_p8d3lT3H67_nK5vi2wqtupQFP2tGqGNriuX1nrbDm0VOejCo0bbNP3XWVrCoBoHVUY6rYFW4bW1XYwWF2o9-fcQ4q_jiST37EgjSPsKT_Il13d1LYzGbRnEFMUSRT8IfEO0slb4-fS_dbn0v1c-izl0rPn3VM4SK4iJNgjyz9jTnbOdZn7dOYo__SBKXlBpj3SwIlw8kPk_2z5AwjwmTE</recordid><startdate>20060203</startdate><enddate>20060203</enddate><creator>Padilla, R.</creator><creator>Espen, P. Van</creator><creator>Torres, P.P. Godo</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope></search><sort><creationdate>20060203</creationdate><title>The suitability of XRF analysis for compositional classification of archaeological ceramic fabric: A comparison with a previous NAA study</title><author>Padilla, R. ; Espen, P. Van ; Torres, P.P. Godo</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c358t-c02be67d8f49b611412d8e52d83f74d17bb9315efacc14e3cf588a12f8451d0c3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2006</creationdate><topic>Analytical chemistry</topic><topic>Archaeological pottery</topic><topic>Chemistry</topic><topic>Compositional classification</topic><topic>Energy dispersive X-ray fluorescence analysis</topic><topic>Exact sciences and technology</topic><topic>Radiochemical methods</topic><topic>Spectrometric and optical methods</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Padilla, R.</creatorcontrib><creatorcontrib>Espen, P. Van</creatorcontrib><creatorcontrib>Torres, P.P. Godo</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Analytica chimica acta</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Padilla, R.</au><au>Espen, P. Van</au><au>Torres, P.P. Godo</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>The suitability of XRF analysis for compositional classification of archaeological ceramic fabric: A comparison with a previous NAA study</atitle><jtitle>Analytica chimica acta</jtitle><date>2006-02-03</date><risdate>2006</risdate><volume>558</volume><issue>1</issue><spage>283</spage><epage>289</epage><pages>283-289</pages><issn>0003-2670</issn><eissn>1873-4324</eissn><coden>ACACAM</coden><abstract>The main drawbacks of EDXRF techniques, restricting its more frequent use for the specific purpose of compositional analysis of archaeological ceramic fabric, have been the insufficient sensitivity to determine some important elements (like Cr, REE, among others), a somewhat worse precision and the inability to perform standard-less quantitative procedures in the absence of suitable certified reference materials (CRM) for ceramic fabric. This paper presents the advantages of combining two energy dispersive X-ray fluorescence methods for fast and non-destructive analysis of ceramic fabric with increased sensitivity. Selective polarized excitation using secondary targets (EDPXRF) and radioisotope excitation (R-XRF) using a
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| source | Elsevier ScienceDirect Journals Complete |
| subjects | Analytical chemistry Archaeological pottery Chemistry Compositional classification Energy dispersive X-ray fluorescence analysis Exact sciences and technology Radiochemical methods Spectrometric and optical methods |
| title | The suitability of XRF analysis for compositional classification of archaeological ceramic fabric: A comparison with a previous NAA study |
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