NiCuZn ferrite thin films grown by a sol–gel method and rapid thermal annealing
Ni 0.8− x Cu 0.2Zn x Fe 2O 4 thin films were fabricated by sol–gel method and rapid thermal annealing (RTA). The X-diffraction and atomic force microscopy (AFM) measurements indicate that the films have a single-phase spinel structure with calcining temperature T⩾600 °C. The saturation magnetization...
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Veröffentlicht in: | Journal of magnetism and magnetic materials 2007-02, Vol.309 (1), p.75-79 |
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Hauptverfasser: | , , , , , |
Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | Ni
0.8−
x
Cu
0.2Zn
x
Fe
2O
4 thin films were fabricated by sol–gel method and rapid thermal annealing (RTA). The X-diffraction and atomic force microscopy (AFM) measurements indicate that the films have a single-phase spinel structure with calcining temperature T⩾600
°C. The saturation magnetization
M
s and coercivity
H
c of the films as a function of the film composition were investigated by alternating gradient magnetometer (AGM). It has been found that the
M
s increases firstly and then decreases with the increasing of Zn content. The
M
s reaches the maximum value about 271.56
emu/cm
3 for
x=0.45, meanwhile the
H
c reaches the minimum value about 15.62
Oe for
x=0.4. The processing parameters were optimized, which includes the coating concentration, the annealing temperature and time for the films. The results indicate that the coating concentration of 0.4
mol/L, crystallization at 600
°C and annealing for 5
min are suitable for NiCuZn ferrite thin film. |
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ISSN: | 0304-8853 |
DOI: | 10.1016/j.jmmm.2006.06.014 |