Nanosize ferrites obtained by ball milling: Crystal structure, cation distribution, size-strain analysis and Raman investigations
Spinels samples Fe 2.85Y 0.15O 4 (S1) and Fe 2.55In 0.45O 4 (S2), such as Fe 3O 4+ γ-Fe 2O 3 (S3) were obtained by ball milling. TEM micrograph as well as XRPD line broadening analyses show nanosize nature of the ferrite powders. Cation distribution, found by Rietveld refinement of the site occupanc...
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| Veröffentlicht in: | Solid state sciences 2006-08, Vol.8 (8), p.908-915 |
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| creator | Cvejic, Zeljka Rakic, Srdjan Kremenovic, Aleksandar Antic, Bratislav Jovalekic, Cedomir Colomban, Philippe |
| description | Spinels samples Fe
2.85Y
0.15O
4 (S1) and Fe
2.55In
0.45O
4 (S2), such as Fe
3O
4+
γ-Fe
2O
3 (S3) were obtained by ball milling. TEM micrograph as well as XRPD line broadening analyses show nanosize nature of the ferrite powders. Cation distribution, found by Rietveld refinement of the site occupancies, indicate Y
3+ ions presence at 16d sites in Fe
2.85Y
0.15O
4, and a random In
3+ ions distribution on both 8a and 16d sites in Fe
2.55In
0.45O
4 (space group Fd
3
¯
m
). From the XRPD line broadening analysis crystallite size and strain values were determined. The crystallite size and strain anisotropy is significant, especially for Fe
2.85Y
0.15O
4 and Fe
2.55In
0.45O
4. This result is discussed regarding the influence of the cation substitutions. The Raman signature confirms the spinel structure and the homogeneity of the particles. |
| doi_str_mv | 10.1016/j.solidstatesciences.2006.02.041 |
| format | Article |
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2.85Y
0.15O
4 (S1) and Fe
2.55In
0.45O
4 (S2), such as Fe
3O
4+
γ-Fe
2O
3 (S3) were obtained by ball milling. TEM micrograph as well as XRPD line broadening analyses show nanosize nature of the ferrite powders. Cation distribution, found by Rietveld refinement of the site occupancies, indicate Y
3+ ions presence at 16d sites in Fe
2.85Y
0.15O
4, and a random In
3+ ions distribution on both 8a and 16d sites in Fe
2.55In
0.45O
4 (space group Fd
3
¯
m
). From the XRPD line broadening analysis crystallite size and strain values were determined. The crystallite size and strain anisotropy is significant, especially for Fe
2.85Y
0.15O
4 and Fe
2.55In
0.45O
4. This result is discussed regarding the influence of the cation substitutions. The Raman signature confirms the spinel structure and the homogeneity of the particles.</description><identifier>ISSN: 1293-2558</identifier><identifier>EISSN: 1873-3085</identifier><identifier>DOI: 10.1016/j.solidstatesciences.2006.02.041</identifier><language>eng</language><publisher>Paris: Elsevier Masson SAS</publisher><subject>Condensed matter: electronic structure, electrical, magnetic, and optical properties ; Condensed matter: structure, mechanical and thermal properties ; Exact sciences and technology ; Infrared and raman spectra and scattering ; Inorganic compounds ; Mechanochemical treatment ; Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation ; Other nonmetallic inorganics ; Physics ; Raman spectra ; Rietveld's analysis ; Spinel ferrites ; Structure of solids and liquids; crystallography ; Structure of specific crystalline solids ; Water, oxides, hydroxides, peroxides</subject><ispartof>Solid state sciences, 2006-08, Vol.8 (8), p.908-915</ispartof><rights>2006 Elsevier SAS</rights><rights>2006 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c469t-40080e6c6300c298fc4c53e71a6a6a9ebcff214da9cc1835cadfab4137c7ba73</citedby><cites>FETCH-LOGICAL-c469t-40080e6c6300c298fc4c53e71a6a6a9ebcff214da9cc1835cadfab4137c7ba73</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S1293255806000914$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65306</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=17984704$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Cvejic, Zeljka</creatorcontrib><creatorcontrib>Rakic, Srdjan</creatorcontrib><creatorcontrib>Kremenovic, Aleksandar</creatorcontrib><creatorcontrib>Antic, Bratislav</creatorcontrib><creatorcontrib>Jovalekic, Cedomir</creatorcontrib><creatorcontrib>Colomban, Philippe</creatorcontrib><title>Nanosize ferrites obtained by ball milling: Crystal structure, cation distribution, size-strain analysis and Raman investigations</title><title>Solid state sciences</title><description>Spinels samples Fe
2.85Y
0.15O
4 (S1) and Fe
2.55In
0.45O
4 (S2), such as Fe
3O
4+
γ-Fe
2O
3 (S3) were obtained by ball milling. TEM micrograph as well as XRPD line broadening analyses show nanosize nature of the ferrite powders. Cation distribution, found by Rietveld refinement of the site occupancies, indicate Y
3+ ions presence at 16d sites in Fe
2.85Y
0.15O
4, and a random In
3+ ions distribution on both 8a and 16d sites in Fe
2.55In
0.45O
4 (space group Fd
3
¯
m
). From the XRPD line broadening analysis crystallite size and strain values were determined. The crystallite size and strain anisotropy is significant, especially for Fe
2.85Y
0.15O
4 and Fe
2.55In
0.45O
4. This result is discussed regarding the influence of the cation substitutions. The Raman signature confirms the spinel structure and the homogeneity of the particles.</description><subject>Condensed matter: electronic structure, electrical, magnetic, and optical properties</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Exact sciences and technology</subject><subject>Infrared and raman spectra and scattering</subject><subject>Inorganic compounds</subject><subject>Mechanochemical treatment</subject><subject>Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation</subject><subject>Other nonmetallic inorganics</subject><subject>Physics</subject><subject>Raman spectra</subject><subject>Rietveld's analysis</subject><subject>Spinel ferrites</subject><subject>Structure of solids and liquids; crystallography</subject><subject>Structure of specific crystalline solids</subject><subject>Water, oxides, hydroxides, peroxides</subject><issn>1293-2558</issn><issn>1873-3085</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2006</creationdate><recordtype>article</recordtype><recordid>eNqNkE1v1DAQhiMEEqXwH3wBcWiCHTtfnEArvqqKSlXv1mTiVLPyOsXjVNre-s_xsitx4ILm4JnRO88rv0XxXslKSdV-2Fa8eJo4QXKM5AI6rmop20rWlTTqWXGm-k6XWvbN89zXgy7rpulfFq-YtzIL286cFU8_ISxMj07MLkbKLLGMCSi4SYx7MYL3YkfeU7j7KDZxn_284BRXTGt0FwIh0RLERHlH43oYLsSBV-ZFxggI4PdMnJtJ3MAOgqDw4DjR3Z9Tfl28mMGze3N6z4vbr19uN9_Lq-tvPzafr0o07ZBKI2UvXYutlhLroZ_RYKNdp6DNNbgR57lWZoIBUfW6QZhmGI3SHXYjdPq8eHfE3sfl15r97Y4YnfcQ3LKyrQejG6OaLPx0FGJcmKOb7X2kHcS9VdIeordb-2_09hC9lbXN0WfE25MXMIKfIwQk_svpht500mTd5VHn8r8fyEV7wk0UHSY7LfT_pr8Bzd6rAA</recordid><startdate>20060801</startdate><enddate>20060801</enddate><creator>Cvejic, Zeljka</creator><creator>Rakic, Srdjan</creator><creator>Kremenovic, Aleksandar</creator><creator>Antic, Bratislav</creator><creator>Jovalekic, Cedomir</creator><creator>Colomban, Philippe</creator><general>Elsevier Masson SAS</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope></search><sort><creationdate>20060801</creationdate><title>Nanosize ferrites obtained by ball milling: Crystal structure, cation distribution, size-strain analysis and Raman investigations</title><author>Cvejic, Zeljka ; Rakic, Srdjan ; Kremenovic, Aleksandar ; Antic, Bratislav ; Jovalekic, Cedomir ; Colomban, Philippe</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c469t-40080e6c6300c298fc4c53e71a6a6a9ebcff214da9cc1835cadfab4137c7ba73</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2006</creationdate><topic>Condensed matter: electronic structure, electrical, magnetic, and optical properties</topic><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Exact sciences and technology</topic><topic>Infrared and raman spectra and scattering</topic><topic>Inorganic compounds</topic><topic>Mechanochemical treatment</topic><topic>Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation</topic><topic>Other nonmetallic inorganics</topic><topic>Physics</topic><topic>Raman spectra</topic><topic>Rietveld's analysis</topic><topic>Spinel ferrites</topic><topic>Structure of solids and liquids; crystallography</topic><topic>Structure of specific crystalline solids</topic><topic>Water, oxides, hydroxides, peroxides</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Cvejic, Zeljka</creatorcontrib><creatorcontrib>Rakic, Srdjan</creatorcontrib><creatorcontrib>Kremenovic, Aleksandar</creatorcontrib><creatorcontrib>Antic, Bratislav</creatorcontrib><creatorcontrib>Jovalekic, Cedomir</creatorcontrib><creatorcontrib>Colomban, Philippe</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Solid state sciences</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Cvejic, Zeljka</au><au>Rakic, Srdjan</au><au>Kremenovic, Aleksandar</au><au>Antic, Bratislav</au><au>Jovalekic, Cedomir</au><au>Colomban, Philippe</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Nanosize ferrites obtained by ball milling: Crystal structure, cation distribution, size-strain analysis and Raman investigations</atitle><jtitle>Solid state sciences</jtitle><date>2006-08-01</date><risdate>2006</risdate><volume>8</volume><issue>8</issue><spage>908</spage><epage>915</epage><pages>908-915</pages><issn>1293-2558</issn><eissn>1873-3085</eissn><abstract>Spinels samples Fe
2.85Y
0.15O
4 (S1) and Fe
2.55In
0.45O
4 (S2), such as Fe
3O
4+
γ-Fe
2O
3 (S3) were obtained by ball milling. TEM micrograph as well as XRPD line broadening analyses show nanosize nature of the ferrite powders. Cation distribution, found by Rietveld refinement of the site occupancies, indicate Y
3+ ions presence at 16d sites in Fe
2.85Y
0.15O
4, and a random In
3+ ions distribution on both 8a and 16d sites in Fe
2.55In
0.45O
4 (space group Fd
3
¯
m
). From the XRPD line broadening analysis crystallite size and strain values were determined. The crystallite size and strain anisotropy is significant, especially for Fe
2.85Y
0.15O
4 and Fe
2.55In
0.45O
4. This result is discussed regarding the influence of the cation substitutions. The Raman signature confirms the spinel structure and the homogeneity of the particles.</abstract><cop>Paris</cop><pub>Elsevier Masson SAS</pub><doi>10.1016/j.solidstatesciences.2006.02.041</doi><tpages>8</tpages></addata></record> |
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| subjects | Condensed matter: electronic structure, electrical, magnetic, and optical properties Condensed matter: structure, mechanical and thermal properties Exact sciences and technology Infrared and raman spectra and scattering Inorganic compounds Mechanochemical treatment Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation Other nonmetallic inorganics Physics Raman spectra Rietveld's analysis Spinel ferrites Structure of solids and liquids crystallography Structure of specific crystalline solids Water, oxides, hydroxides, peroxides |
| title | Nanosize ferrites obtained by ball milling: Crystal structure, cation distribution, size-strain analysis and Raman investigations |
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