Hydrothermal synthesis of hydroxyapatite nanopowders using cationic surfactant as a template
Hydroxyapatite (HAp) nanoparticles with uniform morphologies and controllable size have been synthesized successfully by low-temperature hydrothermal method. The cationic surfactant CTAB as a template is used to regulate the nucleation and crystal growth. The synthesized powders were characterized u...
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Veröffentlicht in: | Materials letters 2006-06, Vol.60 (12), p.1484-1487 |
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creator | Wang, Yingjun Zhang, Shuhua Wei, Kun Zhao, Naru Chen, Jingdi Wang, Xudong |
description | Hydroxyapatite (HAp) nanoparticles with uniform morphologies and controllable size have been synthesized successfully by low-temperature hydrothermal method. The cationic surfactant CTAB as a template is used to regulate the nucleation and crystal growth. The synthesized powders were characterized using X-ray diffraction, Fourier transform infrared spectrograph and transmission electron microscopy. The results indicate that the obtained particles are uniform rod-like monocrystals. Compared with the reaction time, the temperature of reaction is more significant variable in altering the HAp morphology and size. Furthermore, the behavior mechanism of CTAB is discussed. |
doi_str_mv | 10.1016/j.matlet.2005.11.053 |
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The cationic surfactant CTAB as a template is used to regulate the nucleation and crystal growth. The synthesized powders were characterized using X-ray diffraction, Fourier transform infrared spectrograph and transmission electron microscopy. The results indicate that the obtained particles are uniform rod-like monocrystals. Compared with the reaction time, the temperature of reaction is more significant variable in altering the HAp morphology and size. Furthermore, the behavior mechanism of CTAB is discussed.</description><identifier>ISSN: 0167-577X</identifier><identifier>EISSN: 1873-4979</identifier><identifier>DOI: 10.1016/j.matlet.2005.11.053</identifier><language>eng</language><publisher>Elsevier B.V</publisher><subject>Hydrothermal synthesis ; Hydroxyapatite ; Surfactant ; Template</subject><ispartof>Materials letters, 2006-06, Vol.60 (12), p.1484-1487</ispartof><rights>2005 Elsevier B.V.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c465t-da5d98b10c4666329b06981a0a028abb52d1e33bfb506602726fd431cab642ff3</citedby><cites>FETCH-LOGICAL-c465t-da5d98b10c4666329b06981a0a028abb52d1e33bfb506602726fd431cab642ff3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.matlet.2005.11.053$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids></links><search><creatorcontrib>Wang, Yingjun</creatorcontrib><creatorcontrib>Zhang, Shuhua</creatorcontrib><creatorcontrib>Wei, Kun</creatorcontrib><creatorcontrib>Zhao, Naru</creatorcontrib><creatorcontrib>Chen, Jingdi</creatorcontrib><creatorcontrib>Wang, Xudong</creatorcontrib><title>Hydrothermal synthesis of hydroxyapatite nanopowders using cationic surfactant as a template</title><title>Materials letters</title><description>Hydroxyapatite (HAp) nanoparticles with uniform morphologies and controllable size have been synthesized successfully by low-temperature hydrothermal method. The cationic surfactant CTAB as a template is used to regulate the nucleation and crystal growth. The synthesized powders were characterized using X-ray diffraction, Fourier transform infrared spectrograph and transmission electron microscopy. The results indicate that the obtained particles are uniform rod-like monocrystals. Compared with the reaction time, the temperature of reaction is more significant variable in altering the HAp morphology and size. Furthermore, the behavior mechanism of CTAB is discussed.</description><subject>Hydrothermal synthesis</subject><subject>Hydroxyapatite</subject><subject>Surfactant</subject><subject>Template</subject><issn>0167-577X</issn><issn>1873-4979</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2006</creationdate><recordtype>article</recordtype><recordid>eNqNkUFr3DAQhUVJoJs0_6AHnXKzO5Js2boESkiTQiCXFnoIiLE8brTYlitp0-y_r5ftOclpZpjvPYZ5jH0WUAoQ-su2nDCPlEsJUJdClFCrD2wj2kYVlWnMCdusWFPUTfPrIztLaQsAlYFqwx7v9n0M-YnihCNP-3ltk088DPzpsHnZ44LZZ-IzzmEJf3uKie-Sn39zty7C7B1PuzigyzhnjokjzzQtI2b6xE4HHBNd_K_n7Oe3mx_Xd8X9w-3366_3hat0nYse6960nYB11FpJ04E2rUBAkC12XS17QUp1Q1eD1iAbqYe-UsJhpys5DOqcXR59lxj-7ChlO_nkaBxxprBLVhrVglqf8ibYgjSmad4DCpDiAFZH0MWQUqTBLtFPGPdWgD2EY7f2GI49hGOFsOsdq-zqKKP1Lc-eok3O0-yo95Fctn3wrxv8A4Lom80</recordid><startdate>20060601</startdate><enddate>20060601</enddate><creator>Wang, Yingjun</creator><creator>Zhang, Shuhua</creator><creator>Wei, Kun</creator><creator>Zhao, Naru</creator><creator>Chen, Jingdi</creator><creator>Wang, Xudong</creator><general>Elsevier B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>8FD</scope><scope>JG9</scope><scope>7SR</scope><scope>8BQ</scope></search><sort><creationdate>20060601</creationdate><title>Hydrothermal synthesis of hydroxyapatite nanopowders using cationic surfactant as a template</title><author>Wang, Yingjun ; Zhang, Shuhua ; Wei, Kun ; Zhao, Naru ; Chen, Jingdi ; Wang, Xudong</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c465t-da5d98b10c4666329b06981a0a028abb52d1e33bfb506602726fd431cab642ff3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2006</creationdate><topic>Hydrothermal synthesis</topic><topic>Hydroxyapatite</topic><topic>Surfactant</topic><topic>Template</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wang, Yingjun</creatorcontrib><creatorcontrib>Zhang, Shuhua</creatorcontrib><creatorcontrib>Wei, Kun</creatorcontrib><creatorcontrib>Zhao, Naru</creatorcontrib><creatorcontrib>Chen, Jingdi</creatorcontrib><creatorcontrib>Wang, Xudong</creatorcontrib><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><jtitle>Materials letters</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wang, Yingjun</au><au>Zhang, Shuhua</au><au>Wei, Kun</au><au>Zhao, Naru</au><au>Chen, Jingdi</au><au>Wang, Xudong</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Hydrothermal synthesis of hydroxyapatite nanopowders using cationic surfactant as a template</atitle><jtitle>Materials letters</jtitle><date>2006-06-01</date><risdate>2006</risdate><volume>60</volume><issue>12</issue><spage>1484</spage><epage>1487</epage><pages>1484-1487</pages><issn>0167-577X</issn><eissn>1873-4979</eissn><abstract>Hydroxyapatite (HAp) nanoparticles with uniform morphologies and controllable size have been synthesized successfully by low-temperature hydrothermal method. The cationic surfactant CTAB as a template is used to regulate the nucleation and crystal growth. The synthesized powders were characterized using X-ray diffraction, Fourier transform infrared spectrograph and transmission electron microscopy. The results indicate that the obtained particles are uniform rod-like monocrystals. Compared with the reaction time, the temperature of reaction is more significant variable in altering the HAp morphology and size. Furthermore, the behavior mechanism of CTAB is discussed.</abstract><pub>Elsevier B.V</pub><doi>10.1016/j.matlet.2005.11.053</doi><tpages>4</tpages></addata></record> |
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subjects | Hydrothermal synthesis Hydroxyapatite Surfactant Template |
title | Hydrothermal synthesis of hydroxyapatite nanopowders using cationic surfactant as a template |
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