Shape-controlled synthesis of PbS microcrystals in large yields via a solvothermal process

PbS microcrystals including multipods, truncated octahedrons and cubes were produced by the reaction of PbCl 2 and thiosemicarbazide (CH 5N 3S) using diethylene glycol (DEG) as a solvent at 180 °C. When the reaction time was prolonged, the final products grew into single-crystalline PbS cubes with d...

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Veröffentlicht in:Journal of crystal growth 2004-12, Vol.273 (1), p.213-219
Hauptverfasser: Xu, Liqiang, Zhang, Wanqun, Ding, Yanwei, Yu, Weichao, Xing, Jinyun, Li, Fanqing, Qian, Yitai
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Sprache:eng
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