Electrodeposition of paracetamol oxide for intelligent portable ratiometric detection of nicotine and ethyl vanillin β-D-glucoside
Herein, the electrodeposition of paracetamol oxide (PA ox) for the intelligent portable ratiometric detection of nicotine (NIC) and ethyl vanillin β-D-glucoside (EVG) is reported. PA ox electrodeposited on a screen-printed carbon electrode (SPCE) was used as a new fixed state ratiometric reference p...
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Veröffentlicht in: | Analyst (London) 2023-12, Vol.149 (1), p.188-195 |
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creator | Su, Zhaohong Hu, Shiyu Zhang, Yuhang Liang, Zhanning Peng, Yi Cao, Qinyi Yu, Xia Zhu, Zhiyang He, Pei Li, Zhenjie |
description | Herein, the electrodeposition of paracetamol oxide (PA ox) for the intelligent portable ratiometric detection of nicotine (NIC) and ethyl vanillin β-D-glucoside (EVG) is reported. PA ox electrodeposited on a screen-printed carbon electrode (SPCE) was used as a new fixed state ratiometric reference probe. A portable electrochemical workstation combined with a smart phone was applied as an intelligent portable electrochemical sensing platform. The sensor was studied by scanning electron microscopy (SEM), Fourier transform infrared spectrophotometry (FT-IR), ultraviolet-visible spectrophotometry (UV-vis), theoretical calculation, chronoamperometry, cyclic voltammetry (CV), electrochemical impedance spectroscopy (EIS) and square wave voltammetry (SWV). Under optimized conditions, the detection range of NIC is 10-200 μmol L
, and the detection limit is 0.256 μmol L
. The detection range of EVG was 10-180 μmol L
, and the detection limit was 0.058 μmol L
. The sensor can realize the real-time detection of NIC and EVG concentration in cigarette samples quickly and accurately, and has good anti-interference, repeatability and stability. |
doi_str_mv | 10.1039/d3an01718d |
format | Article |
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, and the detection limit is 0.256 μmol L
. The detection range of EVG was 10-180 μmol L
, and the detection limit was 0.058 μmol L
. The sensor can realize the real-time detection of NIC and EVG concentration in cigarette samples quickly and accurately, and has good anti-interference, repeatability and stability.</description><identifier>ISSN: 0003-2654</identifier><identifier>EISSN: 1364-5528</identifier><identifier>DOI: 10.1039/d3an01718d</identifier><identifier>PMID: 38010128</identifier><language>eng</language><publisher>England: Royal Society of Chemistry</publisher><subject>Analgesics ; Electrochemical impedance spectroscopy ; Electrodeposition ; Electrons ; Fourier transforms ; Glucosides ; Infrared spectrophotometers ; Nicotine ; Portability ; Spectrophotometry ; Square waves ; Vanillin ; Voltammetry ; Workstations</subject><ispartof>Analyst (London), 2023-12, Vol.149 (1), p.188-195</ispartof><rights>Copyright Royal Society of Chemistry 2024</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c315t-c52c4508187da65fc2707e422a369b3791b0d7c5c312b2df2f6c126a26370de63</citedby><cites>FETCH-LOGICAL-c315t-c52c4508187da65fc2707e422a369b3791b0d7c5c312b2df2f6c126a26370de63</cites><orcidid>0000-0001-7616-0770</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,2818,27901,27902</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/38010128$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Su, Zhaohong</creatorcontrib><creatorcontrib>Hu, Shiyu</creatorcontrib><creatorcontrib>Zhang, Yuhang</creatorcontrib><creatorcontrib>Liang, Zhanning</creatorcontrib><creatorcontrib>Peng, Yi</creatorcontrib><creatorcontrib>Cao, Qinyi</creatorcontrib><creatorcontrib>Yu, Xia</creatorcontrib><creatorcontrib>Zhu, Zhiyang</creatorcontrib><creatorcontrib>He, Pei</creatorcontrib><creatorcontrib>Li, Zhenjie</creatorcontrib><title>Electrodeposition of paracetamol oxide for intelligent portable ratiometric detection of nicotine and ethyl vanillin β-D-glucoside</title><title>Analyst (London)</title><addtitle>Analyst</addtitle><description>Herein, the electrodeposition of paracetamol oxide (PA ox) for the intelligent portable ratiometric detection of nicotine (NIC) and ethyl vanillin β-D-glucoside (EVG) is reported. PA ox electrodeposited on a screen-printed carbon electrode (SPCE) was used as a new fixed state ratiometric reference probe. A portable electrochemical workstation combined with a smart phone was applied as an intelligent portable electrochemical sensing platform. The sensor was studied by scanning electron microscopy (SEM), Fourier transform infrared spectrophotometry (FT-IR), ultraviolet-visible spectrophotometry (UV-vis), theoretical calculation, chronoamperometry, cyclic voltammetry (CV), electrochemical impedance spectroscopy (EIS) and square wave voltammetry (SWV). Under optimized conditions, the detection range of NIC is 10-200 μmol L
, and the detection limit is 0.256 μmol L
. The detection range of EVG was 10-180 μmol L
, and the detection limit was 0.058 μmol L
. The sensor can realize the real-time detection of NIC and EVG concentration in cigarette samples quickly and accurately, and has good anti-interference, repeatability and stability.</description><subject>Analgesics</subject><subject>Electrochemical impedance spectroscopy</subject><subject>Electrodeposition</subject><subject>Electrons</subject><subject>Fourier transforms</subject><subject>Glucosides</subject><subject>Infrared spectrophotometers</subject><subject>Nicotine</subject><subject>Portability</subject><subject>Spectrophotometry</subject><subject>Square waves</subject><subject>Vanillin</subject><subject>Voltammetry</subject><subject>Workstations</subject><issn>0003-2654</issn><issn>1364-5528</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNpdkUFO3TAQhi1UVF6hGw5QWeqmqhRqj2MnWSIebZEQbMo6cuwJNUrs1HaqsuZGPQhnwpTXLrryWPrmmxn9hBxzdsKZ6D5ZoT3jDW_tHtlwoepKSmhfkQ1jTFSgZH1A3qR0V76cSfaaHIi2VBzaDXk4n9DkGCwuIbnsgqdhpIuO2mDWc5ho-OUs0jFE6nzGaXK36DNdQsx6mJBGXZpmzNEZajEX2c7hnQnZeaTaW4r5-_1Ef2rvisDTx9_VtrqdVlNmWjwi-6OeEr7dvYfk5vP5t7Ov1eX1l4uz08vKCC5zZSSYWrKWt43VSo4GGtZgDaCF6gbRdHxgtjGy0DCAHWFUhoPSoETDLCpxSD68eJcYfqyYcj-7ZMpJ2mNYUw9tVzcAiomCvv8PvQtr9GW7HjoG7TNTF-rjC2ViSCni2C_RzTre95z1z9H0W3F69SeabYHf7ZTrMKP9h_7NQjwBspaLPg</recordid><startdate>20231218</startdate><enddate>20231218</enddate><creator>Su, Zhaohong</creator><creator>Hu, Shiyu</creator><creator>Zhang, Yuhang</creator><creator>Liang, Zhanning</creator><creator>Peng, Yi</creator><creator>Cao, Qinyi</creator><creator>Yu, Xia</creator><creator>Zhu, Zhiyang</creator><creator>He, Pei</creator><creator>Li, Zhenjie</creator><general>Royal Society of Chemistry</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope><scope>7X8</scope><orcidid>https://orcid.org/0000-0001-7616-0770</orcidid></search><sort><creationdate>20231218</creationdate><title>Electrodeposition of paracetamol oxide for intelligent portable ratiometric detection of nicotine and ethyl vanillin β-D-glucoside</title><author>Su, Zhaohong ; Hu, Shiyu ; Zhang, Yuhang ; Liang, Zhanning ; Peng, Yi ; Cao, Qinyi ; Yu, Xia ; Zhu, Zhiyang ; He, Pei ; Li, Zhenjie</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c315t-c52c4508187da65fc2707e422a369b3791b0d7c5c312b2df2f6c126a26370de63</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Analgesics</topic><topic>Electrochemical impedance spectroscopy</topic><topic>Electrodeposition</topic><topic>Electrons</topic><topic>Fourier transforms</topic><topic>Glucosides</topic><topic>Infrared spectrophotometers</topic><topic>Nicotine</topic><topic>Portability</topic><topic>Spectrophotometry</topic><topic>Square waves</topic><topic>Vanillin</topic><topic>Voltammetry</topic><topic>Workstations</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Su, Zhaohong</creatorcontrib><creatorcontrib>Hu, Shiyu</creatorcontrib><creatorcontrib>Zhang, Yuhang</creatorcontrib><creatorcontrib>Liang, Zhanning</creatorcontrib><creatorcontrib>Peng, Yi</creatorcontrib><creatorcontrib>Cao, Qinyi</creatorcontrib><creatorcontrib>Yu, Xia</creatorcontrib><creatorcontrib>Zhu, Zhiyang</creatorcontrib><creatorcontrib>He, Pei</creatorcontrib><creatorcontrib>Li, Zhenjie</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>MEDLINE - Academic</collection><jtitle>Analyst (London)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Su, Zhaohong</au><au>Hu, Shiyu</au><au>Zhang, Yuhang</au><au>Liang, Zhanning</au><au>Peng, Yi</au><au>Cao, Qinyi</au><au>Yu, Xia</au><au>Zhu, Zhiyang</au><au>He, Pei</au><au>Li, Zhenjie</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Electrodeposition of paracetamol oxide for intelligent portable ratiometric detection of nicotine and ethyl vanillin β-D-glucoside</atitle><jtitle>Analyst (London)</jtitle><addtitle>Analyst</addtitle><date>2023-12-18</date><risdate>2023</risdate><volume>149</volume><issue>1</issue><spage>188</spage><epage>195</epage><pages>188-195</pages><issn>0003-2654</issn><eissn>1364-5528</eissn><abstract>Herein, the electrodeposition of paracetamol oxide (PA ox) for the intelligent portable ratiometric detection of nicotine (NIC) and ethyl vanillin β-D-glucoside (EVG) is reported. PA ox electrodeposited on a screen-printed carbon electrode (SPCE) was used as a new fixed state ratiometric reference probe. A portable electrochemical workstation combined with a smart phone was applied as an intelligent portable electrochemical sensing platform. The sensor was studied by scanning electron microscopy (SEM), Fourier transform infrared spectrophotometry (FT-IR), ultraviolet-visible spectrophotometry (UV-vis), theoretical calculation, chronoamperometry, cyclic voltammetry (CV), electrochemical impedance spectroscopy (EIS) and square wave voltammetry (SWV). Under optimized conditions, the detection range of NIC is 10-200 μmol L
, and the detection limit is 0.256 μmol L
. The detection range of EVG was 10-180 μmol L
, and the detection limit was 0.058 μmol L
. The sensor can realize the real-time detection of NIC and EVG concentration in cigarette samples quickly and accurately, and has good anti-interference, repeatability and stability.</abstract><cop>England</cop><pub>Royal Society of Chemistry</pub><pmid>38010128</pmid><doi>10.1039/d3an01718d</doi><tpages>8</tpages><orcidid>https://orcid.org/0000-0001-7616-0770</orcidid></addata></record> |
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source | Royal Society of Chemistry Journals Archive (1841-2007); Royal Society Of Chemistry Journals 2008-; Alma/SFX Local Collection |
subjects | Analgesics Electrochemical impedance spectroscopy Electrodeposition Electrons Fourier transforms Glucosides Infrared spectrophotometers Nicotine Portability Spectrophotometry Square waves Vanillin Voltammetry Workstations |
title | Electrodeposition of paracetamol oxide for intelligent portable ratiometric detection of nicotine and ethyl vanillin β-D-glucoside |
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