Thermal behavior of nitrided TiO2/In2O3 by TG-DSC-MS combined with PulseTA
TiO2/InN (In/(Ti+In)=6DDT5:100mol) was prepared by nitridation of TiO2/In2O3 by NH3 at 580DDGC for 8h. Only the anatase TiO2 phase was detected in the XRD measurements. The highly dispersed InN clusters on the surface of anatase TiO2 nanocrystals were beyond the detection limit of XRD. In order to c...
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| Veröffentlicht in: | Thermochimica acta 2006-01, Vol.440 (2), p.195-199 |
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| container_title | Thermochimica acta |
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| creator | YU, Hui-Mei ZHANG, Qing-Hong QI, Ling-Jun LU, Chang-Wei XI, Tong-Geng LAN LUO |
| description | TiO2/InN (In/(Ti+In)=6DDT5:100mol) was prepared by nitridation of TiO2/In2O3 by NH3 at 580DDGC for 8h. Only the anatase TiO2 phase was detected in the XRD measurements. The highly dispersed InN clusters on the surface of anatase TiO2 nanocrystals were beyond the detection limit of XRD. In order to confirm the existence of InN in the products of nitridation, thermogravimetry-differential scanning calorimetry-mass spectrometry (TG-DSC-MS) coupling techniques were used for a simultaneous characterizing study of the changes of mass, enthalpy and determination of the evolved gases during the thermal decomposition of the InN and the nitrided TiO2/In2O3 samples. Moreover, pulse thermal analysis (PulseTA) was combined with TG-DSC-MS for the quantitative calibration of the evolved nitrogen formed during the thermal decomposition of the InN and the nitrided TiO2/In2O3. The applied technique enabled identification and quantification of the InN in the products of the nitridation of TiO2/In2O3. |
| doi_str_mv | 10.1016/j.tca.2005.11.003 |
| format | Article |
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Only the anatase TiO2 phase was detected in the XRD measurements. The highly dispersed InN clusters on the surface of anatase TiO2 nanocrystals were beyond the detection limit of XRD. In order to confirm the existence of InN in the products of nitridation, thermogravimetry-differential scanning calorimetry-mass spectrometry (TG-DSC-MS) coupling techniques were used for a simultaneous characterizing study of the changes of mass, enthalpy and determination of the evolved gases during the thermal decomposition of the InN and the nitrided TiO2/In2O3 samples. Moreover, pulse thermal analysis (PulseTA) was combined with TG-DSC-MS for the quantitative calibration of the evolved nitrogen formed during the thermal decomposition of the InN and the nitrided TiO2/In2O3. 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Only the anatase TiO2 phase was detected in the XRD measurements. The highly dispersed InN clusters on the surface of anatase TiO2 nanocrystals were beyond the detection limit of XRD. In order to confirm the existence of InN in the products of nitridation, thermogravimetry-differential scanning calorimetry-mass spectrometry (TG-DSC-MS) coupling techniques were used for a simultaneous characterizing study of the changes of mass, enthalpy and determination of the evolved gases during the thermal decomposition of the InN and the nitrided TiO2/In2O3 samples. Moreover, pulse thermal analysis (PulseTA) was combined with TG-DSC-MS for the quantitative calibration of the evolved nitrogen formed during the thermal decomposition of the InN and the nitrided TiO2/In2O3. The applied technique enabled identification and quantification of the InN in the products of the nitridation of TiO2/In2O3.</description><subject>Carbonyl and nitrosyl metals</subject><subject>Chemistry</subject><subject>Exact sciences and technology</subject><subject>Inorganic chemistry and origins of life</subject><subject>Preparations and properties</subject><issn>0040-6031</issn><issn>1872-762X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2006</creationdate><recordtype>article</recordtype><recordid>eNpFkE1LAzEURYMoWKs_wN1sdDfT95KZSbosVWulUqEjuAuZNENT5qMmU6X_3pQWXL27uPc8OITcIyQImI-2Sa9VQgGyBDEBYBdkgILTmOf065IMAFKIc2B4TW683wIAUgED8lZsjGtUHZVmo35s56KuilrbO7s266iwSzqat3TJovIQFbP4aTWN31eR7prStqHwa_tN9LGvvSkmt-SqUiHdne-QfL48F9PXeLGczaeTRawZ5H2cZxWnmgscj1NhIAdjIFMZqlSw8BNxbBRfo6hSDooZoCI1mvOMKsZKJTI2JI8n7s5133vje9lYr01dq9Z0ey-p4Ok4EywU8VTUrvPemUrunG2UO0gEebQmtzJYk0drElEGa2HzcIYrr1VdOdVq6_-HPIPA5uwPpThq4Q</recordid><startdate>20060115</startdate><enddate>20060115</enddate><creator>YU, Hui-Mei</creator><creator>ZHANG, Qing-Hong</creator><creator>QI, Ling-Jun</creator><creator>LU, Chang-Wei</creator><creator>XI, Tong-Geng</creator><creator>LAN LUO</creator><general>Elsevier Science</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20060115</creationdate><title>Thermal behavior of nitrided TiO2/In2O3 by TG-DSC-MS combined with PulseTA</title><author>YU, Hui-Mei ; ZHANG, Qing-Hong ; QI, Ling-Jun ; LU, Chang-Wei ; XI, Tong-Geng ; LAN LUO</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c306t-65f72c7819948e060ee05a51a483ded119ea7d18f470a3e0284ec7752a33ba853</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2006</creationdate><topic>Carbonyl and nitrosyl metals</topic><topic>Chemistry</topic><topic>Exact sciences and technology</topic><topic>Inorganic chemistry and origins of life</topic><topic>Preparations and properties</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>YU, Hui-Mei</creatorcontrib><creatorcontrib>ZHANG, Qing-Hong</creatorcontrib><creatorcontrib>QI, Ling-Jun</creatorcontrib><creatorcontrib>LU, Chang-Wei</creatorcontrib><creatorcontrib>XI, Tong-Geng</creatorcontrib><creatorcontrib>LAN LUO</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Thermochimica acta</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>YU, Hui-Mei</au><au>ZHANG, Qing-Hong</au><au>QI, Ling-Jun</au><au>LU, Chang-Wei</au><au>XI, Tong-Geng</au><au>LAN LUO</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Thermal behavior of nitrided TiO2/In2O3 by TG-DSC-MS combined with PulseTA</atitle><jtitle>Thermochimica acta</jtitle><date>2006-01-15</date><risdate>2006</risdate><volume>440</volume><issue>2</issue><spage>195</spage><epage>199</epage><pages>195-199</pages><issn>0040-6031</issn><eissn>1872-762X</eissn><coden>THACAS</coden><abstract>TiO2/InN (In/(Ti+In)=6DDT5:100mol) was prepared by nitridation of TiO2/In2O3 by NH3 at 580DDGC for 8h. Only the anatase TiO2 phase was detected in the XRD measurements. The highly dispersed InN clusters on the surface of anatase TiO2 nanocrystals were beyond the detection limit of XRD. In order to confirm the existence of InN in the products of nitridation, thermogravimetry-differential scanning calorimetry-mass spectrometry (TG-DSC-MS) coupling techniques were used for a simultaneous characterizing study of the changes of mass, enthalpy and determination of the evolved gases during the thermal decomposition of the InN and the nitrided TiO2/In2O3 samples. Moreover, pulse thermal analysis (PulseTA) was combined with TG-DSC-MS for the quantitative calibration of the evolved nitrogen formed during the thermal decomposition of the InN and the nitrided TiO2/In2O3. The applied technique enabled identification and quantification of the InN in the products of the nitridation of TiO2/In2O3.</abstract><cop>Amsterdam</cop><pub>Elsevier Science</pub><doi>10.1016/j.tca.2005.11.003</doi><tpages>5</tpages></addata></record> |
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| source | ScienceDirect Journals (5 years ago - present) |
| subjects | Carbonyl and nitrosyl metals Chemistry Exact sciences and technology Inorganic chemistry and origins of life Preparations and properties |
| title | Thermal behavior of nitrided TiO2/In2O3 by TG-DSC-MS combined with PulseTA |
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