Insight into the 4-nitrophenol reduction, supercapacitive behavior, and antimicrobial activity of ZnCo2O4-rGO nanocomposite fabricated by the simple reflux method
In this article, binary oxide ZnCo 2 O 4 nanoparticles (NPs) have been developed on reduced graphene oxide surface by simple reflux condensation method. The physicochemical characteristics of the synthesized nanocomposite were computed using X-ray diffraction (XRD), transmission electron microscopy...
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| Veröffentlicht in: | Environmental science and pollution research international 2023-11, Vol.30 (51), p.110764-110778 |
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| creator | Tantubay, Kartik Bairy, Bapan Dutta, Arpita Akhtar, Abu Jahid Pal, Suchetana Dam, Somasri Baskey (Sen), Moni |
| description | In this article, binary oxide ZnCo
2
O
4
nanoparticles (NPs) have been developed on reduced graphene oxide surface by simple reflux condensation method. The physicochemical characteristics of the synthesized nanocomposite were computed using X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), Fourier-transform infrared spectroscopy (FTIR), and UV-Visible spectroscopy. The average size of ZnCo
2
O
4
NPs is found to be about 9 nm. The synthesized nanocomposite was found to be an extremely efficient catalyst for reduction of 4-nitrophenol (4-NP) to produce 4-aminophenol (4-AP) and it is exhibited that about 98% 4-nitrophenol can be reduced in only 20 min. The nanocomposite behaves as supercapacitor due to possessing the specific capacitance value up to 609 F/g and excellent capacitance retention over 1000 cycles. The Brunauer-Emmett-Teller (BET) surface area analysis has been conducted to evaluate surface area and pore size of the synthesized material. The antimicrobial activity of this nanocomposite was performed against bacterial strains of
Escherichia coli
(
E. coli
),
Bacillus subtilis
(
B. subtilis
), and
Staphylococcus aureus
(
S. aureus
) and it is noticed to be a good antimicrobial agent against different bacterial strains. |
| doi_str_mv | 10.1007/s11356-023-30078-7 |
| format | Article |
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2
O
4
nanoparticles (NPs) have been developed on reduced graphene oxide surface by simple reflux condensation method. The physicochemical characteristics of the synthesized nanocomposite were computed using X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), Fourier-transform infrared spectroscopy (FTIR), and UV-Visible spectroscopy. The average size of ZnCo
2
O
4
NPs is found to be about 9 nm. The synthesized nanocomposite was found to be an extremely efficient catalyst for reduction of 4-nitrophenol (4-NP) to produce 4-aminophenol (4-AP) and it is exhibited that about 98% 4-nitrophenol can be reduced in only 20 min. The nanocomposite behaves as supercapacitor due to possessing the specific capacitance value up to 609 F/g and excellent capacitance retention over 1000 cycles. The Brunauer-Emmett-Teller (BET) surface area analysis has been conducted to evaluate surface area and pore size of the synthesized material. The antimicrobial activity of this nanocomposite was performed against bacterial strains of
Escherichia coli
(
E. coli
),
Bacillus subtilis
(
B. subtilis
), and
Staphylococcus aureus
(
S. aureus
) and it is noticed to be a good antimicrobial agent against different bacterial strains.</description><identifier>ISSN: 1614-7499</identifier><identifier>ISSN: 0944-1344</identifier><identifier>EISSN: 1614-7499</identifier><identifier>DOI: 10.1007/s11356-023-30078-7</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Aminophenol ; aminophenols ; anti-infective agents ; Antimicrobial activity ; Antimicrobial agents ; antimicrobial properties ; Aquatic Pollution ; Atmospheric Protection/Air Quality Control/Air Pollution ; Bacillus subtilis ; Capacitance ; Catalysts ; Condensates ; E coli ; Earth and Environmental Science ; Ecotoxicology ; electrochemical capacitors ; Electron microscopy ; Environment ; Environmental Chemistry ; Environmental Health ; Escherichia coli ; Fourier transform infrared spectroscopy ; Fourier transforms ; Graphene ; graphene oxide ; Infrared spectroscopy ; Microscopy ; Nanocomposites ; Nanoparticles ; Nitrophenol ; p-Aminophenol ; p-Nitrophenol ; Pore size ; porosity ; Reduction ; Research Article ; Scanning electron microscopy ; Spectrum analysis ; Staphylococcus aureus ; Strains (organisms) ; Surface area ; Transmission electron microscopy ; ultraviolet-visible spectroscopy ; Waste Water Technology ; Water Management ; Water Pollution Control ; X-ray diffraction</subject><ispartof>Environmental science and pollution research international, 2023-11, Vol.30 (51), p.110764-110778</ispartof><rights>The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c385t-5200bf9ef8a9baede891cc108443dc31656cac9e33740ac2f8b3310e548817653</citedby><cites>FETCH-LOGICAL-c385t-5200bf9ef8a9baede891cc108443dc31656cac9e33740ac2f8b3310e548817653</cites><orcidid>0000-0003-2031-6929</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11356-023-30078-7$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11356-023-30078-7$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Tantubay, Kartik</creatorcontrib><creatorcontrib>Bairy, Bapan</creatorcontrib><creatorcontrib>Dutta, Arpita</creatorcontrib><creatorcontrib>Akhtar, Abu Jahid</creatorcontrib><creatorcontrib>Pal, Suchetana</creatorcontrib><creatorcontrib>Dam, Somasri</creatorcontrib><creatorcontrib>Baskey (Sen), Moni</creatorcontrib><title>Insight into the 4-nitrophenol reduction, supercapacitive behavior, and antimicrobial activity of ZnCo2O4-rGO nanocomposite fabricated by the simple reflux method</title><title>Environmental science and pollution research international</title><addtitle>Environ Sci Pollut Res</addtitle><description>In this article, binary oxide ZnCo
2
O
4
nanoparticles (NPs) have been developed on reduced graphene oxide surface by simple reflux condensation method. The physicochemical characteristics of the synthesized nanocomposite were computed using X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), Fourier-transform infrared spectroscopy (FTIR), and UV-Visible spectroscopy. The average size of ZnCo
2
O
4
NPs is found to be about 9 nm. The synthesized nanocomposite was found to be an extremely efficient catalyst for reduction of 4-nitrophenol (4-NP) to produce 4-aminophenol (4-AP) and it is exhibited that about 98% 4-nitrophenol can be reduced in only 20 min. The nanocomposite behaves as supercapacitor due to possessing the specific capacitance value up to 609 F/g and excellent capacitance retention over 1000 cycles. The Brunauer-Emmett-Teller (BET) surface area analysis has been conducted to evaluate surface area and pore size of the synthesized material. The antimicrobial activity of this nanocomposite was performed against bacterial strains of
Escherichia coli
(
E. coli
),
Bacillus subtilis
(
B. subtilis
), and
Staphylococcus aureus
(
S. aureus
) and it is noticed to be a good antimicrobial agent against different bacterial strains.</description><subject>Aminophenol</subject><subject>aminophenols</subject><subject>anti-infective agents</subject><subject>Antimicrobial activity</subject><subject>Antimicrobial agents</subject><subject>antimicrobial properties</subject><subject>Aquatic Pollution</subject><subject>Atmospheric Protection/Air Quality Control/Air Pollution</subject><subject>Bacillus subtilis</subject><subject>Capacitance</subject><subject>Catalysts</subject><subject>Condensates</subject><subject>E coli</subject><subject>Earth and Environmental Science</subject><subject>Ecotoxicology</subject><subject>electrochemical capacitors</subject><subject>Electron microscopy</subject><subject>Environment</subject><subject>Environmental Chemistry</subject><subject>Environmental Health</subject><subject>Escherichia coli</subject><subject>Fourier transform infrared spectroscopy</subject><subject>Fourier transforms</subject><subject>Graphene</subject><subject>graphene oxide</subject><subject>Infrared spectroscopy</subject><subject>Microscopy</subject><subject>Nanocomposites</subject><subject>Nanoparticles</subject><subject>Nitrophenol</subject><subject>p-Aminophenol</subject><subject>p-Nitrophenol</subject><subject>Pore size</subject><subject>porosity</subject><subject>Reduction</subject><subject>Research Article</subject><subject>Scanning electron microscopy</subject><subject>Spectrum analysis</subject><subject>Staphylococcus aureus</subject><subject>Strains (organisms)</subject><subject>Surface area</subject><subject>Transmission electron microscopy</subject><subject>ultraviolet-visible spectroscopy</subject><subject>Waste Water Technology</subject><subject>Water Management</subject><subject>Water Pollution Control</subject><subject>X-ray 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into the 4-nitrophenol reduction, supercapacitive behavior, and antimicrobial activity of ZnCo2O4-rGO nanocomposite fabricated by the simple reflux method</title><author>Tantubay, Kartik ; Bairy, Bapan ; Dutta, Arpita ; Akhtar, Abu Jahid ; Pal, Suchetana ; Dam, Somasri ; Baskey (Sen), Moni</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c385t-5200bf9ef8a9baede891cc108443dc31656cac9e33740ac2f8b3310e548817653</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Aminophenol</topic><topic>aminophenols</topic><topic>anti-infective agents</topic><topic>Antimicrobial activity</topic><topic>Antimicrobial agents</topic><topic>antimicrobial properties</topic><topic>Aquatic Pollution</topic><topic>Atmospheric Protection/Air Quality Control/Air Pollution</topic><topic>Bacillus subtilis</topic><topic>Capacitance</topic><topic>Catalysts</topic><topic>Condensates</topic><topic>E coli</topic><topic>Earth and Environmental Science</topic><topic>Ecotoxicology</topic><topic>electrochemical capacitors</topic><topic>Electron microscopy</topic><topic>Environment</topic><topic>Environmental Chemistry</topic><topic>Environmental Health</topic><topic>Escherichia coli</topic><topic>Fourier transform infrared spectroscopy</topic><topic>Fourier transforms</topic><topic>Graphene</topic><topic>graphene oxide</topic><topic>Infrared spectroscopy</topic><topic>Microscopy</topic><topic>Nanocomposites</topic><topic>Nanoparticles</topic><topic>Nitrophenol</topic><topic>p-Aminophenol</topic><topic>p-Nitrophenol</topic><topic>Pore size</topic><topic>porosity</topic><topic>Reduction</topic><topic>Research Article</topic><topic>Scanning electron microscopy</topic><topic>Spectrum analysis</topic><topic>Staphylococcus aureus</topic><topic>Strains (organisms)</topic><topic>Surface area</topic><topic>Transmission electron microscopy</topic><topic>ultraviolet-visible 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international</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Tantubay, Kartik</au><au>Bairy, Bapan</au><au>Dutta, Arpita</au><au>Akhtar, Abu Jahid</au><au>Pal, Suchetana</au><au>Dam, Somasri</au><au>Baskey (Sen), Moni</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Insight into the 4-nitrophenol reduction, supercapacitive behavior, and antimicrobial activity of ZnCo2O4-rGO nanocomposite fabricated by the simple reflux method</atitle><jtitle>Environmental science and pollution research international</jtitle><stitle>Environ Sci Pollut Res</stitle><date>2023-11-01</date><risdate>2023</risdate><volume>30</volume><issue>51</issue><spage>110764</spage><epage>110778</epage><pages>110764-110778</pages><issn>1614-7499</issn><issn>0944-1344</issn><eissn>1614-7499</eissn><abstract>In this article, binary oxide ZnCo
2
O
4
nanoparticles (NPs) have been developed on reduced graphene oxide surface by simple reflux condensation method. The physicochemical characteristics of the synthesized nanocomposite were computed using X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), Fourier-transform infrared spectroscopy (FTIR), and UV-Visible spectroscopy. The average size of ZnCo
2
O
4
NPs is found to be about 9 nm. The synthesized nanocomposite was found to be an extremely efficient catalyst for reduction of 4-nitrophenol (4-NP) to produce 4-aminophenol (4-AP) and it is exhibited that about 98% 4-nitrophenol can be reduced in only 20 min. The nanocomposite behaves as supercapacitor due to possessing the specific capacitance value up to 609 F/g and excellent capacitance retention over 1000 cycles. The Brunauer-Emmett-Teller (BET) surface area analysis has been conducted to evaluate surface area and pore size of the synthesized material. The antimicrobial activity of this nanocomposite was performed against bacterial strains of
Escherichia coli
(
E. coli
),
Bacillus subtilis
(
B. subtilis
), and
Staphylococcus aureus
(
S. aureus
) and it is noticed to be a good antimicrobial agent against different bacterial strains.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><doi>10.1007/s11356-023-30078-7</doi><tpages>15</tpages><orcidid>https://orcid.org/0000-0003-2031-6929</orcidid></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1614-7499 |
| ispartof | Environmental science and pollution research international, 2023-11, Vol.30 (51), p.110764-110778 |
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| language | eng |
| recordid | cdi_proquest_miscellaneous_2873249631 |
| source | SpringerLink Journals - AutoHoldings |
| subjects | Aminophenol aminophenols anti-infective agents Antimicrobial activity Antimicrobial agents antimicrobial properties Aquatic Pollution Atmospheric Protection/Air Quality Control/Air Pollution Bacillus subtilis Capacitance Catalysts Condensates E coli Earth and Environmental Science Ecotoxicology electrochemical capacitors Electron microscopy Environment Environmental Chemistry Environmental Health Escherichia coli Fourier transform infrared spectroscopy Fourier transforms Graphene graphene oxide Infrared spectroscopy Microscopy Nanocomposites Nanoparticles Nitrophenol p-Aminophenol p-Nitrophenol Pore size porosity Reduction Research Article Scanning electron microscopy Spectrum analysis Staphylococcus aureus Strains (organisms) Surface area Transmission electron microscopy ultraviolet-visible spectroscopy Waste Water Technology Water Management Water Pollution Control X-ray diffraction |
| title | Insight into the 4-nitrophenol reduction, supercapacitive behavior, and antimicrobial activity of ZnCo2O4-rGO nanocomposite fabricated by the simple reflux method |
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