Reliable determination of freeze-concentration using DSC

The objective of this study was to determine the feature of a DSC endotherm that can be most reliably used to determine the composition of a freeze-concentrate. Samples (3–10 mg) of sucrose in water (0–60%, w/v) were frozen and then heated (at 0.2–2.0 °C/min) on a DSC. The peak ( T peak) and offset...

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Veröffentlicht in:	Thermochimica acta 2005-01, Vol.425 (1), p.149-163
Hauptverfasser:	Bhatnagar, Bakul S., Cardon, Stephane, Pikal, Michael J., Bogner, Robin H.
Format:	Artikel
Sprache:	eng
Schlagworte:	DSC Freeze-concentration Ice melting Sucrose Toffset
Online-Zugang:	Volltext
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