Maintenance of enamel properties after bleaching with high-concentrated hydrogen-peroxide gel containing calcium polyphosphate sub-microparticles
Objective To assessed the physical and chemical properties of human-enamel after treatment with an experimental bleaching gel containing 35%-hydrogen peroxide (HP) and calcium polyphosphate sub-microparticles (CaPP). Materials and methods Enamel/dentin specimens (4 × 4 × 3 mm) were obtained ( n = 1...
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| Veröffentlicht in: | Clinical oral investigations 2023-09, Vol.27 (9), p.5275-5285 |
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| creator | Ortiz, Mariángela Ivette Guanipa dos Santos, Juliana Jarussi Rodrigues-Filho, Ubirajara Pereira Aguiar, Flávio Henrique Baggio Rischka, Klaus Lima, Débora Alves Nunes Leite |
| description | Objective
To assessed the physical and chemical properties of human-enamel after treatment with an experimental bleaching gel containing 35%-hydrogen peroxide (HP) and calcium polyphosphate sub-microparticles (CaPP).
Materials and methods
Enamel/dentin specimens (4 × 4 × 3 mm) were obtained (
n
= 120) and allocated to different groups: control (saliva only); experimental (HP35%); commercial (whiteness-HP-Maxx); CaPP0.5% (HP35% + CaPP0.5wt%); CaPP1.5% (HP35% + CaPP1.5wt%). Three sessions were performed. The specimens’ color was assessed using a spectrophotometer and the color (Δ
E
/Δ
E
00
) and bleaching index (ΔWID) determined. The surface roughness and microhardness were assessed with a roughness tester and Knoop indenter. Raman spectroscopy was performed to obtain the ratios between the areas under the 431, 580, and 1070 cm
−1
and the 960 cm
−1
bands (430:960, 580:960, 1070:960). Kruskal–Wallis and Dunn compared the color, Ra, and SMH data. The Raman data was analyzed with Kruskal–Wallis and Dunn (
α
= 5%).
Results
The Δ
E
, Δ
E
00
, and ΔWID were similar among the bleached groups (
p
> 0.05). The roughness was not different between the groups (
p
> 0.05). After the 3
rd
session, CaPP0.5% had higher microhardness than the experimental (
p
|
| doi_str_mv | 10.1007/s00784-023-05147-3 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_2858989149</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2862848001</sourcerecordid><originalsourceid>FETCH-LOGICAL-c352t-bc4c8a85643a7bdf43afeee9ab0c8148843db52e02c0c6bf9715b570ce3411313</originalsourceid><addsrcrecordid>eNp9kctu3SAQhq0olXJpXyArpGy6IQGDbbysolwqpeqmXSOMxzaRDQ5gpecx-sadk1MpVRbdMCy-b4bhL4oLzq44Y811wkNJykpBWcVlQ8VRccqlqKloGn78z_2kOEvpiTEu60acFr-_GeczeOMtkDAQvC0wkzWGFWJ2kIgZMkTSzWDs5PxIXlyeyOTGidqAks_RZOjJtOtjGMFT9MIv1wMZsQ8iGQfsPWtm67aFrGHerVNI64QeSVtHF2dxnMFxdob0sfgwmDnBp7_1vPh5d_vj5oE-fr__evPlkVpRlZl2VlplVFVLYZquH7AMANCajlnFpVJS9F1VAists3U3tA2vuqphFoTkXHBxXnw-9MVdnzdIWS8uWZhn4yFsSZeqUq1quWwRvXyHPoUtenwdUnWppML_RKo8ULhNShEGvUa3mLjTnOl9SvqQksaU9GtKWqAkDlJC2I8Q31r_x_oDQ8eZKA</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2862848001</pqid></control><display><type>article</type><title>Maintenance of enamel properties after bleaching with high-concentrated hydrogen-peroxide gel containing calcium polyphosphate sub-microparticles</title><source>SpringerLink Journals - AutoHoldings</source><creator>Ortiz, Mariángela Ivette Guanipa ; dos Santos, Juliana Jarussi ; Rodrigues-Filho, Ubirajara Pereira ; Aguiar, Flávio Henrique Baggio ; Rischka, Klaus ; Lima, Débora Alves Nunes Leite</creator><creatorcontrib>Ortiz, Mariángela Ivette Guanipa ; dos Santos, Juliana Jarussi ; Rodrigues-Filho, Ubirajara Pereira ; Aguiar, Flávio Henrique Baggio ; Rischka, Klaus ; Lima, Débora Alves Nunes Leite</creatorcontrib><description>Objective
To assessed the physical and chemical properties of human-enamel after treatment with an experimental bleaching gel containing 35%-hydrogen peroxide (HP) and calcium polyphosphate sub-microparticles (CaPP).
Materials and methods
Enamel/dentin specimens (4 × 4 × 3 mm) were obtained (
n
= 120) and allocated to different groups: control (saliva only); experimental (HP35%); commercial (whiteness-HP-Maxx); CaPP0.5% (HP35% + CaPP0.5wt%); CaPP1.5% (HP35% + CaPP1.5wt%). Three sessions were performed. The specimens’ color was assessed using a spectrophotometer and the color (Δ
E
/Δ
E
00
) and bleaching index (ΔWID) determined. The surface roughness and microhardness were assessed with a roughness tester and Knoop indenter. Raman spectroscopy was performed to obtain the ratios between the areas under the 431, 580, and 1070 cm
−1
and the 960 cm
−1
bands (430:960, 580:960, 1070:960). Kruskal–Wallis and Dunn compared the color, Ra, and SMH data. The Raman data was analyzed with Kruskal–Wallis and Dunn (
α
= 5%).
Results
The Δ
E
, Δ
E
00
, and ΔWID were similar among the bleached groups (
p
> 0.05). The roughness was not different between the groups (
p
> 0.05). After the 3
rd
session, CaPP0.5% had higher microhardness than the experimental (
p
< 0.05). The 1070:960 was higher in the experimental than in the CaPP1.5% and control (
p
< 0.05).
Conclusions
In human enamel, CaPP did not alter the bleaching effectiveness or roughness, and additionally, CaPP-containing gels increased the microhardness and preserved the mineral content when compared to the experimental without CaPP.
Clinical relevance
Experimental bleaching gels containing calcium polyphosphate sub-microparticles as a mineral source reduce the mineral content alteration and superficial microhardness reduction, known potential side effects of the in-office bleaching treatments.</description><identifier>ISSN: 1436-3771</identifier><identifier>ISSN: 1432-6981</identifier><identifier>EISSN: 1436-3771</identifier><identifier>DOI: 10.1007/s00784-023-05147-3</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Bleaching ; Calcium ; Dentistry ; Enamel ; Gels ; Hydrogen peroxide ; Medicine ; Microparticles ; Raman spectroscopy ; Saliva</subject><ispartof>Clinical oral investigations, 2023-09, Vol.27 (9), p.5275-5285</ispartof><rights>The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c352t-bc4c8a85643a7bdf43afeee9ab0c8148843db52e02c0c6bf9715b570ce3411313</citedby><cites>FETCH-LOGICAL-c352t-bc4c8a85643a7bdf43afeee9ab0c8148843db52e02c0c6bf9715b570ce3411313</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s00784-023-05147-3$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s00784-023-05147-3$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27903,27904,41467,42536,51297</link.rule.ids></links><search><creatorcontrib>Ortiz, Mariángela Ivette Guanipa</creatorcontrib><creatorcontrib>dos Santos, Juliana Jarussi</creatorcontrib><creatorcontrib>Rodrigues-Filho, Ubirajara Pereira</creatorcontrib><creatorcontrib>Aguiar, Flávio Henrique Baggio</creatorcontrib><creatorcontrib>Rischka, Klaus</creatorcontrib><creatorcontrib>Lima, Débora Alves Nunes Leite</creatorcontrib><title>Maintenance of enamel properties after bleaching with high-concentrated hydrogen-peroxide gel containing calcium polyphosphate sub-microparticles</title><title>Clinical oral investigations</title><addtitle>Clin Oral Invest</addtitle><description>Objective
To assessed the physical and chemical properties of human-enamel after treatment with an experimental bleaching gel containing 35%-hydrogen peroxide (HP) and calcium polyphosphate sub-microparticles (CaPP).
Materials and methods
Enamel/dentin specimens (4 × 4 × 3 mm) were obtained (
n
= 120) and allocated to different groups: control (saliva only); experimental (HP35%); commercial (whiteness-HP-Maxx); CaPP0.5% (HP35% + CaPP0.5wt%); CaPP1.5% (HP35% + CaPP1.5wt%). Three sessions were performed. The specimens’ color was assessed using a spectrophotometer and the color (Δ
E
/Δ
E
00
) and bleaching index (ΔWID) determined. The surface roughness and microhardness were assessed with a roughness tester and Knoop indenter. Raman spectroscopy was performed to obtain the ratios between the areas under the 431, 580, and 1070 cm
−1
and the 960 cm
−1
bands (430:960, 580:960, 1070:960). Kruskal–Wallis and Dunn compared the color, Ra, and SMH data. The Raman data was analyzed with Kruskal–Wallis and Dunn (
α
= 5%).
Results
The Δ
E
, Δ
E
00
, and ΔWID were similar among the bleached groups (
p
> 0.05). The roughness was not different between the groups (
p
> 0.05). After the 3
rd
session, CaPP0.5% had higher microhardness than the experimental (
p
< 0.05). The 1070:960 was higher in the experimental than in the CaPP1.5% and control (
p
< 0.05).
Conclusions
In human enamel, CaPP did not alter the bleaching effectiveness or roughness, and additionally, CaPP-containing gels increased the microhardness and preserved the mineral content when compared to the experimental without CaPP.
Clinical relevance
Experimental bleaching gels containing calcium polyphosphate sub-microparticles as a mineral source reduce the mineral content alteration and superficial microhardness reduction, known potential side effects of the in-office bleaching treatments.</description><subject>Bleaching</subject><subject>Calcium</subject><subject>Dentistry</subject><subject>Enamel</subject><subject>Gels</subject><subject>Hydrogen peroxide</subject><subject>Medicine</subject><subject>Microparticles</subject><subject>Raman spectroscopy</subject><subject>Saliva</subject><issn>1436-3771</issn><issn>1432-6981</issn><issn>1436-3771</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><recordid>eNp9kctu3SAQhq0olXJpXyArpGy6IQGDbbysolwqpeqmXSOMxzaRDQ5gpecx-sadk1MpVRbdMCy-b4bhL4oLzq44Y811wkNJykpBWcVlQ8VRccqlqKloGn78z_2kOEvpiTEu60acFr-_GeczeOMtkDAQvC0wkzWGFWJ2kIgZMkTSzWDs5PxIXlyeyOTGidqAks_RZOjJtOtjGMFT9MIv1wMZsQ8iGQfsPWtm67aFrGHerVNI64QeSVtHF2dxnMFxdob0sfgwmDnBp7_1vPh5d_vj5oE-fr__evPlkVpRlZl2VlplVFVLYZquH7AMANCajlnFpVJS9F1VAists3U3tA2vuqphFoTkXHBxXnw-9MVdnzdIWS8uWZhn4yFsSZeqUq1quWwRvXyHPoUtenwdUnWppML_RKo8ULhNShEGvUa3mLjTnOl9SvqQksaU9GtKWqAkDlJC2I8Q31r_x_oDQ8eZKA</recordid><startdate>20230901</startdate><enddate>20230901</enddate><creator>Ortiz, Mariángela Ivette Guanipa</creator><creator>dos Santos, Juliana Jarussi</creator><creator>Rodrigues-Filho, Ubirajara Pereira</creator><creator>Aguiar, Flávio Henrique Baggio</creator><creator>Rischka, Klaus</creator><creator>Lima, Débora Alves Nunes Leite</creator><general>Springer Berlin Heidelberg</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>7X7</scope><scope>7XB</scope><scope>88E</scope><scope>8AO</scope><scope>8C1</scope><scope>8FE</scope><scope>8FH</scope><scope>8FI</scope><scope>8FJ</scope><scope>8FK</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BBNVY</scope><scope>BENPR</scope><scope>BHPHI</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>FYUFA</scope><scope>GHDGH</scope><scope>GNUQQ</scope><scope>HCIFZ</scope><scope>K9.</scope><scope>LK8</scope><scope>M0S</scope><scope>M1P</scope><scope>M7P</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>7X8</scope></search><sort><creationdate>20230901</creationdate><title>Maintenance of enamel properties after bleaching with high-concentrated hydrogen-peroxide gel containing calcium polyphosphate sub-microparticles</title><author>Ortiz, Mariángela Ivette Guanipa ; dos Santos, Juliana Jarussi ; Rodrigues-Filho, Ubirajara Pereira ; Aguiar, Flávio Henrique Baggio ; Rischka, Klaus ; Lima, Débora Alves Nunes Leite</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c352t-bc4c8a85643a7bdf43afeee9ab0c8148843db52e02c0c6bf9715b570ce3411313</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Bleaching</topic><topic>Calcium</topic><topic>Dentistry</topic><topic>Enamel</topic><topic>Gels</topic><topic>Hydrogen peroxide</topic><topic>Medicine</topic><topic>Microparticles</topic><topic>Raman spectroscopy</topic><topic>Saliva</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Ortiz, Mariángela Ivette Guanipa</creatorcontrib><creatorcontrib>dos Santos, Juliana Jarussi</creatorcontrib><creatorcontrib>Rodrigues-Filho, Ubirajara Pereira</creatorcontrib><creatorcontrib>Aguiar, Flávio Henrique Baggio</creatorcontrib><creatorcontrib>Rischka, Klaus</creatorcontrib><creatorcontrib>Lima, Débora Alves Nunes Leite</creatorcontrib><collection>CrossRef</collection><collection>ProQuest Central (Corporate)</collection><collection>Health & Medical Collection</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>Medical Database (Alumni Edition)</collection><collection>ProQuest Pharma Collection</collection><collection>Public Health Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Natural Science Collection</collection><collection>Hospital Premium Collection</collection><collection>Hospital Premium Collection (Alumni Edition)</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>Biological Science Collection</collection><collection>ProQuest Central</collection><collection>Natural Science Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Central Korea</collection><collection>Health Research Premium Collection</collection><collection>Health Research Premium Collection (Alumni)</collection><collection>ProQuest Central Student</collection><collection>SciTech Premium Collection</collection><collection>ProQuest Health & Medical Complete (Alumni)</collection><collection>ProQuest Biological Science Collection</collection><collection>Health & Medical Collection (Alumni Edition)</collection><collection>Medical Database</collection><collection>Biological Science Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>MEDLINE - Academic</collection><jtitle>Clinical oral investigations</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Ortiz, Mariángela Ivette Guanipa</au><au>dos Santos, Juliana Jarussi</au><au>Rodrigues-Filho, Ubirajara Pereira</au><au>Aguiar, Flávio Henrique Baggio</au><au>Rischka, Klaus</au><au>Lima, Débora Alves Nunes Leite</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Maintenance of enamel properties after bleaching with high-concentrated hydrogen-peroxide gel containing calcium polyphosphate sub-microparticles</atitle><jtitle>Clinical oral investigations</jtitle><stitle>Clin Oral Invest</stitle><date>2023-09-01</date><risdate>2023</risdate><volume>27</volume><issue>9</issue><spage>5275</spage><epage>5285</epage><pages>5275-5285</pages><issn>1436-3771</issn><issn>1432-6981</issn><eissn>1436-3771</eissn><abstract>Objective
To assessed the physical and chemical properties of human-enamel after treatment with an experimental bleaching gel containing 35%-hydrogen peroxide (HP) and calcium polyphosphate sub-microparticles (CaPP).
Materials and methods
Enamel/dentin specimens (4 × 4 × 3 mm) were obtained (
n
= 120) and allocated to different groups: control (saliva only); experimental (HP35%); commercial (whiteness-HP-Maxx); CaPP0.5% (HP35% + CaPP0.5wt%); CaPP1.5% (HP35% + CaPP1.5wt%). Three sessions were performed. The specimens’ color was assessed using a spectrophotometer and the color (Δ
E
/Δ
E
00
) and bleaching index (ΔWID) determined. The surface roughness and microhardness were assessed with a roughness tester and Knoop indenter. Raman spectroscopy was performed to obtain the ratios between the areas under the 431, 580, and 1070 cm
−1
and the 960 cm
−1
bands (430:960, 580:960, 1070:960). Kruskal–Wallis and Dunn compared the color, Ra, and SMH data. The Raman data was analyzed with Kruskal–Wallis and Dunn (
α
= 5%).
Results
The Δ
E
, Δ
E
00
, and ΔWID were similar among the bleached groups (
p
> 0.05). The roughness was not different between the groups (
p
> 0.05). After the 3
rd
session, CaPP0.5% had higher microhardness than the experimental (
p
< 0.05). The 1070:960 was higher in the experimental than in the CaPP1.5% and control (
p
< 0.05).
Conclusions
In human enamel, CaPP did not alter the bleaching effectiveness or roughness, and additionally, CaPP-containing gels increased the microhardness and preserved the mineral content when compared to the experimental without CaPP.
Clinical relevance
Experimental bleaching gels containing calcium polyphosphate sub-microparticles as a mineral source reduce the mineral content alteration and superficial microhardness reduction, known potential side effects of the in-office bleaching treatments.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><doi>10.1007/s00784-023-05147-3</doi><tpages>11</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1436-3771 |
| ispartof | Clinical oral investigations, 2023-09, Vol.27 (9), p.5275-5285 |
| issn | 1436-3771 1432-6981 1436-3771 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_2858989149 |
| source | SpringerLink Journals - AutoHoldings |
| subjects | Bleaching Calcium Dentistry Enamel Gels Hydrogen peroxide Medicine Microparticles Raman spectroscopy Saliva |
| title | Maintenance of enamel properties after bleaching with high-concentrated hydrogen-peroxide gel containing calcium polyphosphate sub-microparticles |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-26T06%3A11%3A57IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Maintenance%20of%20enamel%20properties%20after%20bleaching%20with%20high-concentrated%20hydrogen-peroxide%20gel%20containing%20calcium%20polyphosphate%20sub-microparticles&rft.jtitle=Clinical%20oral%20investigations&rft.au=Ortiz,%20Mari%C3%A1ngela%20Ivette%20Guanipa&rft.date=2023-09-01&rft.volume=27&rft.issue=9&rft.spage=5275&rft.epage=5285&rft.pages=5275-5285&rft.issn=1436-3771&rft.eissn=1436-3771&rft_id=info:doi/10.1007/s00784-023-05147-3&rft_dat=%3Cproquest_cross%3E2862848001%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2862848001&rft_id=info:pmid/&rfr_iscdi=true |