Reconstruction of three-dimensional strain field in an asymmetrical curved core–shell hetero-nanowire

Crystal orientation and strain mapping of an individual curved and asymmetrical core-shell hetero-nanowire is performed based on transmission electron microscopy. It relies on a comprehensive analysis of scanning nanobeam electron diffraction data obtained for 1.3 nm electron probe size. The propose...

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Veröffentlicht in:Nanotechnology 2023-10, Vol.34 (44), p.445705
Hauptverfasser: Kryvyi, Serhii, Kret, Slawomir, Domagala, Jaroslaw Z, Wojnar, Piotr
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container_issue 44
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container_title Nanotechnology
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creator Kryvyi, Serhii
Kret, Slawomir
Domagala, Jaroslaw Z
Wojnar, Piotr
description Crystal orientation and strain mapping of an individual curved and asymmetrical core-shell hetero-nanowire is performed based on transmission electron microscopy. It relies on a comprehensive analysis of scanning nanobeam electron diffraction data obtained for 1.3 nm electron probe size. The proposed approach also handles the problem of appearing twinning defects on diffraction patterns and allows for the investigation of materials with high defect densities. Based on the experimental maps and their comparison with finite element simulations, the entire core-shell geometry including full three-dimensional strain distribution within the curved core-shell nanowire are obtained. Our approach represents, therefore, a low-dose quasi-tomography of the strain field within a nanoobject using only a single zone axis diffraction experiment. Our approach is applicable also for electron beam-sensitive materials for which performing conventional tomography is a difficult task.
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subjects 3D strain reconstruction
nanobeam electron diffraction
nanowire
orientation mapping
quasi-tomography
strain mapping
title Reconstruction of three-dimensional strain field in an asymmetrical curved core–shell hetero-nanowire
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