Synthesis of B–C–N nanotubes by means of gas arc discharge with a rotating anode

B–C–N nanotubes were synthesized by plasma rotating electrode process (PREP) and examined by scanning electron microscope (SEM) and X-ray diffraction (XRD). Compared with results at 0 rpm of the anode, the number of B–C–N nanotubes was increased by rotating the anode. In addition, peak intensity rat...

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Veröffentlicht in:Materials letters 2004-09, Vol.58 (22), p.2878-2881
Hauptverfasser: Kim, Chang Su, Jeong, Soon Moon, Koo, Won Hoe, Baik, Hong Koo, Lee, Se-Jong, Song, Kie Moon
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Sprache:eng
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Zusammenfassung:B–C–N nanotubes were synthesized by plasma rotating electrode process (PREP) and examined by scanning electron microscope (SEM) and X-ray diffraction (XRD). Compared with results at 0 rpm of the anode, the number of B–C–N nanotubes was increased by rotating the anode. In addition, peak intensity ratio of h-(BN) 0.26C 0.74 to graphite was increased with rotation of the anode and/or the increase of metal concentration. That indicates the yield of B–C–N nanotubes was increased. These results could be explained by an increase of plasma temperature and a swirl in the plasma by rotation of the anode that promote the mixing to aid chemical reactions between evaporated species and atomic nitrogen.
ISSN:0167-577X
1873-4979
DOI:10.1016/j.matlet.2004.05.053