Recovery of the aging-induced changes in microstructures and local structures of yttria-stabilized zirconia due to ion and atom milling

The effect of ion milling and atom milling on the microstructure and the local structure of yttria-stabilized zirconia before and after aging was investigated. For samples after aging, all thinning methods except atom milling without cooling had a significant effect, restoring them to the original s...

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Veröffentlicht in:Journal of alloys and compounds 2004-02, Vol.364 (1), p.257-270
1. Verfasser: Kondoh, Junya
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description The effect of ion milling and atom milling on the microstructure and the local structure of yttria-stabilized zirconia before and after aging was investigated. For samples after aging, all thinning methods except atom milling without cooling had a significant effect, restoring them to the original states before aging. These effects are attributed to current flow exceeding the mobility-controlled threshold depending on the temperature through a specimen. Because atom milling with cooling and ion milling completely eliminates aging-induced changes, these methods cannot be used in preparing transmission electron microscopy specimens to examine changes in the microstructures and the local structures of stabilized zirconia after aging.
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subjects Ceramics
Cross-disciplinary physics: materials science
rheology
Crystal structure
Exact sciences and technology
Ionic conduction
Materials science
Oxide materials
Physics
Point defects
TEM
Treatment of materials and its effects on microstructure and properties
title Recovery of the aging-induced changes in microstructures and local structures of yttria-stabilized zirconia due to ion and atom milling
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