Green extraction of Quercus infectoria gall with supercritical CO2 and methanol co-solvent
Green extraction of supercritical liquid CO 2 (SCFE-CO 2 ) using co-solvent methanol can produce a more complete phenolic acid composition and a higher quantity when compared to those without using co-solvent. The extract was devoid of toxicity. SCFE-CO 2 is carried out by putting 100 g of Quercus i...
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| Veröffentlicht in: | Environmental science and pollution research international 2023-11, Vol.30 (55), p.116952-116959 |
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| creator | Purbowati, Retno Taufikurohmah, Titik Syahrani, Achmad |
| description | Green extraction of supercritical liquid CO
2
(SCFE-CO
2
) using co-solvent methanol can produce a more complete phenolic acid composition and a higher quantity when compared to those without using co-solvent. The extract was devoid of toxicity. SCFE-CO
2
is carried out by putting 100 g of
Quercus infectoria
gall of size 0.3 mm into extraction tube at temperature of 60 °C and the pressure of 20 MPa with a CO
2
flow rate of 25 ml/min using co-solvent methanol with variation of flow speed 0.05, 0.5, 1.5, 3, and 6 for 60 min. The extract is analyzed using LC–MS/MS, the total phenolic content is determined using the Folin-Ceocateu method, and the toxicity value is determined using the Vero cell. According to the results, the green method of extracting SCFE-CO
2
with methanol co-solvent can produce a peak and identify about 27 phenolic compounds, and increasing the rate of flow of methane co-solvent will greatly affect the outcome of the extraction to a flow rate of 0.5 ml/min, while adding a co-solvent with a flow speed above 0.5 does not affect the result. Repeated extraction of some of the largest phenolic peaks provide phenol content with minimal extract variability (div. sd. 0.1%), and the addition of soluble methanol will also increase the TPC concentration but does not increase the IC
50
toxicity value above 1000. |
| doi_str_mv | 10.1007/s11356-023-28047-1 |
| format | Article |
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2
(SCFE-CO
2
) using co-solvent methanol can produce a more complete phenolic acid composition and a higher quantity when compared to those without using co-solvent. The extract was devoid of toxicity. SCFE-CO
2
is carried out by putting 100 g of
Quercus infectoria
gall of size 0.3 mm into extraction tube at temperature of 60 °C and the pressure of 20 MPa with a CO
2
flow rate of 25 ml/min using co-solvent methanol with variation of flow speed 0.05, 0.5, 1.5, 3, and 6 for 60 min. The extract is analyzed using LC–MS/MS, the total phenolic content is determined using the Folin-Ceocateu method, and the toxicity value is determined using the Vero cell. According to the results, the green method of extracting SCFE-CO
2
with methanol co-solvent can produce a peak and identify about 27 phenolic compounds, and increasing the rate of flow of methane co-solvent will greatly affect the outcome of the extraction to a flow rate of 0.5 ml/min, while adding a co-solvent with a flow speed above 0.5 does not affect the result. Repeated extraction of some of the largest phenolic peaks provide phenol content with minimal extract variability (div. sd. 0.1%), and the addition of soluble methanol will also increase the TPC concentration but does not increase the IC
50
toxicity value above 1000.</description><identifier>ISSN: 1614-7499</identifier><identifier>ISSN: 0944-1344</identifier><identifier>EISSN: 1614-7499</identifier><identifier>DOI: 10.1007/s11356-023-28047-1</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Aquatic Pollution ; Atmospheric Protection/Air Quality Control/Air Pollution ; Carbon dioxide ; Earth and Environmental Science ; Ecotoxicology ; Environment ; Environmental and Economic Returns ; Environmental Chemistry ; Environmental Health ; Flow rates ; Flow velocity ; Gall ; Methanol ; Phenolic acids ; Phenols ; Quercus infectoria ; Solvents ; Supercritical gas extraction ; Sustainable Energy for Better Social ; Toxicity ; Waste Water Technology ; Water Management ; Water Pollution Control</subject><ispartof>Environmental science and pollution research international, 2023-11, Vol.30 (55), p.116952-116959</ispartof><rights>The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c396t-439291febfa55c0b9c9a043bd6a5c95a74a3d3fb56b785b87a952a60a833b67f3</citedby><cites>FETCH-LOGICAL-c396t-439291febfa55c0b9c9a043bd6a5c95a74a3d3fb56b785b87a952a60a833b67f3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11356-023-28047-1$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11356-023-28047-1$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Purbowati, Retno</creatorcontrib><creatorcontrib>Taufikurohmah, Titik</creatorcontrib><creatorcontrib>Syahrani, Achmad</creatorcontrib><title>Green extraction of Quercus infectoria gall with supercritical CO2 and methanol co-solvent</title><title>Environmental science and pollution research international</title><addtitle>Environ Sci Pollut Res</addtitle><description>Green extraction of supercritical liquid CO
2
(SCFE-CO
2
) using co-solvent methanol can produce a more complete phenolic acid composition and a higher quantity when compared to those without using co-solvent. The extract was devoid of toxicity. SCFE-CO
2
is carried out by putting 100 g of
Quercus infectoria
gall of size 0.3 mm into extraction tube at temperature of 60 °C and the pressure of 20 MPa with a CO
2
flow rate of 25 ml/min using co-solvent methanol with variation of flow speed 0.05, 0.5, 1.5, 3, and 6 for 60 min. The extract is analyzed using LC–MS/MS, the total phenolic content is determined using the Folin-Ceocateu method, and the toxicity value is determined using the Vero cell. According to the results, the green method of extracting SCFE-CO
2
with methanol co-solvent can produce a peak and identify about 27 phenolic compounds, and increasing the rate of flow of methane co-solvent will greatly affect the outcome of the extraction to a flow rate of 0.5 ml/min, while adding a co-solvent with a flow speed above 0.5 does not affect the result. Repeated extraction of some of the largest phenolic peaks provide phenol content with minimal extract variability (div. sd. 0.1%), and the addition of soluble methanol will also increase the TPC concentration but does not increase the IC
50
toxicity value above 1000.</description><subject>Aquatic Pollution</subject><subject>Atmospheric Protection/Air Quality Control/Air Pollution</subject><subject>Carbon dioxide</subject><subject>Earth and Environmental Science</subject><subject>Ecotoxicology</subject><subject>Environment</subject><subject>Environmental and Economic Returns</subject><subject>Environmental Chemistry</subject><subject>Environmental Health</subject><subject>Flow rates</subject><subject>Flow velocity</subject><subject>Gall</subject><subject>Methanol</subject><subject>Phenolic acids</subject><subject>Phenols</subject><subject>Quercus infectoria</subject><subject>Solvents</subject><subject>Supercritical gas extraction</subject><subject>Sustainable Energy for Better Social</subject><subject>Toxicity</subject><subject>Waste Water Technology</subject><subject>Water Management</subject><subject>Water Pollution 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Titik</au><au>Syahrani, Achmad</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Green extraction of Quercus infectoria gall with supercritical CO2 and methanol co-solvent</atitle><jtitle>Environmental science and pollution research international</jtitle><stitle>Environ Sci Pollut Res</stitle><date>2023-11-01</date><risdate>2023</risdate><volume>30</volume><issue>55</issue><spage>116952</spage><epage>116959</epage><pages>116952-116959</pages><issn>1614-7499</issn><issn>0944-1344</issn><eissn>1614-7499</eissn><abstract>Green extraction of supercritical liquid CO
2
(SCFE-CO
2
) using co-solvent methanol can produce a more complete phenolic acid composition and a higher quantity when compared to those without using co-solvent. The extract was devoid of toxicity. SCFE-CO
2
is carried out by putting 100 g of
Quercus infectoria
gall of size 0.3 mm into extraction tube at temperature of 60 °C and the pressure of 20 MPa with a CO
2
flow rate of 25 ml/min using co-solvent methanol with variation of flow speed 0.05, 0.5, 1.5, 3, and 6 for 60 min. The extract is analyzed using LC–MS/MS, the total phenolic content is determined using the Folin-Ceocateu method, and the toxicity value is determined using the Vero cell. According to the results, the green method of extracting SCFE-CO
2
with methanol co-solvent can produce a peak and identify about 27 phenolic compounds, and increasing the rate of flow of methane co-solvent will greatly affect the outcome of the extraction to a flow rate of 0.5 ml/min, while adding a co-solvent with a flow speed above 0.5 does not affect the result. Repeated extraction of some of the largest phenolic peaks provide phenol content with minimal extract variability (div. sd. 0.1%), and the addition of soluble methanol will also increase the TPC concentration but does not increase the IC
50
toxicity value above 1000.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><doi>10.1007/s11356-023-28047-1</doi><tpages>8</tpages><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1614-7499 |
| ispartof | Environmental science and pollution research international, 2023-11, Vol.30 (55), p.116952-116959 |
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| subjects | Aquatic Pollution Atmospheric Protection/Air Quality Control/Air Pollution Carbon dioxide Earth and Environmental Science Ecotoxicology Environment Environmental and Economic Returns Environmental Chemistry Environmental Health Flow rates Flow velocity Gall Methanol Phenolic acids Phenols Quercus infectoria Solvents Supercritical gas extraction Sustainable Energy for Better Social Toxicity Waste Water Technology Water Management Water Pollution Control |
| title | Green extraction of Quercus infectoria gall with supercritical CO2 and methanol co-solvent |
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