Hydrogen sulfide removal from normal heptane using zinc oxide, silicon dioxide and zeolite 13X: adsorption capacity, kinetics, selectivity, breakthrough and regeneration
This article focuses on the H 2 S adsorption from normal heptane (nC 7 ) as synthetic natural gas liquids (NGL) using ZnO, SiO 2 and zeolite 13X in static mode. Results of the isotherm and kinetics of the investigated adsorbents for H 2 S adsorption under ambient condition showed that ZnO had the hi...
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| Veröffentlicht in: | Environmental science and pollution research international 2023-07, Vol.30 (35), p.84314-84333 |
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| creator | Zaeri, Mohammad Reza Esmaeilzadeh, Feridun |
| description | This article focuses on the H
2
S adsorption from normal heptane (nC
7
) as synthetic natural gas liquids (NGL) using ZnO, SiO
2
and zeolite 13X in static mode. Results of the isotherm and kinetics of the investigated adsorbents for H
2
S adsorption under ambient condition showed that ZnO had the highest H
2
S adsorption capacity between 260 and 700 mgH
2
S.g
-1
in the initial concentration range of 2500 and 7500 ppmH
2
S with an equilibrium time of less than 30 minutes. Additionally, the ZnO selectivity was greater than 3.16. In continued, H
2
S removal from nC
7
with ZnO was examined in dynamic mode. The H
2
S breakthrough time for ZnO reduced from 210 to 25 minutes as weight hourly space velocity (WHSV) was increased from 5 to 20 h
-1
at 30 bar. Also, the breakthrough time at 30 bar was about 2.5 times greater than that at atmospheric pressure. Furthermore, H
2
S/CO
2
mixture (i.e., 1000 ppmH
2
S + 1000 ppmCO
2
) caused the H
2
S breakthrough time to increase approximately by 1.11-fold. Alternatively, the ZnO regeneration conditions with hot stagnant air were optimized at different initial H
2
S concentrations (1000 ~ 3000 ppmH
2
S) using the Box-Behnken design. For instance, ZnO contaminated with 1000 ppmH
2
S was regenerated with an efficiency of more than 98 % for 160 minutes at 285 °C. |
| doi_str_mv | 10.1007/s11356-023-28411-1 |
| format | Article |
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2
S adsorption from normal heptane (nC
7
) as synthetic natural gas liquids (NGL) using ZnO, SiO
2
and zeolite 13X in static mode. Results of the isotherm and kinetics of the investigated adsorbents for H
2
S adsorption under ambient condition showed that ZnO had the highest H
2
S adsorption capacity between 260 and 700 mgH
2
S.g
-1
in the initial concentration range of 2500 and 7500 ppmH
2
S with an equilibrium time of less than 30 minutes. Additionally, the ZnO selectivity was greater than 3.16. In continued, H
2
S removal from nC
7
with ZnO was examined in dynamic mode. The H
2
S breakthrough time for ZnO reduced from 210 to 25 minutes as weight hourly space velocity (WHSV) was increased from 5 to 20 h
-1
at 30 bar. Also, the breakthrough time at 30 bar was about 2.5 times greater than that at atmospheric pressure. Furthermore, H
2
S/CO
2
mixture (i.e., 1000 ppmH
2
S + 1000 ppmCO
2
) caused the H
2
S breakthrough time to increase approximately by 1.11-fold. Alternatively, the ZnO regeneration conditions with hot stagnant air were optimized at different initial H
2
S concentrations (1000 ~ 3000 ppmH
2
S) using the Box-Behnken design. For instance, ZnO contaminated with 1000 ppmH
2
S was regenerated with an efficiency of more than 98 % for 160 minutes at 285 °C.</description><identifier>ISSN: 1614-7499</identifier><identifier>ISSN: 0944-1344</identifier><identifier>EISSN: 1614-7499</identifier><identifier>DOI: 10.1007/s11356-023-28411-1</identifier><identifier>PMID: 37365364</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Adsorption ; Aquatic Pollution ; Atmospheric Protection/Air Quality Control/Air Pollution ; Carbon dioxide ; Earth and Environmental Science ; Ecotoxicology ; Environment ; Environmental Chemistry ; Environmental Health ; Environmental science ; Heptanes ; Hydrogen Sulfide ; Kinetics ; Natural gas ; Regeneration ; Research Article ; Silicon Dioxide ; Substitute natural gas ; Waste Water Technology ; Water Management ; Water Pollution Control ; Zeolites ; Zinc Oxide ; Zinc oxides</subject><ispartof>Environmental science and pollution research international, 2023-07, Vol.30 (35), p.84314-84333</ispartof><rights>The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><rights>2023. The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c375t-e6c556dadebf6e49c01429a58e4a6c61ce54d9b8d32050373b1acb81e8c5b41b3</citedby><cites>FETCH-LOGICAL-c375t-e6c556dadebf6e49c01429a58e4a6c61ce54d9b8d32050373b1acb81e8c5b41b3</cites><orcidid>0000-0001-9801-9276</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11356-023-28411-1$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11356-023-28411-1$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/37365364$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Zaeri, Mohammad Reza</creatorcontrib><creatorcontrib>Esmaeilzadeh, Feridun</creatorcontrib><title>Hydrogen sulfide removal from normal heptane using zinc oxide, silicon dioxide and zeolite 13X: adsorption capacity, kinetics, selectivity, breakthrough and regeneration</title><title>Environmental science and pollution research international</title><addtitle>Environ Sci Pollut Res</addtitle><addtitle>Environ Sci Pollut Res Int</addtitle><description>This article focuses on the H
2
S adsorption from normal heptane (nC
7
) as synthetic natural gas liquids (NGL) using ZnO, SiO
2
and zeolite 13X in static mode. Results of the isotherm and kinetics of the investigated adsorbents for H
2
S adsorption under ambient condition showed that ZnO had the highest H
2
S adsorption capacity between 260 and 700 mgH
2
S.g
-1
in the initial concentration range of 2500 and 7500 ppmH
2
S with an equilibrium time of less than 30 minutes. Additionally, the ZnO selectivity was greater than 3.16. In continued, H
2
S removal from nC
7
with ZnO was examined in dynamic mode. The H
2
S breakthrough time for ZnO reduced from 210 to 25 minutes as weight hourly space velocity (WHSV) was increased from 5 to 20 h
-1
at 30 bar. Also, the breakthrough time at 30 bar was about 2.5 times greater than that at atmospheric pressure. Furthermore, H
2
S/CO
2
mixture (i.e., 1000 ppmH
2
S + 1000 ppmCO
2
) caused the H
2
S breakthrough time to increase approximately by 1.11-fold. Alternatively, the ZnO regeneration conditions with hot stagnant air were optimized at different initial H
2
S concentrations (1000 ~ 3000 ppmH
2
S) using the Box-Behnken design. For instance, ZnO contaminated with 1000 ppmH
2
S was regenerated with an efficiency of more than 98 % for 160 minutes at 285 °C.</description><subject>Adsorption</subject><subject>Aquatic Pollution</subject><subject>Atmospheric Protection/Air Quality Control/Air Pollution</subject><subject>Carbon dioxide</subject><subject>Earth and Environmental Science</subject><subject>Ecotoxicology</subject><subject>Environment</subject><subject>Environmental Chemistry</subject><subject>Environmental Health</subject><subject>Environmental science</subject><subject>Heptanes</subject><subject>Hydrogen Sulfide</subject><subject>Kinetics</subject><subject>Natural gas</subject><subject>Regeneration</subject><subject>Research Article</subject><subject>Silicon Dioxide</subject><subject>Substitute natural gas</subject><subject>Waste Water Technology</subject><subject>Water Management</subject><subject>Water Pollution Control</subject><subject>Zeolites</subject><subject>Zinc Oxide</subject><subject>Zinc 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science and pollution research international</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zaeri, Mohammad Reza</au><au>Esmaeilzadeh, Feridun</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Hydrogen sulfide removal from normal heptane using zinc oxide, silicon dioxide and zeolite 13X: adsorption capacity, kinetics, selectivity, breakthrough and regeneration</atitle><jtitle>Environmental science and pollution research international</jtitle><stitle>Environ Sci Pollut Res</stitle><addtitle>Environ Sci Pollut Res Int</addtitle><date>2023-07-01</date><risdate>2023</risdate><volume>30</volume><issue>35</issue><spage>84314</spage><epage>84333</epage><pages>84314-84333</pages><issn>1614-7499</issn><issn>0944-1344</issn><eissn>1614-7499</eissn><abstract>This article focuses on the H
2
S adsorption from normal heptane (nC
7
) as synthetic natural gas liquids (NGL) using ZnO, SiO
2
and zeolite 13X in static mode. Results of the isotherm and kinetics of the investigated adsorbents for H
2
S adsorption under ambient condition showed that ZnO had the highest H
2
S adsorption capacity between 260 and 700 mgH
2
S.g
-1
in the initial concentration range of 2500 and 7500 ppmH
2
S with an equilibrium time of less than 30 minutes. Additionally, the ZnO selectivity was greater than 3.16. In continued, H
2
S removal from nC
7
with ZnO was examined in dynamic mode. The H
2
S breakthrough time for ZnO reduced from 210 to 25 minutes as weight hourly space velocity (WHSV) was increased from 5 to 20 h
-1
at 30 bar. Also, the breakthrough time at 30 bar was about 2.5 times greater than that at atmospheric pressure. Furthermore, H
2
S/CO
2
mixture (i.e., 1000 ppmH
2
S + 1000 ppmCO
2
) caused the H
2
S breakthrough time to increase approximately by 1.11-fold. Alternatively, the ZnO regeneration conditions with hot stagnant air were optimized at different initial H
2
S concentrations (1000 ~ 3000 ppmH
2
S) using the Box-Behnken design. For instance, ZnO contaminated with 1000 ppmH
2
S was regenerated with an efficiency of more than 98 % for 160 minutes at 285 °C.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><pmid>37365364</pmid><doi>10.1007/s11356-023-28411-1</doi><tpages>20</tpages><orcidid>https://orcid.org/0000-0001-9801-9276</orcidid></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1614-7499 |
| ispartof | Environmental science and pollution research international, 2023-07, Vol.30 (35), p.84314-84333 |
| issn | 1614-7499 0944-1344 1614-7499 |
| language | eng |
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| source | MEDLINE; SpringerNature Journals |
| subjects | Adsorption Aquatic Pollution Atmospheric Protection/Air Quality Control/Air Pollution Carbon dioxide Earth and Environmental Science Ecotoxicology Environment Environmental Chemistry Environmental Health Environmental science Heptanes Hydrogen Sulfide Kinetics Natural gas Regeneration Research Article Silicon Dioxide Substitute natural gas Waste Water Technology Water Management Water Pollution Control Zeolites Zinc Oxide Zinc oxides |
| title | Hydrogen sulfide removal from normal heptane using zinc oxide, silicon dioxide and zeolite 13X: adsorption capacity, kinetics, selectivity, breakthrough and regeneration |
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