Synthesis and structure determination of a chain-like aluminophosphate obtained with 1,2-diaminopropane as the structure-directing agent
Colorless plate-like crystals (AlPO-1,2DAP) crystallize from a clear ‘AlPO 4-1,2-diaminopropane’ reaction system. The results of elemental, thermal and FTIR analyses give the following chemical formula: (NH 4 +)(1,2-H 2DAP) 2+(AlP 2O 8) 3−, confirmed also by single crystal structure determination. T...
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| Veröffentlicht in: | The Journal of physics and chemistry of solids 2003-07, Vol.64 (7), p.1097-1103 |
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| container_title | The Journal of physics and chemistry of solids |
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| creator | Rajic, Nevenka Logar, Natasa Zabukovec Golobic, Amalija Kaucic, Venceslav |
| description | Colorless plate-like crystals (AlPO-1,2DAP) crystallize from a clear ‘AlPO
4-1,2-diaminopropane’ reaction system. The results of elemental, thermal and FTIR analyses give the following chemical formula: (NH
4
+)(1,2-H
2DAP)
2+(AlP
2O
8)
3−, confirmed also by single crystal structure determination. The X-ray diffraction data collected at 150
K reveal the space group Pc2
1n with
a=8.2788(2),
b=16.7882(3),
c=8.6608(2)
Å, and
V=1203.73(5)
Å
3. The AlPO-1,2DAP has a chain structure related to the aluminophosphate AlPO-enA structure. Two occluded cations, NH
4
+ and doubly protonated diamine, balance the negative charge and interact with the chain oxygen atoms via hydrogen bond network. |
| doi_str_mv | 10.1016/S0022-3697(03)00002-7 |
| format | Article |
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4-1,2-diaminopropane’ reaction system. The results of elemental, thermal and FTIR analyses give the following chemical formula: (NH
4
+)(1,2-H
2DAP)
2+(AlP
2O
8)
3−, confirmed also by single crystal structure determination. The X-ray diffraction data collected at 150
K reveal the space group Pc2
1n with
a=8.2788(2),
b=16.7882(3),
c=8.6608(2)
Å, and
V=1203.73(5)
Å
3. The AlPO-1,2DAP has a chain structure related to the aluminophosphate AlPO-enA structure. Two occluded cations, NH
4
+ and doubly protonated diamine, balance the negative charge and interact with the chain oxygen atoms via hydrogen bond network.</description><identifier>ISSN: 0022-3697</identifier><identifier>EISSN: 1879-2553</identifier><identifier>DOI: 10.1016/S0022-3697(03)00002-7</identifier><language>eng</language><publisher>Oxford: Elsevier Ltd</publisher><subject>C. X-ray diffraction ; Condensed matter: structure, mechanical and thermal properties ; Cross-disciplinary physics: materials science; rheology ; D. Crystal structure ; Exact sciences and technology ; Inorganic compounds ; Materials science ; Materials testing ; Physics ; Structure of solids and liquids; crystallography ; Structure of specific crystalline solids ; Thermal analysis, differential thermal analysis (DTA), differential thermogravimetric analysis</subject><ispartof>The Journal of physics and chemistry of solids, 2003-07, Vol.64 (7), p.1097-1103</ispartof><rights>2003 Elsevier Science Ltd</rights><rights>2003 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c368t-7dc2a97758ef0401a7d1ed76d495b3ccdc24e26dc9c36027828a54cbd8057a883</citedby><cites>FETCH-LOGICAL-c368t-7dc2a97758ef0401a7d1ed76d495b3ccdc24e26dc9c36027828a54cbd8057a883</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/S0022-3697(03)00002-7$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=14765861$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Rajic, Nevenka</creatorcontrib><creatorcontrib>Logar, Natasa Zabukovec</creatorcontrib><creatorcontrib>Golobic, Amalija</creatorcontrib><creatorcontrib>Kaucic, Venceslav</creatorcontrib><title>Synthesis and structure determination of a chain-like aluminophosphate obtained with 1,2-diaminopropane as the structure-directing agent</title><title>The Journal of physics and chemistry of solids</title><description>Colorless plate-like crystals (AlPO-1,2DAP) crystallize from a clear ‘AlPO
4-1,2-diaminopropane’ reaction system. The results of elemental, thermal and FTIR analyses give the following chemical formula: (NH
4
+)(1,2-H
2DAP)
2+(AlP
2O
8)
3−, confirmed also by single crystal structure determination. The X-ray diffraction data collected at 150
K reveal the space group Pc2
1n with
a=8.2788(2),
b=16.7882(3),
c=8.6608(2)
Å, and
V=1203.73(5)
Å
3. The AlPO-1,2DAP has a chain structure related to the aluminophosphate AlPO-enA structure. Two occluded cations, NH
4
+ and doubly protonated diamine, balance the negative charge and interact with the chain oxygen atoms via hydrogen bond network.</description><subject>C. X-ray diffraction</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>D. Crystal structure</subject><subject>Exact sciences and technology</subject><subject>Inorganic compounds</subject><subject>Materials science</subject><subject>Materials testing</subject><subject>Physics</subject><subject>Structure of solids and liquids; crystallography</subject><subject>Structure of specific crystalline solids</subject><subject>Thermal analysis, differential thermal analysis (DTA), differential thermogravimetric analysis</subject><issn>0022-3697</issn><issn>1879-2553</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2003</creationdate><recordtype>article</recordtype><recordid>eNqFkEFv1DAQhS0EEkvhJyD50gqkBmwnjp0TQhVtkSpxKJytWXvSuM3ai-0U9R_ws-vdreiRufjwvjdv_Ah5z9knznj_-ZoxIZq2H9QH1n5kdUSjXpAV12pohJTtS7L6h7wmb3K-rYzkA1-Rv9cPoUyYfaYQHM0lLbYsCanDgmnjAxQfA40jBWon8KGZ_R1SmJeqxe0U83aCgjSuSxXR0T--TJSfisZ52CMpbiFUR6Y15zmg6glt8eGGwg2G8pa8GmHO-O7pPSK_zr_9PLtsrn5cfD_7etXYttelUc4KGJSSGkfWMQ7KcXSqd90g1621Ve5Q9M4OlWdCaaFBdnbtNJMKtG6PyMlhbz3s94K5mI3PFue5HhmXbIRm7a6nCsoDaFPMOeFotslvID0Yzsyud7Pv3exgw1qz793sfMdPAZAtzGOCYH1-Nneql7rnlfty4LD-9t5jMtl6DBYPxRgX_X-SHgFVHpo3</recordid><startdate>20030701</startdate><enddate>20030701</enddate><creator>Rajic, Nevenka</creator><creator>Logar, Natasa Zabukovec</creator><creator>Golobic, Amalija</creator><creator>Kaucic, Venceslav</creator><general>Elsevier Ltd</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20030701</creationdate><title>Synthesis and structure determination of a chain-like aluminophosphate obtained with 1,2-diaminopropane as the structure-directing agent</title><author>Rajic, Nevenka ; Logar, Natasa Zabukovec ; Golobic, Amalija ; Kaucic, Venceslav</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c368t-7dc2a97758ef0401a7d1ed76d495b3ccdc24e26dc9c36027828a54cbd8057a883</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2003</creationdate><topic>C. X-ray diffraction</topic><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>D. Crystal structure</topic><topic>Exact sciences and technology</topic><topic>Inorganic compounds</topic><topic>Materials science</topic><topic>Materials testing</topic><topic>Physics</topic><topic>Structure of solids and liquids; crystallography</topic><topic>Structure of specific crystalline solids</topic><topic>Thermal analysis, differential thermal analysis (DTA), differential thermogravimetric analysis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Rajic, Nevenka</creatorcontrib><creatorcontrib>Logar, Natasa Zabukovec</creatorcontrib><creatorcontrib>Golobic, Amalija</creatorcontrib><creatorcontrib>Kaucic, Venceslav</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>The Journal of physics and chemistry of solids</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Rajic, Nevenka</au><au>Logar, Natasa Zabukovec</au><au>Golobic, Amalija</au><au>Kaucic, Venceslav</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and structure determination of a chain-like aluminophosphate obtained with 1,2-diaminopropane as the structure-directing agent</atitle><jtitle>The Journal of physics and chemistry of solids</jtitle><date>2003-07-01</date><risdate>2003</risdate><volume>64</volume><issue>7</issue><spage>1097</spage><epage>1103</epage><pages>1097-1103</pages><issn>0022-3697</issn><eissn>1879-2553</eissn><abstract>Colorless plate-like crystals (AlPO-1,2DAP) crystallize from a clear ‘AlPO
4-1,2-diaminopropane’ reaction system. The results of elemental, thermal and FTIR analyses give the following chemical formula: (NH
4
+)(1,2-H
2DAP)
2+(AlP
2O
8)
3−, confirmed also by single crystal structure determination. The X-ray diffraction data collected at 150
K reveal the space group Pc2
1n with
a=8.2788(2),
b=16.7882(3),
c=8.6608(2)
Å, and
V=1203.73(5)
Å
3. The AlPO-1,2DAP has a chain structure related to the aluminophosphate AlPO-enA structure. Two occluded cations, NH
4
+ and doubly protonated diamine, balance the negative charge and interact with the chain oxygen atoms via hydrogen bond network.</abstract><cop>Oxford</cop><pub>Elsevier Ltd</pub><doi>10.1016/S0022-3697(03)00002-7</doi><tpages>7</tpages></addata></record> |
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| subjects | C. X-ray diffraction Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science rheology D. Crystal structure Exact sciences and technology Inorganic compounds Materials science Materials testing Physics Structure of solids and liquids crystallography Structure of specific crystalline solids Thermal analysis, differential thermal analysis (DTA), differential thermogravimetric analysis |
| title | Synthesis and structure determination of a chain-like aluminophosphate obtained with 1,2-diaminopropane as the structure-directing agent |
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