Continuous deposition of thermally co-evaporated YBCO/CeO/sub 2//Ni coated conductors

By using a simple single-pass reel-to-reel system, we demonstrate a simple and robust in-situ route for the continuous deposition of 1-2 m long Coated Conductors (CC) consisting of 1 /spl mu/m thick superconducting YBa/sub 2/Cu/sub 3/O/sub 7/ (YBCO) films deposited by thermal co-evaporation onto 100...

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Veröffentlicht in:IEEE transactions on applied superconductivity 2005-06, Vol.15 (2), p.2628-2631
Hauptverfasser: Gauzzi, A., Bindi, M., Gianni, L., Ginocchio, S., Zannella, S., Baldini, A., Holzapfel, B., Bolzoni, F.
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container_end_page 2631
container_issue 2
container_start_page 2628
container_title IEEE transactions on applied superconductivity
container_volume 15
creator Gauzzi, A.
Bindi, M.
Gianni, L.
Ginocchio, S.
Zannella, S.
Baldini, A.
Holzapfel, B.
Bolzoni, F.
description By using a simple single-pass reel-to-reel system, we demonstrate a simple and robust in-situ route for the continuous deposition of 1-2 m long Coated Conductors (CC) consisting of 1 /spl mu/m thick superconducting YBa/sub 2/Cu/sub 3/O/sub 7/ (YBCO) films deposited by thermal co-evaporation onto 100 nm thick CeO/sub 2/ buffered cube textured Ni tapes. The buffer layer was deposited by either e-beam or thermal evaporation using respectively ceria or metallic cerium. The structural and morphological properties of the samples were investigated by X-ray /spl thetav/-2/spl thetav/ Bragg-Brentano, and pole figure diffraction, Nomarsky optical microscopy and Scanning Electron Microscopy (SEM) analysis. The 123 composition was controlled during deposition by means of an atomic absorption system. The optimized buffer layer and YBCO layer are grown at 690/spl deg/C in respectively forming gas and oxygen partial pressures of 5/spl times/10/sup -5/ mbar. These conditions ensure the growth of dense and crack-free layers with good biaxial texture, as indicated by FWHM's values in the 5-7/spl deg/ range for both in- and out-of-plane orientations. Zero-resistance critical temperatures T/sub c/=86-87 K with transition widths /spl Delta/T/sub c/
doi_str_mv 10.1109/TASC.2005.847685
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The buffer layer was deposited by either e-beam or thermal evaporation using respectively ceria or metallic cerium. The structural and morphological properties of the samples were investigated by X-ray /spl thetav/-2/spl thetav/ Bragg-Brentano, and pole figure diffraction, Nomarsky optical microscopy and Scanning Electron Microscopy (SEM) analysis. The 123 composition was controlled during deposition by means of an atomic absorption system. The optimized buffer layer and YBCO layer are grown at 690/spl deg/C in respectively forming gas and oxygen partial pressures of 5/spl times/10/sup -5/ mbar. These conditions ensure the growth of dense and crack-free layers with good biaxial texture, as indicated by FWHM's values in the 5-7/spl deg/ range for both in- and out-of-plane orientations. Zero-resistance critical temperatures T/sub c/=86-87 K with transition widths /spl Delta/T/sub c/&lt;3 K are reproducibly obtained. End-to-end critical current densities J/sub c/ at 77 K and self-field typically are in the 1.5-2.5 MA/cm/sup 2/ range, as measured by transport measurements. 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End-to-end critical current densities J/sub c/ at 77 K and self-field typically are in the 1.5-2.5 MA/cm/sup 2/ range, as measured by transport measurements. 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The buffer layer was deposited by either e-beam or thermal evaporation using respectively ceria or metallic cerium. The structural and morphological properties of the samples were investigated by X-ray /spl thetav/-2/spl thetav/ Bragg-Brentano, and pole figure diffraction, Nomarsky optical microscopy and Scanning Electron Microscopy (SEM) analysis. The 123 composition was controlled during deposition by means of an atomic absorption system. The optimized buffer layer and YBCO layer are grown at 690/spl deg/C in respectively forming gas and oxygen partial pressures of 5/spl times/10/sup -5/ mbar. These conditions ensure the growth of dense and crack-free layers with good biaxial texture, as indicated by FWHM's values in the 5-7/spl deg/ range for both in- and out-of-plane orientations. Zero-resistance critical temperatures T/sub c/=86-87 K with transition widths /spl Delta/T/sub c/&lt;3 K are reproducibly obtained. End-to-end critical current densities J/sub c/ at 77 K and self-field typically are in the 1.5-2.5 MA/cm/sup 2/ range, as measured by transport measurements. It is found that tape motion does not significantly affect these properties.</abstract><pub>IEEE</pub><doi>10.1109/TASC.2005.847685</doi><tpages>4</tpages></addata></record>
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subjects Buffer layers
Conductive films
continuous deposition
Current measurement
Density measurement
Optical buffering
Optical microscopy
Robustness
Scanning electron microscopy
Superconducting films
thermal co-evaporation
YBCO
Yttrium barium copper oxide
title Continuous deposition of thermally co-evaporated YBCO/CeO/sub 2//Ni coated conductors
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