Sintering of Pollucite Using Amorphous Powder and Its Low Thermal Expansion Property
Calcined powders were prepared for sintering of cubic Cs0.9Al0.9Si2.1O6 by calcining a mixture of Al2O3/SiO2 fine powder and CsNO3 powder at temperatures of 798 to 1123K for 20h in air. The amorphous phase produced in the case of a lower calcination temperature, while the crystallinity of the calcin...
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Veröffentlicht in: | Journal of the Ceramic Society of Japan 2003, Vol.111(1296), pp.533-536 |
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creator | YANASE, Ikuo TAMAI, Sachiko KOBAYASHI, Hidehiko |
description | Calcined powders were prepared for sintering of cubic Cs0.9Al0.9Si2.1O6 by calcining a mixture of Al2O3/SiO2 fine powder and CsNO3 powder at temperatures of 798 to 1123K for 20h in air. The amorphous phase produced in the case of a lower calcination temperature, while the crystallinity of the calcined powder increased with increasing calcination temperature. Densification of the Cs0.9Al0.9Si2.1O6 green body was significantly enhanced using the amorphous calcined powder. The relative density of the Cs0.9Al0.9Si2.1O6 sintered body reached 94.5% when the green body of the amorphous calcined powder, including a slight amount of CsNO3, was sintered at 1673K for 20h in air. The dense cubic Cs0.9Al0.9Si2.1O6 sintered body showed linear thermal expansion without hysteresis, resulting in a thermal expansion rate of ca. 0.13% at 1273K. |
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The amorphous phase produced in the case of a lower calcination temperature, while the crystallinity of the calcined powder increased with increasing calcination temperature. Densification of the Cs0.9Al0.9Si2.1O6 green body was significantly enhanced using the amorphous calcined powder. The relative density of the Cs0.9Al0.9Si2.1O6 sintered body reached 94.5% when the green body of the amorphous calcined powder, including a slight amount of CsNO3, was sintered at 1673K for 20h in air. The dense cubic Cs0.9Al0.9Si2.1O6 sintered body showed linear thermal expansion without hysteresis, resulting in a thermal expansion rate of ca. 0.13% at 1273K.</description><identifier>ISSN: 0914-5400</identifier><identifier>EISSN: 1882-1022</identifier><identifier>DOI: 10.2109/jcersj.111.533</identifier><language>eng</language><publisher>The Ceramic Society of Japan</publisher><subject>Calcined powder ; Cubic ; Low thermal expansion ; Pollucite ; Sintered body</subject><ispartof>Journal of the Ceramic Society of Japan, 2003, Vol.111(1296), pp.533-536</ispartof><rights>2003 The Ceramic Society of Japan</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c400t-66e64c6fdf6a6224e7bdb06cf08f2e5c293a341397efea549b120423c56053443</citedby><cites>FETCH-LOGICAL-c400t-66e64c6fdf6a6224e7bdb06cf08f2e5c293a341397efea549b120423c56053443</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,1876,27903,27904</link.rule.ids></links><search><creatorcontrib>YANASE, Ikuo</creatorcontrib><creatorcontrib>TAMAI, Sachiko</creatorcontrib><creatorcontrib>KOBAYASHI, Hidehiko</creatorcontrib><title>Sintering of Pollucite Using Amorphous Powder and Its Low Thermal Expansion Property</title><title>Journal of the Ceramic Society of Japan</title><addtitle>J. Ceram. Soc. Japan</addtitle><description>Calcined powders were prepared for sintering of cubic Cs0.9Al0.9Si2.1O6 by calcining a mixture of Al2O3/SiO2 fine powder and CsNO3 powder at temperatures of 798 to 1123K for 20h in air. The amorphous phase produced in the case of a lower calcination temperature, while the crystallinity of the calcined powder increased with increasing calcination temperature. Densification of the Cs0.9Al0.9Si2.1O6 green body was significantly enhanced using the amorphous calcined powder. The relative density of the Cs0.9Al0.9Si2.1O6 sintered body reached 94.5% when the green body of the amorphous calcined powder, including a slight amount of CsNO3, was sintered at 1673K for 20h in air. The dense cubic Cs0.9Al0.9Si2.1O6 sintered body showed linear thermal expansion without hysteresis, resulting in a thermal expansion rate of ca. 0.13% at 1273K.</description><subject>Calcined powder</subject><subject>Cubic</subject><subject>Low thermal expansion</subject><subject>Pollucite</subject><subject>Sintered body</subject><issn>0914-5400</issn><issn>1882-1022</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2003</creationdate><recordtype>article</recordtype><recordid>eNpNkE1PwkAQhjdGEwly9bwnb6371aV7JAQVQyKJcN5st1Moabt1twT595bUoKeZzDzvZPIg9EhJzChRzwcLPhxiSmmccH6DRjRNWUQJY7doRBQVUSIIuUeTEMqMECZSIQkfoc1n2XTgy2aHXYHXrqqOtuwAb8NlNKudb_fuGPrNKQePTZPjZRfwyp3wZg--NhVefLemCaVr8Nq7Fnx3fkB3hakCTH7rGG1fFpv5W7T6eF3OZ6vI9r90kZQghZVFXkgjGRMwzfKMSFuQtGCQWKa44YJyNYUCTCJURhkRjNtEkoQLwcfoabjbevd1hNDpugwWqso00D-t2VQpSRTvwXgArXcheCh068va-LOmRF_86cGf7v3p3l8feB8Ch9CZHVxx47vSVvAfp0zJv6YPXyG7N15Dw38AoGF-gA</recordid><startdate>20030801</startdate><enddate>20030801</enddate><creator>YANASE, Ikuo</creator><creator>TAMAI, Sachiko</creator><creator>KOBAYASHI, Hidehiko</creator><general>The Ceramic Society of Japan</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20030801</creationdate><title>Sintering of Pollucite Using Amorphous Powder and Its Low Thermal Expansion Property</title><author>YANASE, Ikuo ; TAMAI, Sachiko ; KOBAYASHI, Hidehiko</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c400t-66e64c6fdf6a6224e7bdb06cf08f2e5c293a341397efea549b120423c56053443</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2003</creationdate><topic>Calcined powder</topic><topic>Cubic</topic><topic>Low thermal expansion</topic><topic>Pollucite</topic><topic>Sintered body</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>YANASE, Ikuo</creatorcontrib><creatorcontrib>TAMAI, Sachiko</creatorcontrib><creatorcontrib>KOBAYASHI, Hidehiko</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of the Ceramic Society of Japan</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>YANASE, Ikuo</au><au>TAMAI, Sachiko</au><au>KOBAYASHI, Hidehiko</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Sintering of Pollucite Using Amorphous Powder and Its Low Thermal Expansion Property</atitle><jtitle>Journal of the Ceramic Society of Japan</jtitle><addtitle>J. Ceram. Soc. Japan</addtitle><date>2003-08-01</date><risdate>2003</risdate><volume>111</volume><issue>1296</issue><spage>533</spage><epage>536</epage><pages>533-536</pages><issn>0914-5400</issn><eissn>1882-1022</eissn><abstract>Calcined powders were prepared for sintering of cubic Cs0.9Al0.9Si2.1O6 by calcining a mixture of Al2O3/SiO2 fine powder and CsNO3 powder at temperatures of 798 to 1123K for 20h in air. The amorphous phase produced in the case of a lower calcination temperature, while the crystallinity of the calcined powder increased with increasing calcination temperature. Densification of the Cs0.9Al0.9Si2.1O6 green body was significantly enhanced using the amorphous calcined powder. The relative density of the Cs0.9Al0.9Si2.1O6 sintered body reached 94.5% when the green body of the amorphous calcined powder, including a slight amount of CsNO3, was sintered at 1673K for 20h in air. The dense cubic Cs0.9Al0.9Si2.1O6 sintered body showed linear thermal expansion without hysteresis, resulting in a thermal expansion rate of ca. 0.13% at 1273K.</abstract><pub>The Ceramic Society of Japan</pub><doi>10.2109/jcersj.111.533</doi><tpages>4</tpages><oa>free_for_read</oa></addata></record> |
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subjects | Calcined powder Cubic Low thermal expansion Pollucite Sintered body |
title | Sintering of Pollucite Using Amorphous Powder and Its Low Thermal Expansion Property |
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