Electroplating of iron from alkaline gluconate baths
Electroplating of iron onto copper substrates from non-polluting baths containing ferrous sulfate and sodium gluconate has been investigated under different bath composition, pH, temperature and current density conditions. A detailed study has been made on the influence of these parameters on potent...
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| Veröffentlicht in: | Thin solid films 2003-10, Vol.443 (1), p.53-59 |
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| creator | Abd El Meguid, E.A Abd El Rehim, S.S Moustafa, E.M |
| description | Electroplating of iron onto copper substrates from non-polluting baths containing ferrous sulfate and sodium gluconate has been investigated under different bath composition, pH, temperature and current density conditions. A detailed study has been made on the influence of these parameters on potentiodynamic polarization curves, cathodic current efficiency and throwing power of the baths. The optimum plating bath has been found to be: 0.072 mol/l FeSO
4·7H
2O, 0.23 mol/l sodium gluconate, pH 12, current density of 0.167 A dm
−2 and at 25 °C. This bath is characterized by an excellent throwing power. The surface morphology of the as-deposited iron was investigated by using scanning electron microscope (SEM) while the crystal structure was examined by using X-ray diffraction analysis. |
| doi_str_mv | 10.1016/S0040-6090(03)00942-8 |
| format | Article |
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4·7H
2O, 0.23 mol/l sodium gluconate, pH 12, current density of 0.167 A dm
−2 and at 25 °C. This bath is characterized by an excellent throwing power. The surface morphology of the as-deposited iron was investigated by using scanning electron microscope (SEM) while the crystal structure was examined by using X-ray diffraction analysis.</description><identifier>ISSN: 0040-6090</identifier><identifier>EISSN: 1879-2731</identifier><identifier>DOI: 10.1016/S0040-6090(03)00942-8</identifier><identifier>CODEN: THSFAP</identifier><language>eng</language><publisher>Lausanne: Elsevier B.V</publisher><subject>Applied sciences ; Coatings ; Cross-disciplinary physics: materials science; rheology ; Electrodeposition, electroplating ; Electroplating ; Exact sciences and technology ; Iron ; Materials science ; Metallic coatings ; Metals. Metallurgy ; Methods of deposition of films and coatings; film growth and epitaxy ; Physics ; Production techniques ; Surface treatment</subject><ispartof>Thin solid films, 2003-10, Vol.443 (1), p.53-59</ispartof><rights>2003 Elsevier B.V.</rights><rights>2003 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c368t-82c072460652f84a317750f1c7c455d6f65891ab3157f9cb0c2350c4d796343c3</citedby><cites>FETCH-LOGICAL-c368t-82c072460652f84a317750f1c7c455d6f65891ab3157f9cb0c2350c4d796343c3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/S0040-6090(03)00942-8$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3548,27922,27923,45993</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=15155115$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Abd El Meguid, E.A</creatorcontrib><creatorcontrib>Abd El Rehim, S.S</creatorcontrib><creatorcontrib>Moustafa, E.M</creatorcontrib><title>Electroplating of iron from alkaline gluconate baths</title><title>Thin solid films</title><description>Electroplating of iron onto copper substrates from non-polluting baths containing ferrous sulfate and sodium gluconate has been investigated under different bath composition, pH, temperature and current density conditions. A detailed study has been made on the influence of these parameters on potentiodynamic polarization curves, cathodic current efficiency and throwing power of the baths. The optimum plating bath has been found to be: 0.072 mol/l FeSO
4·7H
2O, 0.23 mol/l sodium gluconate, pH 12, current density of 0.167 A dm
−2 and at 25 °C. This bath is characterized by an excellent throwing power. The surface morphology of the as-deposited iron was investigated by using scanning electron microscope (SEM) while the crystal structure was examined by using X-ray diffraction analysis.</description><subject>Applied sciences</subject><subject>Coatings</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Electrodeposition, electroplating</subject><subject>Electroplating</subject><subject>Exact sciences and technology</subject><subject>Iron</subject><subject>Materials science</subject><subject>Metallic coatings</subject><subject>Metals. Metallurgy</subject><subject>Methods of deposition of films and coatings; film growth and epitaxy</subject><subject>Physics</subject><subject>Production techniques</subject><subject>Surface treatment</subject><issn>0040-6090</issn><issn>1879-2731</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2003</creationdate><recordtype>article</recordtype><recordid>eNqFkEtLAzEUhYMoWKs_QZiNoovRm3dmJVLqAwou1HVI06RG00lNpoL_3ukDXbq6m--cw_0QOsVwhQGL62cABrWABi6AXgI0jNRqDw2wkk1NJMX7aPCLHKKjUt4BABNCB4iNo7NdTstoutDOq-SrkFNb-ZwWlYkfJobWVfO4sqk1naumpnsrx-jAm1jcye4O0evd-GX0UE-e7h9Ht5PaUqG6WhELkjABghOvmKFYSg4eW2kZ5zPhBVcNNlOKufSNnYIllINlM9kIyqilQ3S-7V3m9LlypdOLUKyL0bQurYomUhGJCfQg34I2p1Ky83qZw8Lkb41Brx3pjSO9FqCB6o0jrfrc2W7AFGuiz6a1ofyFOeYcY95zN1vO9d9-BZd1scG11s1C7vXpWQr_LP0Adbd4wQ</recordid><startdate>20031022</startdate><enddate>20031022</enddate><creator>Abd El Meguid, E.A</creator><creator>Abd El Rehim, S.S</creator><creator>Moustafa, E.M</creator><general>Elsevier B.V</general><general>Elsevier Science</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20031022</creationdate><title>Electroplating of iron from alkaline gluconate baths</title><author>Abd El Meguid, E.A ; Abd El Rehim, S.S ; Moustafa, E.M</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c368t-82c072460652f84a317750f1c7c455d6f65891ab3157f9cb0c2350c4d796343c3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2003</creationdate><topic>Applied sciences</topic><topic>Coatings</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Electrodeposition, electroplating</topic><topic>Electroplating</topic><topic>Exact sciences and technology</topic><topic>Iron</topic><topic>Materials science</topic><topic>Metallic coatings</topic><topic>Metals. Metallurgy</topic><topic>Methods of deposition of films and coatings; film growth and epitaxy</topic><topic>Physics</topic><topic>Production techniques</topic><topic>Surface treatment</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Abd El Meguid, E.A</creatorcontrib><creatorcontrib>Abd El Rehim, S.S</creatorcontrib><creatorcontrib>Moustafa, E.M</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Thin solid films</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Abd El Meguid, E.A</au><au>Abd El Rehim, S.S</au><au>Moustafa, E.M</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Electroplating of iron from alkaline gluconate baths</atitle><jtitle>Thin solid films</jtitle><date>2003-10-22</date><risdate>2003</risdate><volume>443</volume><issue>1</issue><spage>53</spage><epage>59</epage><pages>53-59</pages><issn>0040-6090</issn><eissn>1879-2731</eissn><coden>THSFAP</coden><abstract>Electroplating of iron onto copper substrates from non-polluting baths containing ferrous sulfate and sodium gluconate has been investigated under different bath composition, pH, temperature and current density conditions. A detailed study has been made on the influence of these parameters on potentiodynamic polarization curves, cathodic current efficiency and throwing power of the baths. The optimum plating bath has been found to be: 0.072 mol/l FeSO
4·7H
2O, 0.23 mol/l sodium gluconate, pH 12, current density of 0.167 A dm
−2 and at 25 °C. This bath is characterized by an excellent throwing power. The surface morphology of the as-deposited iron was investigated by using scanning electron microscope (SEM) while the crystal structure was examined by using X-ray diffraction analysis.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/S0040-6090(03)00942-8</doi><tpages>7</tpages></addata></record> |
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| subjects | Applied sciences Coatings Cross-disciplinary physics: materials science rheology Electrodeposition, electroplating Electroplating Exact sciences and technology Iron Materials science Metallic coatings Metals. Metallurgy Methods of deposition of films and coatings film growth and epitaxy Physics Production techniques Surface treatment |
| title | Electroplating of iron from alkaline gluconate baths |
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