Development for the Simultaneous Analytical Method of Furan and Alkyl Furans in Processed Foods
A simultaneous analytical method was developed for the determination of alkyl furans (Furan, 2-methylfuran, 3-methylfuran and 2,5-dimethylfuran) in processed foods by headspace-GC-MS. Single-laboratory validation data of furan, 2-methylfuran, 3-methylfuran and 2,5-dimethylfuran showed good precision...
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Veröffentlicht in: | Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi) 2023/02/25, Vol.64(1), pp.29-33 |
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container_title | Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi) |
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creator | Ogiso, Motoki Hashimoto, Chihiro Toriumi, Eisuke Nishimura, Kanako Iizuka, Seiichiro Sakamoto, Kazuhiro Yamamoto, Yushi Yamada, Yukiko |
description | A simultaneous analytical method was developed for the determination of alkyl furans (Furan, 2-methylfuran, 3-methylfuran and 2,5-dimethylfuran) in processed foods by headspace-GC-MS. Single-laboratory validation data of furan, 2-methylfuran, 3-methylfuran and 2,5-dimethylfuran showed good precision and accuracy. The mean recoveries ranged from 92 to 116%, the intermediate precision (RSDi) ranged from 0.9 to 12.9%. The level of LOQ ranged from 0.5 to 1.2 μg/kg (coffee), from 3.5 to 4.1 μg/kg (soy sauce), from 0.4 to 1.3 μg/kg (other foods: clear apple juice, infant formula and baby food), respectively. This method has the sensitivity to detect low levels of furan and alkyl furans contaminated in various foods and is thus applicable to surveillance for risk management in food safety. |
doi_str_mv | 10.3358/shokueishi.64.29 |
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Single-laboratory validation data of furan, 2-methylfuran, 3-methylfuran and 2,5-dimethylfuran showed good precision and accuracy. The mean recoveries ranged from 92 to 116%, the intermediate precision (RSDi) ranged from 0.9 to 12.9%. The level of LOQ ranged from 0.5 to 1.2 μg/kg (coffee), from 3.5 to 4.1 μg/kg (soy sauce), from 0.4 to 1.3 μg/kg (other foods: clear apple juice, infant formula and baby food), respectively. This method has the sensitivity to detect low levels of furan and alkyl furans contaminated in various foods and is thus applicable to surveillance for risk management in food safety.</description><identifier>ISSN: 0015-6426</identifier><identifier>EISSN: 1882-1006</identifier><identifier>DOI: 10.3358/shokueishi.64.29</identifier><identifier>PMID: 36858589</identifier><language>eng ; jpn</language><publisher>Japan: Japanese Society for Food Hygiene and Safety</publisher><subject>Analytical methods ; apple juice ; baby food ; Baby foods ; Coffee ; dimethylfuran ; Food contamination ; Food processing ; Food Safety ; Food, Processed ; Fruit juices ; furan ; Furans ; headspace-GC-MS ; Humans ; Infant ; infant formula ; methylfuran ; Pesticides ; Processed foods ; Risk management ; Safety management ; Soy sauce</subject><ispartof>Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi), 2023/02/25, Vol.64(1), pp.29-33</ispartof><rights>2023 Japanese Society for Food Hygiene and Safety</rights><rights>Copyright Japan Science and Technology Agency 2023</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c1859-eb387e12b957b980fa9f1f8c32fd87d299c5a5a9328a59db67ffd184a5bc69643</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,4010,27900,27901,27902</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/36858589$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Ogiso, Motoki</creatorcontrib><creatorcontrib>Hashimoto, Chihiro</creatorcontrib><creatorcontrib>Toriumi, Eisuke</creatorcontrib><creatorcontrib>Nishimura, Kanako</creatorcontrib><creatorcontrib>Iizuka, Seiichiro</creatorcontrib><creatorcontrib>Sakamoto, Kazuhiro</creatorcontrib><creatorcontrib>Yamamoto, Yushi</creatorcontrib><creatorcontrib>Yamada, Yukiko</creatorcontrib><title>Development for the Simultaneous Analytical Method of Furan and Alkyl Furans in Processed Foods</title><title>Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi)</title><addtitle>Food Hyg. Saf. Sci.</addtitle><description>A simultaneous analytical method was developed for the determination of alkyl furans (Furan, 2-methylfuran, 3-methylfuran and 2,5-dimethylfuran) in processed foods by headspace-GC-MS. Single-laboratory validation data of furan, 2-methylfuran, 3-methylfuran and 2,5-dimethylfuran showed good precision and accuracy. The mean recoveries ranged from 92 to 116%, the intermediate precision (RSDi) ranged from 0.9 to 12.9%. The level of LOQ ranged from 0.5 to 1.2 μg/kg (coffee), from 3.5 to 4.1 μg/kg (soy sauce), from 0.4 to 1.3 μg/kg (other foods: clear apple juice, infant formula and baby food), respectively. This method has the sensitivity to detect low levels of furan and alkyl furans contaminated in various foods and is thus applicable to surveillance for risk management in food safety.</description><subject>Analytical methods</subject><subject>apple juice</subject><subject>baby food</subject><subject>Baby foods</subject><subject>Coffee</subject><subject>dimethylfuran</subject><subject>Food contamination</subject><subject>Food processing</subject><subject>Food Safety</subject><subject>Food, Processed</subject><subject>Fruit juices</subject><subject>furan</subject><subject>Furans</subject><subject>headspace-GC-MS</subject><subject>Humans</subject><subject>Infant</subject><subject>infant formula</subject><subject>methylfuran</subject><subject>Pesticides</subject><subject>Processed foods</subject><subject>Risk management</subject><subject>Safety management</subject><subject>Soy sauce</subject><issn>0015-6426</issn><issn>1882-1006</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNpdkE1r3DAQhkVpaZY0956KoJdevNWHJUvHZZttAykttD0LWRrVTmRrK9mF_fd1cLqBMIdhmGcemBeht5RsORfqY-nS_Qx96fqtrLdMv0AbqhSrKCHyJdoQQkUlayYv0FUpfUsI0Q3jjL1GF1wqsZTeIPMJ_kJMxwHGCYeU8dQB_tEPc5zsCGkueDfaeJp6ZyP-ClOXPE4BH-ZsR2xHj3fx_hTXueB-xN9zclAKeHxIyZc36FWwscDVY79Evw7XP_dfqttvn2_2u9vKUSV0BS1XDVDWatG0WpFgdaBBOc6CV41nWjthhdWcKSu0b2UTgqeqtqJ1UsuaX6IPq_eY058ZymSGvjiIcf3CsEZRyTihbEHfP0Pv0pyXLxdKMdFQWtMHIVkpl1MpGYI55n6w-WQoMQ_5m6f8jawN08vJu0fx3A7gzwf_016A_Qrclcn-hjNg85JvhGdGumrPW9fZbGDk_wB07pyv</recordid><startdate>2023</startdate><enddate>2023</enddate><creator>Ogiso, Motoki</creator><creator>Hashimoto, Chihiro</creator><creator>Toriumi, Eisuke</creator><creator>Nishimura, Kanako</creator><creator>Iizuka, Seiichiro</creator><creator>Sakamoto, Kazuhiro</creator><creator>Yamamoto, Yushi</creator><creator>Yamada, Yukiko</creator><general>Japanese Society for Food Hygiene and Safety</general><general>Japan Science and Technology Agency</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7T2</scope><scope>7T7</scope><scope>7U7</scope><scope>8FD</scope><scope>C1K</scope><scope>F1W</scope><scope>FR3</scope><scope>H95</scope><scope>H96</scope><scope>H97</scope><scope>H98</scope><scope>H99</scope><scope>L.F</scope><scope>L.G</scope><scope>P64</scope><scope>7X8</scope></search><sort><creationdate>2023</creationdate><title>Development for the Simultaneous Analytical Method of Furan and Alkyl Furans in Processed Foods</title><author>Ogiso, Motoki ; 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subjects | Analytical methods apple juice baby food Baby foods Coffee dimethylfuran Food contamination Food processing Food Safety Food, Processed Fruit juices furan Furans headspace-GC-MS Humans Infant infant formula methylfuran Pesticides Processed foods Risk management Safety management Soy sauce |
title | Development for the Simultaneous Analytical Method of Furan and Alkyl Furans in Processed Foods |
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