Centrifugal Casting of Thin-Walled Ceramic Tubes from Preceramic Polymers
Thin‐walled (wall thickness, 100–2000 μm) mono‐ and bilayered ceramic tubes in the system Si–O–C–(N) were obtained by centrifugal casting of a polysiloxane/filler suspension. Si and SiC powders were dispersed in polyorganosiloxane/triethoxysilane solutions. After centrifugal casting in a Teflon tube...
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Veröffentlicht in: | Journal of the American Ceramic Society 2003-07, Vol.86 (7), p.1211-1213 |
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creator | Melcher, Reinhold Cromme, Peter Scheffler, Michael Greil, Peter |
description | Thin‐walled (wall thickness, 100–2000 μm) mono‐ and bilayered ceramic tubes in the system Si–O–C–(N) were obtained by centrifugal casting of a polysiloxane/filler suspension. Si and SiC powders were dispersed in polyorganosiloxane/triethoxysilane solutions. After centrifugal casting in a Teflon tube with a rotational speed of 2000 rpm and subsequent cross‐linking at 130°C and 60 rpm, the tubes were pyrolyzed in argon or in nitrogen at 1400–1600°C. Bilayered tubes with controlled variation of porosity were obtained by overcasting the monolayer green tubes with a modified slurry composition. |
doi_str_mv | 10.1111/j.1151-2916.2003.tb03451.x |
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Si and SiC powders were dispersed in polyorganosiloxane/triethoxysilane solutions. After centrifugal casting in a Teflon tube with a rotational speed of 2000 rpm and subsequent cross‐linking at 130°C and 60 rpm, the tubes were pyrolyzed in argon or in nitrogen at 1400–1600°C. Bilayered tubes with controlled variation of porosity were obtained by overcasting the monolayer green tubes with a modified slurry composition.</description><identifier>ISSN: 0002-7820</identifier><identifier>EISSN: 1551-2916</identifier><identifier>DOI: 10.1111/j.1151-2916.2003.tb03451.x</identifier><identifier>CODEN: JACTAW</identifier><language>eng</language><publisher>Westerville, Ohio: American Ceramics Society</publisher><subject>Applied sciences ; Building materials. Ceramics. 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Si and SiC powders were dispersed in polyorganosiloxane/triethoxysilane solutions. After centrifugal casting in a Teflon tube with a rotational speed of 2000 rpm and subsequent cross‐linking at 130°C and 60 rpm, the tubes were pyrolyzed in argon or in nitrogen at 1400–1600°C. Bilayered tubes with controlled variation of porosity were obtained by overcasting the monolayer green tubes with a modified slurry composition.</description><subject>Applied sciences</subject><subject>Building materials. Ceramics. Glasses</subject><subject>Ceramic industries</subject><subject>Chemical industry and chemicals</subject><subject>Exact sciences and technology</subject><subject>layered ceramics</subject><subject>Miscellaneous</subject><subject>pores/porosity</subject><subject>rheology/rheometry</subject><subject>Technical ceramics</subject><issn>0002-7820</issn><issn>1551-2916</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2003</creationdate><recordtype>article</recordtype><recordid>eNqVkU1v1DAQhi0EEkvhP0SV4JbFn3XMiSpqS1dLWaGVerQc77h4cZJiJ2L33-NoIypxKr6M7HnmHc-8CJ0TvCT5fNznIEhJFblYUozZcmgw44IsDy_Qgog59RItMMa0lBXFr9GblPb5SlTFF-i2hm6I3o0PJhS1SYPvHoreFdsfvivvTQiwK2qIpvW22I4NpMLFvi02Eez8uunDsYWY3qJXzoQE7-Z4hr5fX23rL-X6281tfbkuLZf5P44JzIyRzHJuGqWUFAasa6jDioAB0UjpJMcNYAlKEdcIvGM7xmVlGDtDH06ij7H_NUIadOuThRBMB_2YNJVV3gcnzwKZ5DSD5_-A-36MXZ5AUyIV5YrIDH06QTb2KUVw-jH61sSjJlhPRui9nozQ07b1ZISejdCHXPx-7mCSNcFF01mfnhS4EpxRkbnPJ-63D3D8jw56dVlfEUqmqcuThE8DHP5KmPhTX0gmhb6_u9Gr1de7Cq_WesP-ANNGq1g</recordid><startdate>200307</startdate><enddate>200307</enddate><creator>Melcher, Reinhold</creator><creator>Cromme, Peter</creator><creator>Scheffler, Michael</creator><creator>Greil, Peter</creator><general>American Ceramics Society</general><general>Blackwell</general><general>Wiley Subscription Services, Inc</general><scope>BSCLL</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>200307</creationdate><title>Centrifugal Casting of Thin-Walled Ceramic Tubes from Preceramic Polymers</title><author>Melcher, Reinhold ; Cromme, Peter ; Scheffler, Michael ; Greil, Peter</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4751-f3503aa73c44ab99975aecfb2f091eae5b77f740be07e991fb50d3d3478a33</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2003</creationdate><topic>Applied sciences</topic><topic>Building materials. Ceramics. Glasses</topic><topic>Ceramic industries</topic><topic>Chemical industry and chemicals</topic><topic>Exact sciences and technology</topic><topic>layered ceramics</topic><topic>Miscellaneous</topic><topic>pores/porosity</topic><topic>rheology/rheometry</topic><topic>Technical ceramics</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Melcher, Reinhold</creatorcontrib><creatorcontrib>Cromme, Peter</creatorcontrib><creatorcontrib>Scheffler, Michael</creatorcontrib><creatorcontrib>Greil, Peter</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of the American Ceramic Society</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Melcher, Reinhold</au><au>Cromme, Peter</au><au>Scheffler, Michael</au><au>Greil, Peter</au><au>WCA</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Centrifugal Casting of Thin-Walled Ceramic Tubes from Preceramic Polymers</atitle><jtitle>Journal of the American Ceramic Society</jtitle><date>2003-07</date><risdate>2003</risdate><volume>86</volume><issue>7</issue><spage>1211</spage><epage>1213</epage><pages>1211-1213</pages><issn>0002-7820</issn><eissn>1551-2916</eissn><coden>JACTAW</coden><abstract>Thin‐walled (wall thickness, 100–2000 μm) mono‐ and bilayered ceramic tubes in the system Si–O–C–(N) were obtained by centrifugal casting of a polysiloxane/filler suspension. Si and SiC powders were dispersed in polyorganosiloxane/triethoxysilane solutions. After centrifugal casting in a Teflon tube with a rotational speed of 2000 rpm and subsequent cross‐linking at 130°C and 60 rpm, the tubes were pyrolyzed in argon or in nitrogen at 1400–1600°C. Bilayered tubes with controlled variation of porosity were obtained by overcasting the monolayer green tubes with a modified slurry composition.</abstract><cop>Westerville, Ohio</cop><pub>American Ceramics Society</pub><doi>10.1111/j.1151-2916.2003.tb03451.x</doi><tpages>3</tpages></addata></record> |
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source | Wiley Online Library Journals Frontfile Complete |
subjects | Applied sciences Building materials. Ceramics. Glasses Ceramic industries Chemical industry and chemicals Exact sciences and technology layered ceramics Miscellaneous pores/porosity rheology/rheometry Technical ceramics |
title | Centrifugal Casting of Thin-Walled Ceramic Tubes from Preceramic Polymers |
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