Synthesis of nanocrystalline NiCuZn ferrite powders by sol–gel auto-combustion method
A nitrate–citrate gel was prepared from metal nitrates and citric acid by sol–gel process, in order to synthesize Ni 0.25Cu 0.25Zn 0.50Fe 2O 4 ferrite. The thermal decomposition process was investigated by DTA-TG, IR and XRD techniques. The results revealed that the nitrate–citrate gel exhibits self...
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Veröffentlicht in: | Journal of magnetism and magnetic materials 2000, Vol.208 (1), p.55-60 |
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container_title | Journal of magnetism and magnetic materials |
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creator | Yue, Zhenxing Zhou, Ji Li, Longtu Zhang, Hongguo Gui, Zhilun |
description | A nitrate–citrate gel was prepared from metal nitrates and citric acid by sol–gel process, in order to synthesize Ni
0.25Cu
0.25Zn
0.50Fe
2O
4 ferrite. The thermal decomposition process was investigated by DTA-TG, IR and XRD techniques. The results revealed that the nitrate–citrate gel exhibits self-propagating combustion behavior. After combustion, the gel directly transformed into single-phase, nano-sized NiCuZn ferrite particles with spinel crystal structure. The synthesized powder can be densified at a temperature lower than 900°C. The sintered body possesses fine-grained microstructure, good frequency stability and high-quality factor compared to the sample prepared by conventional ceramic route. |
doi_str_mv | 10.1016/S0304-8853(99)00566-1 |
format | Article |
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0.25Cu
0.25Zn
0.50Fe
2O
4 ferrite. The thermal decomposition process was investigated by DTA-TG, IR and XRD techniques. The results revealed that the nitrate–citrate gel exhibits self-propagating combustion behavior. After combustion, the gel directly transformed into single-phase, nano-sized NiCuZn ferrite particles with spinel crystal structure. The synthesized powder can be densified at a temperature lower than 900°C. The sintered body possesses fine-grained microstructure, good frequency stability and high-quality factor compared to the sample prepared by conventional ceramic route.</description><identifier>ISSN: 0304-8853</identifier><identifier>DOI: 10.1016/S0304-8853(99)00566-1</identifier><identifier>CODEN: JMMMDC</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Auto-combustion ; Chemical synthesis; combustion synthesis ; Condensed matter: electronic structure, electrical, magnetic, and optical properties ; Cross-disciplinary physics: materials science; rheology ; Domain effects, magnetization curves, and hysteresis ; Exact sciences and technology ; Ferrites ; Magnetic properties ; Magnetic properties and materials ; Magnetization curves, hysteresis, Barkhausen and related effects ; Magnetization curves, magnetization reversal, hysteresis, barkhausen and related effects ; Materials science ; Materials synthesis; materials processing ; Nanocrystalline powder ; Nanoscale materials and structures: fabrication and characterization ; Physics ; Sol–gel technique</subject><ispartof>Journal of magnetism and magnetic materials, 2000, Vol.208 (1), p.55-60</ispartof><rights>2000 Elsevier Science B.V.</rights><rights>2000 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c433t-9fd04ff842f20c82cf6daf84fa2a38929bdfe1c75920c18ddd35213e43ade77b3</citedby><cites>FETCH-LOGICAL-c433t-9fd04ff842f20c82cf6daf84fa2a38929bdfe1c75920c18ddd35213e43ade77b3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/S0304-8853(99)00566-1$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>315,781,785,3551,4025,27928,27929,27930,46000</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=1208044$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Yue, Zhenxing</creatorcontrib><creatorcontrib>Zhou, Ji</creatorcontrib><creatorcontrib>Li, Longtu</creatorcontrib><creatorcontrib>Zhang, Hongguo</creatorcontrib><creatorcontrib>Gui, Zhilun</creatorcontrib><title>Synthesis of nanocrystalline NiCuZn ferrite powders by sol–gel auto-combustion method</title><title>Journal of magnetism and magnetic materials</title><description>A nitrate–citrate gel was prepared from metal nitrates and citric acid by sol–gel process, in order to synthesize Ni
0.25Cu
0.25Zn
0.50Fe
2O
4 ferrite. The thermal decomposition process was investigated by DTA-TG, IR and XRD techniques. The results revealed that the nitrate–citrate gel exhibits self-propagating combustion behavior. After combustion, the gel directly transformed into single-phase, nano-sized NiCuZn ferrite particles with spinel crystal structure. The synthesized powder can be densified at a temperature lower than 900°C. The sintered body possesses fine-grained microstructure, good frequency stability and high-quality factor compared to the sample prepared by conventional ceramic route.</description><subject>Auto-combustion</subject><subject>Chemical synthesis; combustion synthesis</subject><subject>Condensed matter: electronic structure, electrical, magnetic, and optical properties</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Domain effects, magnetization curves, and hysteresis</subject><subject>Exact sciences and technology</subject><subject>Ferrites</subject><subject>Magnetic properties</subject><subject>Magnetic properties and materials</subject><subject>Magnetization curves, hysteresis, Barkhausen and related effects</subject><subject>Magnetization curves, magnetization reversal, hysteresis, barkhausen and related effects</subject><subject>Materials science</subject><subject>Materials synthesis; materials processing</subject><subject>Nanocrystalline powder</subject><subject>Nanoscale materials and structures: fabrication and characterization</subject><subject>Physics</subject><subject>Sol–gel technique</subject><issn>0304-8853</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2000</creationdate><recordtype>article</recordtype><recordid>eNqFkMtKQzEQhs9CwXp5BCELEV0cTU7OdSVSvEHRRRXBTUiTiY2cJjWTo3TnO_iGPomnrejS1TAz_z8_8yXJPqMnjLLydEw5zdO6LvhR0xxTWpRlyjaSwe94K9lGfKGUsrwuB8njeOHiFNAi8YY46bwKC4yyba0DcmuH3ZMjBkKwEcjcv2sISCYLgr79-vh8hpbILvpU-dmkw2i9IzOIU693k00jW4S9n7qTPFxe3A-v09Hd1c3wfJSqnPOYNkbT3Jg6z0xGVZ0pU2rZt0ZmktdN1ky0AaaqounXrNZa8yJjHHIuNVTVhO8kh-u78-BfO8AoZhYVtK104DsUWVWVFS94LyzWQhU8YgAj5sHOZFgIRsUSnVihE0tGomnECp1gve_gJ0Cikq0J0imLf-aM1jTPe9nZWgb9s28WgkBlwSnQNoCKQnv7T9A34tCHsA</recordid><startdate>2000</startdate><enddate>2000</enddate><creator>Yue, Zhenxing</creator><creator>Zhou, Ji</creator><creator>Li, Longtu</creator><creator>Zhang, Hongguo</creator><creator>Gui, Zhilun</creator><general>Elsevier B.V</general><general>Elsevier Science</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SP</scope><scope>8FD</scope><scope>L7M</scope></search><sort><creationdate>2000</creationdate><title>Synthesis of nanocrystalline NiCuZn ferrite powders by sol–gel auto-combustion method</title><author>Yue, Zhenxing ; Zhou, Ji ; Li, Longtu ; Zhang, Hongguo ; Gui, Zhilun</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c433t-9fd04ff842f20c82cf6daf84fa2a38929bdfe1c75920c18ddd35213e43ade77b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2000</creationdate><topic>Auto-combustion</topic><topic>Chemical synthesis; combustion synthesis</topic><topic>Condensed matter: electronic structure, electrical, magnetic, and optical properties</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Domain effects, magnetization curves, and hysteresis</topic><topic>Exact sciences and technology</topic><topic>Ferrites</topic><topic>Magnetic properties</topic><topic>Magnetic properties and materials</topic><topic>Magnetization curves, hysteresis, Barkhausen and related effects</topic><topic>Magnetization curves, magnetization reversal, hysteresis, barkhausen and related effects</topic><topic>Materials science</topic><topic>Materials synthesis; materials processing</topic><topic>Nanocrystalline powder</topic><topic>Nanoscale materials and structures: fabrication and characterization</topic><topic>Physics</topic><topic>Sol–gel technique</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Yue, Zhenxing</creatorcontrib><creatorcontrib>Zhou, Ji</creatorcontrib><creatorcontrib>Li, Longtu</creatorcontrib><creatorcontrib>Zhang, Hongguo</creatorcontrib><creatorcontrib>Gui, Zhilun</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Electronics & Communications Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of magnetism and magnetic materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Yue, Zhenxing</au><au>Zhou, Ji</au><au>Li, Longtu</au><au>Zhang, Hongguo</au><au>Gui, Zhilun</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of nanocrystalline NiCuZn ferrite powders by sol–gel auto-combustion method</atitle><jtitle>Journal of magnetism and magnetic materials</jtitle><date>2000</date><risdate>2000</risdate><volume>208</volume><issue>1</issue><spage>55</spage><epage>60</epage><pages>55-60</pages><issn>0304-8853</issn><coden>JMMMDC</coden><abstract>A nitrate–citrate gel was prepared from metal nitrates and citric acid by sol–gel process, in order to synthesize Ni
0.25Cu
0.25Zn
0.50Fe
2O
4 ferrite. The thermal decomposition process was investigated by DTA-TG, IR and XRD techniques. The results revealed that the nitrate–citrate gel exhibits self-propagating combustion behavior. After combustion, the gel directly transformed into single-phase, nano-sized NiCuZn ferrite particles with spinel crystal structure. The synthesized powder can be densified at a temperature lower than 900°C. The sintered body possesses fine-grained microstructure, good frequency stability and high-quality factor compared to the sample prepared by conventional ceramic route.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/S0304-8853(99)00566-1</doi><tpages>6</tpages></addata></record> |
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source | Elsevier ScienceDirect Journals Complete |
subjects | Auto-combustion Chemical synthesis combustion synthesis Condensed matter: electronic structure, electrical, magnetic, and optical properties Cross-disciplinary physics: materials science rheology Domain effects, magnetization curves, and hysteresis Exact sciences and technology Ferrites Magnetic properties Magnetic properties and materials Magnetization curves, hysteresis, Barkhausen and related effects Magnetization curves, magnetization reversal, hysteresis, barkhausen and related effects Materials science Materials synthesis materials processing Nanocrystalline powder Nanoscale materials and structures: fabrication and characterization Physics Sol–gel technique |
title | Synthesis of nanocrystalline NiCuZn ferrite powders by sol–gel auto-combustion method |
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