Synthesis and deposition of ZnO based particles by aerosol spray pyrolysis

Synthesis and deposition of ZnO based particles by aerosol spray pyrolysis

Spray pyrolysis was used for the deposition of well defined submicronic to nanosize particles based on ZnO. The influence of the temperature in the range from 345 to 1165 K, solution concentration (0.004 and 1.5 mol dm −3) and the residence time on the particle morphology is discussed. X-ray diffrac...

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Veröffentlicht in:Thin solid films 1997, Vol.296 (1), p.44-48
Hauptverfasser: Milošević, Olivera, Gagić, Vladimir, Vodnik, Jože, Mitrović, Aleksandra, Karanović, Ljiljana, Stojanović, Biljana, ſivković, Ljiljana
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Aerosol spray pyrolysis
Deposition
Synthesis
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container_end_page 48
container_issue 1
container_start_page 44
container_title Thin solid films
container_volume 296
creator Milošević, Olivera
Gagić, Vladimir
Vodnik, Jože
Mitrović, Aleksandra
Karanović, Ljiljana
Stojanović, Biljana
ſivković, Ljiljana
description Spray pyrolysis was used for the deposition of well defined submicronic to nanosize particles based on ZnO. The influence of the temperature in the range from 345 to 1165 K, solution concentration (0.004 and 1.5 mol dm −3) and the residence time on the particle morphology is discussed. X-ray diffraction, differential scanning calorimetry and scanning electron microscopy were used in particle characterization. With the presumption that certain particle morphology is formed during the evaporation/drying stage of spray pyrolysis, the corresponding mathematical model for droplets evaporation is developed and correlated with the empirical results.
doi_str_mv 10.1016/S0040-6090(96)09358-3
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subjects Aerosol spray pyrolysis
Deposition
Synthesis
title Synthesis and deposition of ZnO based particles by aerosol spray pyrolysis
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