Oxygen Content and Structures of La1−xCaxMnO3+d as a Function of Synthesis Conditions
Using thermogravimetric analysis measurements, oxygen content was measured for La1−xCaxMnO3+d (0≤x≤0.38) samples prepared at high oxygen pressure. The oxygen content was found to decrease uniformly with increasing x for samples annealed at 12 and 140 atm O2 at 800°C, slowly cooled in 1, 20, and 100%...
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Veröffentlicht in: | Journal of solid state chemistry 1999-09, Vol.146 (2), p.448-457 |
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