Surface oxide debonding in field assisted powder sintering

Field activated sintering techniques (FAST) have been applied to two high-temperature powder materials: tungsten and NiAl. High and atomic resolution electron microscopy (HREM/ARM) of tungsten powder sintered via FAST showed essentially clean boundaries. Analytical transmission electron microscopy (...

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Veröffentlicht in:Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 1999-09, Vol.270 (2), p.278-282
Hauptverfasser: Anderson, K.R, Groza, J.R, Fendorf, M, Echer, C.J
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container_title Materials science & engineering. A, Structural materials : properties, microstructure and processing
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creator Anderson, K.R
Groza, J.R
Fendorf, M
Echer, C.J
description Field activated sintering techniques (FAST) have been applied to two high-temperature powder materials: tungsten and NiAl. High and atomic resolution electron microscopy (HREM/ARM) of tungsten powder sintered via FAST showed essentially clean boundaries. Analytical transmission electron microscopy (TEM) of FAST sintered NiAl also showed boundaries free of surface oxide layer(s). However, small alumina precipitates were found at and near prior particle (grain) boundaries. The boundary cleaning and precipitation phenomena are manifestations of an applied pulsed electric field.
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subjects Applied sciences
Clean grain boundaries
Cross-disciplinary physics: materials science
rheology
Exact sciences and technology
Field activation
HREM
Materials science
Materials synthesis
materials processing
Metals. Metallurgy
Phase diagrams and microstructures developed by solidification and solid-solid phase transformations
Physics
Powder processing: powder metallurgy, compaction, sintering, mechanical alloying, and granulation
Precipitation
Sintering
Solid-phase precipitation
title Surface oxide debonding in field assisted powder sintering
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