Preparation and Characterization of CuO Nanocrystals
Monoclinic CuO nanoparticles were prepared by using a one-step solid state reaction method under ambient conditions. The CuO particles with an average size of 12 nm were pressed into pellets under high pressure. They were studied by X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), tr...
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| Veröffentlicht in: | Journal of solid state chemistry 1999-11, Vol.147 (2), p.516-519 |
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| container_end_page | 519 |
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| container_issue | 2 |
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| container_title | Journal of solid state chemistry |
| container_volume | 147 |
| creator | Xu, J.F. Ji, W. Shen, Z.X. Tang, S.H. Ye, X.R. Jia, D.Z. Xin, X.Q. |
| description | Monoclinic CuO nanoparticles were prepared by using a one-step solid state reaction method under ambient conditions. The CuO particles with an average size of 12 nm were pressed into pellets under high pressure. They were studied by X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), transmission electron microscopy (TEM), and Raman spectroscopy. The CuO grains in pellets grow with time at room temperature. The gradual increase in the grain size with time is clearly reflected in their Raman spectra and the XRD results. The correlation between the Raman spectra and the crystal dimension is discussed. |
| doi_str_mv | 10.1006/jssc.1999.8409 |
| format | Article |
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| subjects | Clusters, nanoparticles, and nanocrystalline materials Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science rheology Exact sciences and technology Materials science Nanoscale materials and structures: fabrication and characterization Nanoscale materials: clusters, nanoparticles, nanotubes, and nanocrystals Physics Structure of solids and liquids crystallography |
| title | Preparation and Characterization of CuO Nanocrystals |
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