Haasen plot analysis of the Hall–Petch effect in Cu/Nb nanolayer composites

We investigate the effects of layer thickness (t) on hardness (H) and rate sensitivity of the hardness (∂H/∂ ln ) in 1 μm-thick Cu/Nb nanolayer composites. For t < 10 nm, we find that H correlates with t according to H = H0 = H1t-1/2, suggestive of a Hall–Petch mechanism with layer interfaces rep...

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Veröffentlicht in:Journal of Materials Research 1999-02, Vol.14 (2), p.407-417
Hauptverfasser: Tambwe, M. F., Stone, D. S., Griffin, A. J., Kung, H., Cheng, Y., Nastasi, M.
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container_end_page 417
container_issue 2
container_start_page 407
container_title Journal of Materials Research
container_volume 14
creator Tambwe, M. F.
Stone, D. S.
Griffin, A. J.
Kung, H.
Cheng, Y.
Nastasi, M.
description We investigate the effects of layer thickness (t) on hardness (H) and rate sensitivity of the hardness (∂H/∂ ln ) in 1 μm-thick Cu/Nb nanolayer composites. For t < 10 nm, we find that H correlates with t according to H = H0 = H1t-1/2, suggestive of a Hall–Petch mechanism with layer interfaces replacing grain boundaries as barriers against dislocation motion. The measured levels of ∂H/∂ ln clearly indicate the operation of bulk-like dislocation mechanisms consistent with a Hall–Petch mechanism. However, based on a Haasen-plot activation analysis, it appears that the Hall–Petch coefficient, H1, is strongly rate-dependent, inconsistent with a conventional Hall–Petch mechanism. For specimens with t < 10 nm there is a saturation in hardness, but the rate sensitivity data indicate no clear evidence of a corresponding change in mechanism. Simple models are proposed.
doi_str_mv 10.1557/JMR.1999.0059
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subjects COMPOSITE MATERIALS
COPPER
DEFORMATION
DISLOCATIONS
HARDENING
HARDNESS
MATERIALS SCIENCE
NIOBIUM
STRAIN HARDENING
STRAIN RATE
title Haasen plot analysis of the Hall–Petch effect in Cu/Nb nanolayer composites
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