Mechanochemical-hydrothermal preparation of crystalline hydroxyapatite powders at room temperature

Mechanochemical-hydrothermal preparation of crystalline hydroxyapatite powders at room temperature

Crystalline hydroxyapatite (HAp) powders were prepared at room temperature from heterogeneous reaction between Ca(OH)2powders and (NH4)2HPO4 solutions via the mechanochemical-hydrothermal route. X-ray diffraction, infrared spectroscopy, thermogravimetric characterization, and chemical analysis were...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Journal of materials research 2001-05, Vol.16 (5), p.1231-1234
Hauptverfasser: Shuk, Pavel, Suchanek, Wojciech L., Hao, Tian, Gulliver, Eric, Riman, Richard E., Senna, Mamoru, TenHuisen, Kevor S., Janas, Victor F.
Format: Artikel
Sprache:eng
Schlagworte:
Rapid Communications
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page 1234
container_issue 5
container_start_page 1231
container_title Journal of materials research
container_volume 16
creator Shuk, Pavel
Suchanek, Wojciech L.
Hao, Tian
Gulliver, Eric
Riman, Richard E.
Senna, Mamoru
TenHuisen, Kevor S.
Janas, Victor F.
description Crystalline hydroxyapatite (HAp) powders were prepared at room temperature from heterogeneous reaction between Ca(OH)2powders and (NH4)2HPO4 solutions via the mechanochemical-hydrothermal route. X-ray diffraction, infrared spectroscopy, thermogravimetric characterization, and chemical analysis were performed, and it was determined that the room temperature products were phase-pure, thermally stable HAp with a nearly stoichiometric composition. Dynamic light scattering revealed that the dispersed particle size distribution of the room temperature HAp powders was in the range of 0.15–3.0 μm with a specific surface area of ≈90 m2/g. Both specific surface area measurements and scanning electron microscopy confirmed that the HAp powders consisted of agglomerates containing hundreds of ≈20 nm HAp crystals.
doi_str_mv 10.1557/JMR.2001.0170
format Article
fullrecord <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_26791754</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><cupid>10_1557_JMR_2001_0170</cupid><sourcerecordid>26791754</sourcerecordid><originalsourceid>FETCH-LOGICAL-c441t-ea94827361040c0c6e4974337116f4413db3c25d10200ffd8e5cb753d76d23d23</originalsourceid><addsrcrecordid>eNqN0MtLwzAcwPEgCs7H0XtP3rolzas9ivjEKb7AW0jTX121bWqS4fbfm7mhJ0EI5JBPfiFfhI4IHhPO5eR6-jDOMCZjTCTeQqMMM5ZymoltNMJ5ztKsIGwX7Xn_FhXHko1QOQUz0701M-gao9t0tqycDTNwnW6TwcGgnQ6N7RNbJ8YtfdBt2_SQfLvFUg_xNEAy2M8KnE90SJy1XRKgGyDenDs4QDu1bj0cbvZ99Hx-9nR6md7cXVydntykhjESUtAFyzNJBcEMG2wEsEIySiUhoo6CViU1Ga8Ijn-s6yoHbkrJaSVFldG49tHxeu7g7MccfFBd4w20re7Bzr3KhCyI5Ow_MOdCrmC6hsZZ7x3UanBNp91SEaxWyVVMrlbJ1Sr5r298gMUP1u5dCUklV-LiXt0SRs5fHqeKRj_ZzNdd6ZrqFdSbnbs-VvrjhS9lZ5Nl</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>26785674</pqid></control><display><type>article</type><title>Mechanochemical-hydrothermal preparation of crystalline hydroxyapatite powders at room temperature</title><source>Springer Nature - Complete Springer Journals</source><creator>Shuk, Pavel ; Suchanek, Wojciech L. ; Hao, Tian ; Gulliver, Eric ; Riman, Richard E. ; Senna, Mamoru ; TenHuisen, Kevor S. ; Janas, Victor F.</creator><contributor>WCA</contributor><creatorcontrib>Shuk, Pavel ; Suchanek, Wojciech L. ; Hao, Tian ; Gulliver, Eric ; Riman, Richard E. ; Senna, Mamoru ; TenHuisen, Kevor S. ; Janas, Victor F. ; WCA</creatorcontrib><description>Crystalline hydroxyapatite (HAp) powders were prepared at room temperature from heterogeneous reaction between Ca(OH)2powders and (NH4)2HPO4 solutions via the mechanochemical-hydrothermal route. X-ray diffraction, infrared spectroscopy, thermogravimetric characterization, and chemical analysis were performed, and it was determined that the room temperature products were phase-pure, thermally stable HAp with a nearly stoichiometric composition. Dynamic light scattering revealed that the dispersed particle size distribution of the room temperature HAp powders was in the range of 0.15–3.0 μm with a specific surface area of ≈90 m2/g. Both specific surface area measurements and scanning electron microscopy confirmed that the HAp powders consisted of agglomerates containing hundreds of ≈20 nm HAp crystals.</description><identifier>ISSN: 0884-2914</identifier><identifier>EISSN: 2044-5326</identifier><identifier>DOI: 10.1557/JMR.2001.0170</identifier><language>eng</language><publisher>New York, USA: Cambridge University Press</publisher><subject>Rapid Communications</subject><ispartof>Journal of materials research, 2001-05, Vol.16 (5), p.1231-1234</ispartof><rights>Copyright © Materials Research Society 2001</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c441t-ea94827361040c0c6e4974337116f4413db3c25d10200ffd8e5cb753d76d23d23</citedby><cites>FETCH-LOGICAL-c441t-ea94827361040c0c6e4974337116f4413db3c25d10200ffd8e5cb753d76d23d23</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27901,27902</link.rule.ids></links><search><contributor>WCA</contributor><creatorcontrib>Shuk, Pavel</creatorcontrib><creatorcontrib>Suchanek, Wojciech L.</creatorcontrib><creatorcontrib>Hao, Tian</creatorcontrib><creatorcontrib>Gulliver, Eric</creatorcontrib><creatorcontrib>Riman, Richard E.</creatorcontrib><creatorcontrib>Senna, Mamoru</creatorcontrib><creatorcontrib>TenHuisen, Kevor S.</creatorcontrib><creatorcontrib>Janas, Victor F.</creatorcontrib><title>Mechanochemical-hydrothermal preparation of crystalline hydroxyapatite powders at room temperature</title><title>Journal of materials research</title><addtitle>J. Mater. Res</addtitle><description>Crystalline hydroxyapatite (HAp) powders were prepared at room temperature from heterogeneous reaction between Ca(OH)2powders and (NH4)2HPO4 solutions via the mechanochemical-hydrothermal route. X-ray diffraction, infrared spectroscopy, thermogravimetric characterization, and chemical analysis were performed, and it was determined that the room temperature products were phase-pure, thermally stable HAp with a nearly stoichiometric composition. Dynamic light scattering revealed that the dispersed particle size distribution of the room temperature HAp powders was in the range of 0.15–3.0 μm with a specific surface area of ≈90 m2/g. Both specific surface area measurements and scanning electron microscopy confirmed that the HAp powders consisted of agglomerates containing hundreds of ≈20 nm HAp crystals.</description><subject>Rapid Communications</subject><issn>0884-2914</issn><issn>2044-5326</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2001</creationdate><recordtype>article</recordtype><recordid>eNqN0MtLwzAcwPEgCs7H0XtP3rolzas9ivjEKb7AW0jTX121bWqS4fbfm7mhJ0EI5JBPfiFfhI4IHhPO5eR6-jDOMCZjTCTeQqMMM5ZymoltNMJ5ztKsIGwX7Xn_FhXHko1QOQUz0701M-gao9t0tqycDTNwnW6TwcGgnQ6N7RNbJ8YtfdBt2_SQfLvFUg_xNEAy2M8KnE90SJy1XRKgGyDenDs4QDu1bj0cbvZ99Hx-9nR6md7cXVydntykhjESUtAFyzNJBcEMG2wEsEIySiUhoo6CViU1Ga8Ijn-s6yoHbkrJaSVFldG49tHxeu7g7MccfFBd4w20re7Bzr3KhCyI5Ow_MOdCrmC6hsZZ7x3UanBNp91SEaxWyVVMrlbJ1Sr5r298gMUP1u5dCUklV-LiXt0SRs5fHqeKRj_ZzNdd6ZrqFdSbnbs-VvrjhS9lZ5Nl</recordid><startdate>20010501</startdate><enddate>20010501</enddate><creator>Shuk, Pavel</creator><creator>Suchanek, Wojciech L.</creator><creator>Hao, Tian</creator><creator>Gulliver, Eric</creator><creator>Riman, Richard E.</creator><creator>Senna, Mamoru</creator><creator>TenHuisen, Kevor S.</creator><creator>Janas, Victor F.</creator><general>Cambridge University Press</general><scope>BSCLL</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope><scope>7QQ</scope></search><sort><creationdate>20010501</creationdate><title>Mechanochemical-hydrothermal preparation of crystalline hydroxyapatite powders at room temperature</title><author>Shuk, Pavel ; Suchanek, Wojciech L. ; Hao, Tian ; Gulliver, Eric ; Riman, Richard E. ; Senna, Mamoru ; TenHuisen, Kevor S. ; Janas, Victor F.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c441t-ea94827361040c0c6e4974337116f4413db3c25d10200ffd8e5cb753d76d23d23</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2001</creationdate><topic>Rapid Communications</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Shuk, Pavel</creatorcontrib><creatorcontrib>Suchanek, Wojciech L.</creatorcontrib><creatorcontrib>Hao, Tian</creatorcontrib><creatorcontrib>Gulliver, Eric</creatorcontrib><creatorcontrib>Riman, Richard E.</creatorcontrib><creatorcontrib>Senna, Mamoru</creatorcontrib><creatorcontrib>TenHuisen, Kevor S.</creatorcontrib><creatorcontrib>Janas, Victor F.</creatorcontrib><collection>Istex</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Ceramic Abstracts</collection><jtitle>Journal of materials research</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Shuk, Pavel</au><au>Suchanek, Wojciech L.</au><au>Hao, Tian</au><au>Gulliver, Eric</au><au>Riman, Richard E.</au><au>Senna, Mamoru</au><au>TenHuisen, Kevor S.</au><au>Janas, Victor F.</au><au>WCA</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Mechanochemical-hydrothermal preparation of crystalline hydroxyapatite powders at room temperature</atitle><jtitle>Journal of materials research</jtitle><addtitle>J. Mater. Res</addtitle><date>2001-05-01</date><risdate>2001</risdate><volume>16</volume><issue>5</issue><spage>1231</spage><epage>1234</epage><pages>1231-1234</pages><issn>0884-2914</issn><eissn>2044-5326</eissn><abstract>Crystalline hydroxyapatite (HAp) powders were prepared at room temperature from heterogeneous reaction between Ca(OH)2powders and (NH4)2HPO4 solutions via the mechanochemical-hydrothermal route. X-ray diffraction, infrared spectroscopy, thermogravimetric characterization, and chemical analysis were performed, and it was determined that the room temperature products were phase-pure, thermally stable HAp with a nearly stoichiometric composition. Dynamic light scattering revealed that the dispersed particle size distribution of the room temperature HAp powders was in the range of 0.15–3.0 μm with a specific surface area of ≈90 m2/g. Both specific surface area measurements and scanning electron microscopy confirmed that the HAp powders consisted of agglomerates containing hundreds of ≈20 nm HAp crystals.</abstract><cop>New York, USA</cop><pub>Cambridge University Press</pub><doi>10.1557/JMR.2001.0170</doi><tpages>4</tpages></addata></record>
fulltext fulltext
identifier ISSN: 0884-2914
ispartof Journal of materials research, 2001-05, Vol.16 (5), p.1231-1234
issn 0884-2914
2044-5326
language eng
recordid cdi_proquest_miscellaneous_26791754
source Springer Nature - Complete Springer Journals
subjects Rapid Communications
title Mechanochemical-hydrothermal preparation of crystalline hydroxyapatite powders at room temperature
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-02-10T16%3A46%3A41IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Mechanochemical-hydrothermal%20preparation%20of%20crystalline%20hydroxyapatite%20powders%20at%20room%20temperature&rft.jtitle=Journal%20of%20materials%20research&rft.au=Shuk,%20Pavel&rft.date=2001-05-01&rft.volume=16&rft.issue=5&rft.spage=1231&rft.epage=1234&rft.pages=1231-1234&rft.issn=0884-2914&rft.eissn=2044-5326&rft_id=info:doi/10.1557/JMR.2001.0170&rft_dat=%3Cproquest_cross%3E26791754%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=26785674&rft_id=info:pmid/&rft_cupid=10_1557_JMR_2001_0170&rfr_iscdi=true