Nanomaterial Deposits Formed by DC Plasma Spraying of Liquid Feedstocks

An experimental system consisting of an axial feed plasma gun, a variable‐rate liquid delivery system, a liquid atomizer‐feeder, and a substrate movement and control system was designed and assembled for preparing nanograined ceramic deposits. Sprayed deposits were produced with different spray and...

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Veröffentlicht in:Journal of the American Ceramic Society 1998-01, Vol.81 (1), p.121-128
Hauptverfasser: Karthikeyan, Jeganathan, Berndt, Christopher C., Reddy, Sri, Wang, Jenn-Yue, King, Alexander H., Herman, Herbert
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container_end_page 128
container_issue 1
container_start_page 121
container_title Journal of the American Ceramic Society
container_volume 81
creator Karthikeyan, Jeganathan
Berndt, Christopher C.
Reddy, Sri
Wang, Jenn-Yue
King, Alexander H.
Herman, Herbert
description An experimental system consisting of an axial feed plasma gun, a variable‐rate liquid delivery system, a liquid atomizer‐feeder, and a substrate movement and control system was designed and assembled for preparing nanograined ceramic deposits. Sprayed deposits were produced with different spray and sol feed parameters and investigated in both the as‐sprayed and heat‐treated conditions. As‐sprayed deposits were predominately hydroxide phases and were strongly adherent to the substrates. Postspray heat treatment at 873 K led to conversion of the alumina and zirconia deposits to γ‐alumina and tetragonal zirconia phases, respectively. Subsequent heat treatment at 1273 K resulted in densification of the deposits and formation of high‐temperature phases. A small increase in the grain size was observed with heat treatment, but the specimens still retained nanosized grains.
doi_str_mv 10.1111/j.1151-2916.1998.tb02303.x
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subjects Cross-disciplinary physics: materials science
rheology
Exact sciences and technology
Materials science
Methods of deposition of films and coatings
film growth and epitaxy
Physics
Spray coating techniques
title Nanomaterial Deposits Formed by DC Plasma Spraying of Liquid Feedstocks
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