Combustion characteristics of WO3/Zn reaction system in SHS process

Tungsten powder was prepared by the Self-Propagating High-Temperature Synthesis (SHS) Process of WO3-Zn mixture. Zn vapor was discovered to affect significantly the combustion parameters such as combustion temperature (Tc), combustion velocity (U), relative mass change (Δm) and relative elongation (...

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Veröffentlicht in:Journal of materials science 2001-11, Vol.36 (22), p.5311-5314
Hauptverfasser: Lee, J H, Seo, D H, Won, C W, Borovinskaya, I P, Vershinnikov, V I
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container_end_page 5314
container_issue 22
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container_title Journal of materials science
container_volume 36
creator Lee, J H
Seo, D H
Won, C W
Borovinskaya, I P
Vershinnikov, V I
description Tungsten powder was prepared by the Self-Propagating High-Temperature Synthesis (SHS) Process of WO3-Zn mixture. Zn vapor was discovered to affect significantly the combustion parameters such as combustion temperature (Tc), combustion velocity (U), relative mass change (Δm) and relative elongation (Δh) of the sample. These effects could be reduced by decreasing internal Ar pressure and sample density. The ZnO in the product was leached with an HCl solution. The Zinc-thermal reduction mechanism was revealed through a quenching of the sample.
doi_str_mv 10.1023/A:1012426808855
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subjects Combustion temperature
Elongation
High temperature
Materials science
Self propagating high temperature synthesis
Thermal reduction
Tungsten oxides
Zinc oxide
title Combustion characteristics of WO3/Zn reaction system in SHS process
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