Determination of manganese by electrothermal atomisation atomic absorption spectrometry following coprecipitation with yttrium hydroxide
Coprecipitation is applied to the determination of trace amounts of manganese by electrothermal atomisation atomic absorption spectrometry. Manganese (0.05–1μg) is coprecipitated quantitatively from the sample solution (50–500 ml) with yttrium hydroxide at pH 9.0–11.3. The atomic absorbance of manga...
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Veröffentlicht in: | Analytica chimica acta 1994-12, Vol.298 (3), p.375-379 |
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creator | Takeda, Kikuo Akamatsu, Chikashi Ishikawa, Yoshihiro |
description | Coprecipitation is applied to the determination of trace amounts of manganese by electrothermal atomisation atomic absorption spectrometry. Manganese (0.05–1μg) is coprecipitated quantitatively from the sample solution (50–500 ml) with yttrium hydroxide at pH 9.0–11.3. The atomic absorbance of manganese is increased about 3 times by using an yttrium-impregnated graphite cuvette. The calibration curve is linear from 0.002 to 0.04 μg ml
−1 of manganese. Twenty-three different ions investigated did not produce serious interferences. The proposed method was successfully applied to the determination of trace amounts of manganese in zinc metal. |
doi_str_mv | 10.1016/0003-2670(94)00296-7 |
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−1 of manganese. Twenty-three different ions investigated did not produce serious interferences. The proposed method was successfully applied to the determination of trace amounts of manganese in zinc metal.</description><subject>Analytical chemistry</subject><subject>Applied sciences</subject><subject>Atomic absorption spectrometry</subject><subject>Chemistry</subject><subject>Coprecipitation</subject><subject>Electrothermal AAS</subject><subject>Exact sciences and technology</subject><subject>Manganese</subject><subject>Metals. Metallurgy</subject><subject>Spectrometric and optical methods</subject><issn>0003-2670</issn><issn>1873-4324</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1994</creationdate><recordtype>article</recordtype><recordid>eNp9kMtOhDAUhhujiePoG7jowhhdoAfaobAxMeM1MXGj66aUw0wNUGw7Km_gYwuDcemql3z_af-PkOMYLmKI00sAYFGSCjjL-TlAkqeR2CGzOBMs4izhu2T2h-yTA-_fhmMSA5-R7xsM6BrTqmBsS21FG9WuVIseadFTrFEHZ8N6YFRNVbCN8RO63WuqCm9dt73x3RZuMLieVrau7adpV1TbzqE2nQlT8NOENe1DcGbT0HVfOvtlSjwke5WqPR79rnPyenf7snyInp7vH5fXT5FORB4inRd6kYFQVYkKIM1YBZkoCsFjlvIsWzAOSue8SPIir4BrBSLJSsE5K9J4IdicnE5zO2ffN-iDHBpprOuhs914maQcBMtGkE-gdtZ7h5XsnGmU62UMctQuR6dydCpzLrfa5Rg7-Z2vvFZ15VSrjf_LsuF_YsEH7GrCcOj6YdBJrw22GkszyAqytOb_d34A7tGaUg</recordid><startdate>19941210</startdate><enddate>19941210</enddate><creator>Takeda, Kikuo</creator><creator>Akamatsu, Chikashi</creator><creator>Ishikawa, Yoshihiro</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>19941210</creationdate><title>Determination of manganese by electrothermal atomisation atomic absorption spectrometry following coprecipitation with yttrium hydroxide</title><author>Takeda, Kikuo ; Akamatsu, Chikashi ; Ishikawa, Yoshihiro</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c279t-c9bc5807afdea00683f087bb741364885340ac94b29b9f04ca0728d7443b61573</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1994</creationdate><topic>Analytical chemistry</topic><topic>Applied sciences</topic><topic>Atomic absorption spectrometry</topic><topic>Chemistry</topic><topic>Coprecipitation</topic><topic>Electrothermal AAS</topic><topic>Exact sciences and technology</topic><topic>Manganese</topic><topic>Metals. Metallurgy</topic><topic>Spectrometric and optical methods</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Takeda, Kikuo</creatorcontrib><creatorcontrib>Akamatsu, Chikashi</creatorcontrib><creatorcontrib>Ishikawa, Yoshihiro</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Analytica chimica acta</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Takeda, Kikuo</au><au>Akamatsu, Chikashi</au><au>Ishikawa, Yoshihiro</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Determination of manganese by electrothermal atomisation atomic absorption spectrometry following coprecipitation with yttrium hydroxide</atitle><jtitle>Analytica chimica acta</jtitle><date>1994-12-10</date><risdate>1994</risdate><volume>298</volume><issue>3</issue><spage>375</spage><epage>379</epage><pages>375-379</pages><issn>0003-2670</issn><eissn>1873-4324</eissn><coden>ACACAM</coden><abstract>Coprecipitation is applied to the determination of trace amounts of manganese by electrothermal atomisation atomic absorption spectrometry. Manganese (0.05–1μg) is coprecipitated quantitatively from the sample solution (50–500 ml) with yttrium hydroxide at pH 9.0–11.3. The atomic absorbance of manganese is increased about 3 times by using an yttrium-impregnated graphite cuvette. The calibration curve is linear from 0.002 to 0.04 μg ml
−1 of manganese. Twenty-three different ions investigated did not produce serious interferences. The proposed method was successfully applied to the determination of trace amounts of manganese in zinc metal.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/0003-2670(94)00296-7</doi><tpages>5</tpages></addata></record> |
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source | ScienceDirect Journals (5 years ago - present) |
subjects | Analytical chemistry Applied sciences Atomic absorption spectrometry Chemistry Coprecipitation Electrothermal AAS Exact sciences and technology Manganese Metals. Metallurgy Spectrometric and optical methods |
title | Determination of manganese by electrothermal atomisation atomic absorption spectrometry following coprecipitation with yttrium hydroxide |
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