Real-time monitoring and control during MOVPE growth of CdTe using multiwavelength ellipsometry

New multi-wavelength in-situ ellipsometer hardware and data analysis software are described. The hardware can simultaneously acquire accurate ellipsometric data at 12 wavelengths in less than 1 s, is simple and compact and is well suited for in-situ monitoring. The data analysis software implements...

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Veröffentlicht in:Thin solid films 1993-01, Vol.233 (1), p.293-296
Hauptverfasser: Johs, Blaine, Doerr, Dave, Pittal, Shakil, Bhat, I.B., Dakshinamurthy, S.
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container_end_page 296
container_issue 1
container_start_page 293
container_title Thin solid films
container_volume 233
creator Johs, Blaine
Doerr, Dave
Pittal, Shakil
Bhat, I.B.
Dakshinamurthy, S.
description New multi-wavelength in-situ ellipsometer hardware and data analysis software are described. The hardware can simultaneously acquire accurate ellipsometric data at 12 wavelengths in less than 1 s, is simple and compact and is well suited for in-situ monitoring. The data analysis software implements a “virtual interface” approach to determine in real time the characteristics (growth rate and composition) of the near-surface region of the film. These new tools were used to study the metal-organic vapor phase epitaxy (MOVPE) growth of CdTe on GaAs. From a post-deposition analysis of the in-situ data, dielectric constants of CdTe at growth temperature were obtained. Non-uniformity in the CdTe film thickness, and film nucleation during the initial stages of growth, were also observed in the post-deposition analysis. The determined CdTe dielectric constants were utilized in subsequent depositions to determine the growth rate of a CdTe film in real time. Feedback control of the CdTe growth rate was effected by connecting an analog control voltage line from the data acquisition/analysis computer to the Cd mass flow controller.
doi_str_mv 10.1016/0040-6090(93)90111-2
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subjects Condensed matter: structure, mechanical and thermal properties
Exact sciences and technology
Physics
Solid surfaces and solid-solid interfaces
Surface and interface dynamics and vibrations
Surfaces and interfaces
thin films and whiskers (structure and nonelectronic properties)
Thin film structure and morphology
title Real-time monitoring and control during MOVPE growth of CdTe using multiwavelength ellipsometry
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