Synthesis and Configuration of O‑Acetyl Microgrewiapine A: Phantomization of O‑Acetyl 6-epi-Microgrewiapine A

The formation of O-acetyl microgrewiapine A is investigated. NMR data for the authentic sample derived from the natural product are corrected. Wholly synthetic samples, produced from reductive N-methylation of synthetic microcosamine A (to give synthetic microgrewiapine A) followed by O-acetylation,...

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Veröffentlicht in:	Journal of natural products (Washington, D.C.) D.C.), 2022-01, Vol.85 (1), p.306-312
Hauptverfasser:	Davies, Stephen G, Fletcher, Ai M, Roberts, Paul M, Taylor, Cameron E, Thomson, James E
Format:	Artikel
Sprache:	eng
Schlagworte:	Acetylation Alkaloids - chemical synthesis Alkaloids - chemistry Biological Products - chemistry Carbon-13 Magnetic Resonance Spectroscopy Methylation Molecular Structure Piperidines - chemical synthesis Piperidines - chemistry Proton Magnetic Resonance Spectroscopy
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