Double crucible method for the growth of large superconducting YBCO single crystals

In this paper we report an effective procedure for the growth of large superconducting YBCO single crystals by using a double crucible method which facilitates detachment of the as-grown crystals from flux. As-grown crystals with dimensions up to 5 × 5 mm 2 have been obtained. The Superconducting tr...

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Veröffentlicht in:Journal of crystal growth 1990-11, Vol.106 (2), p.483-486
Hauptverfasser: Wang, Yaoshui, Bennema, P., van der Linden, P.
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creator Wang, Yaoshui
Bennema, P.
van der Linden, P.
description In this paper we report an effective procedure for the growth of large superconducting YBCO single crystals by using a double crucible method which facilitates detachment of the as-grown crystals from flux. As-grown crystals with dimensions up to 5 × 5 mm 2 have been obtained. The Superconducting transition occurs at about 90 K. The growth principle is based on the melt growth and phase separation method. We find that by using BaO 2 instead of BaCO 3 as raw material, the quality of as-grown crystals was much better and the superconducting transition temperature was a few degrees higher than in case of using BaCO 3.
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subjects Cross-disciplinary physics: materials science
rheology
Exact sciences and technology
Materials science
Methods of crystal growth
physics of crystal growth
Physics
title Double crucible method for the growth of large superconducting YBCO single crystals
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