Small-angle neutron scattering from fatigued copper single crystals

Copper single crystals oriented for single and multiple slip were studied by small-angle neutron scattering (SANS) after fatigue tests at a constant plastic shear strain amplitude y γ pl = 0.15% . For the SANS measurements, a special sample holder was used in order to obtain more reliable informatio...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 1991-01, Vol.131 (2), p.171-176
Hauptverfasser: Lepistö, T.K., Kostorz, G., Kuokkala, V.-T., Kettunen, P.
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page 176
container_issue 2
container_start_page 171
container_title Materials science & engineering. A, Structural materials : properties, microstructure and processing
container_volume 131
creator Lepistö, T.K.
Kostorz, G.
Kuokkala, V.-T.
Kettunen, P.
description Copper single crystals oriented for single and multiple slip were studied by small-angle neutron scattering (SANS) after fatigue tests at a constant plastic shear strain amplitude y γ pl = 0.15% . For the SANS measurements, a special sample holder was used in order to obtain more reliable information about the small differences in the neutron scattering from individual samples. The size of the voids in the samples oriented for single slip increased as a function of the number of fatigue cycles, varying from 0.74 nm to 0.91 nm, but the volume fraction remained more or less constant. The dislocation density observed by SANS was found to increase from 6 × 10 7 mm −2 at τ max/2 to 4 × 10 8 mm −2 at τ max, but remained constant in the saturation stage of cyclic strain hardening. The SANS results obtained are in good agreement with positron annihilation data and transmission electron microscopy observations from the same specimens.
doi_str_mv 10.1016/0921-5093(91)90393-2
format Article
fullrecord <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_25439705</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>0921509391903932</els_id><sourcerecordid>25439705</sourcerecordid><originalsourceid>FETCH-LOGICAL-c365t-162a5a1fc7a2ca8380dbc2fd043676b4ad0a8ca764a69f96adfe6648a9ea2bbf3</originalsourceid><addsrcrecordid>eNp9kEtLxDAUhYMoOI7-AxfdKLqoJk2aNhtBBl8w4EJdh9v0Zoj0ZZIK8-_tPNCdq7P5zrncj5BzRm8YZfKWqoylOVX8SrFrRbniaXZAZqwseCoUl4dk9osck5MQPimlTNB8RhZvLTRNCt2qwaTDMfq-S4KBGNG7bpVY37eJhehWI9aJ6YcBfRLcFjd-HSI04ZQc2SnwbJ9z8vH48L54TpevTy-L-2VquMxjymQGOTBrCsgMlLykdWUyW1PBZSErATWF0kAhBUhllYTaopSiBIWQVZXlc3K52x18_zViiLp1wWDTQIf9GHSWC64Kmk-g2IHG9yF4tHrwrgW_1ozqjTG90aE3OrRiemtMZ1PtYr8Pk4HGeuiMC39dJQpWCjpxdzsOp2e_HXodjMPOYO08mqjr3v1_6AekTYCG</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>25439705</pqid></control><display><type>article</type><title>Small-angle neutron scattering from fatigued copper single crystals</title><source>Elsevier ScienceDirect Journals</source><creator>Lepistö, T.K. ; Kostorz, G. ; Kuokkala, V.-T. ; Kettunen, P.</creator><creatorcontrib>Lepistö, T.K. ; Kostorz, G. ; Kuokkala, V.-T. ; Kettunen, P.</creatorcontrib><description>Copper single crystals oriented for single and multiple slip were studied by small-angle neutron scattering (SANS) after fatigue tests at a constant plastic shear strain amplitude y γ pl = 0.15% . For the SANS measurements, a special sample holder was used in order to obtain more reliable information about the small differences in the neutron scattering from individual samples. The size of the voids in the samples oriented for single slip increased as a function of the number of fatigue cycles, varying from 0.74 nm to 0.91 nm, but the volume fraction remained more or less constant. The dislocation density observed by SANS was found to increase from 6 × 10 7 mm −2 at τ max/2 to 4 × 10 8 mm −2 at τ max, but remained constant in the saturation stage of cyclic strain hardening. The SANS results obtained are in good agreement with positron annihilation data and transmission electron microscopy observations from the same specimens.</description><identifier>ISSN: 0921-5093</identifier><identifier>EISSN: 1873-4936</identifier><identifier>DOI: 10.1016/0921-5093(91)90393-2</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Applied sciences ; Condensed matter: structure, mechanical and thermal properties ; Exact sciences and technology ; Fatigue, brittleness, fracture, and cracks ; Mechanical and acoustical properties of condensed matter ; Mechanical properties of solids ; Metals. Metallurgy ; Physics</subject><ispartof>Materials science &amp; engineering. A, Structural materials : properties, microstructure and processing, 1991-01, Vol.131 (2), p.171-176</ispartof><rights>1991</rights><rights>1991 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c365t-162a5a1fc7a2ca8380dbc2fd043676b4ad0a8ca764a69f96adfe6648a9ea2bbf3</citedby><cites>FETCH-LOGICAL-c365t-162a5a1fc7a2ca8380dbc2fd043676b4ad0a8ca764a69f96adfe6648a9ea2bbf3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/0921509391903932$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65306</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&amp;idt=19471840$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Lepistö, T.K.</creatorcontrib><creatorcontrib>Kostorz, G.</creatorcontrib><creatorcontrib>Kuokkala, V.-T.</creatorcontrib><creatorcontrib>Kettunen, P.</creatorcontrib><title>Small-angle neutron scattering from fatigued copper single crystals</title><title>Materials science &amp; engineering. A, Structural materials : properties, microstructure and processing</title><description>Copper single crystals oriented for single and multiple slip were studied by small-angle neutron scattering (SANS) after fatigue tests at a constant plastic shear strain amplitude y γ pl = 0.15% . For the SANS measurements, a special sample holder was used in order to obtain more reliable information about the small differences in the neutron scattering from individual samples. The size of the voids in the samples oriented for single slip increased as a function of the number of fatigue cycles, varying from 0.74 nm to 0.91 nm, but the volume fraction remained more or less constant. The dislocation density observed by SANS was found to increase from 6 × 10 7 mm −2 at τ max/2 to 4 × 10 8 mm −2 at τ max, but remained constant in the saturation stage of cyclic strain hardening. The SANS results obtained are in good agreement with positron annihilation data and transmission electron microscopy observations from the same specimens.</description><subject>Applied sciences</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Exact sciences and technology</subject><subject>Fatigue, brittleness, fracture, and cracks</subject><subject>Mechanical and acoustical properties of condensed matter</subject><subject>Mechanical properties of solids</subject><subject>Metals. Metallurgy</subject><subject>Physics</subject><issn>0921-5093</issn><issn>1873-4936</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1991</creationdate><recordtype>article</recordtype><recordid>eNp9kEtLxDAUhYMoOI7-AxfdKLqoJk2aNhtBBl8w4EJdh9v0Zoj0ZZIK8-_tPNCdq7P5zrncj5BzRm8YZfKWqoylOVX8SrFrRbniaXZAZqwseCoUl4dk9osck5MQPimlTNB8RhZvLTRNCt2qwaTDMfq-S4KBGNG7bpVY37eJhehWI9aJ6YcBfRLcFjd-HSI04ZQc2SnwbJ9z8vH48L54TpevTy-L-2VquMxjymQGOTBrCsgMlLykdWUyW1PBZSErATWF0kAhBUhllYTaopSiBIWQVZXlc3K52x18_zViiLp1wWDTQIf9GHSWC64Kmk-g2IHG9yF4tHrwrgW_1ozqjTG90aE3OrRiemtMZ1PtYr8Pk4HGeuiMC39dJQpWCjpxdzsOp2e_HXodjMPOYO08mqjr3v1_6AekTYCG</recordid><startdate>19910120</startdate><enddate>19910120</enddate><creator>Lepistö, T.K.</creator><creator>Kostorz, G.</creator><creator>Kuokkala, V.-T.</creator><creator>Kettunen, P.</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>8BQ</scope><scope>8FD</scope><scope>H8G</scope><scope>JG9</scope></search><sort><creationdate>19910120</creationdate><title>Small-angle neutron scattering from fatigued copper single crystals</title><author>Lepistö, T.K. ; Kostorz, G. ; Kuokkala, V.-T. ; Kettunen, P.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c365t-162a5a1fc7a2ca8380dbc2fd043676b4ad0a8ca764a69f96adfe6648a9ea2bbf3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1991</creationdate><topic>Applied sciences</topic><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Exact sciences and technology</topic><topic>Fatigue, brittleness, fracture, and cracks</topic><topic>Mechanical and acoustical properties of condensed matter</topic><topic>Mechanical properties of solids</topic><topic>Metals. Metallurgy</topic><topic>Physics</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Lepistö, T.K.</creatorcontrib><creatorcontrib>Kostorz, G.</creatorcontrib><creatorcontrib>Kuokkala, V.-T.</creatorcontrib><creatorcontrib>Kettunen, P.</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Copper Technical Reference Library</collection><collection>Materials Research Database</collection><jtitle>Materials science &amp; engineering. A, Structural materials : properties, microstructure and processing</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Lepistö, T.K.</au><au>Kostorz, G.</au><au>Kuokkala, V.-T.</au><au>Kettunen, P.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Small-angle neutron scattering from fatigued copper single crystals</atitle><jtitle>Materials science &amp; engineering. A, Structural materials : properties, microstructure and processing</jtitle><date>1991-01-20</date><risdate>1991</risdate><volume>131</volume><issue>2</issue><spage>171</spage><epage>176</epage><pages>171-176</pages><issn>0921-5093</issn><eissn>1873-4936</eissn><abstract>Copper single crystals oriented for single and multiple slip were studied by small-angle neutron scattering (SANS) after fatigue tests at a constant plastic shear strain amplitude y γ pl = 0.15% . For the SANS measurements, a special sample holder was used in order to obtain more reliable information about the small differences in the neutron scattering from individual samples. The size of the voids in the samples oriented for single slip increased as a function of the number of fatigue cycles, varying from 0.74 nm to 0.91 nm, but the volume fraction remained more or less constant. The dislocation density observed by SANS was found to increase from 6 × 10 7 mm −2 at τ max/2 to 4 × 10 8 mm −2 at τ max, but remained constant in the saturation stage of cyclic strain hardening. The SANS results obtained are in good agreement with positron annihilation data and transmission electron microscopy observations from the same specimens.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/0921-5093(91)90393-2</doi><tpages>6</tpages></addata></record>
fulltext fulltext
identifier ISSN: 0921-5093
ispartof Materials science & engineering. A, Structural materials : properties, microstructure and processing, 1991-01, Vol.131 (2), p.171-176
issn 0921-5093
1873-4936
language eng
recordid cdi_proquest_miscellaneous_25439705
source Elsevier ScienceDirect Journals
subjects Applied sciences
Condensed matter: structure, mechanical and thermal properties
Exact sciences and technology
Fatigue, brittleness, fracture, and cracks
Mechanical and acoustical properties of condensed matter
Mechanical properties of solids
Metals. Metallurgy
Physics
title Small-angle neutron scattering from fatigued copper single crystals
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-02-08T09%3A58%3A32IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Small-angle%20neutron%20scattering%20from%20fatigued%20copper%20single%20crystals&rft.jtitle=Materials%20science%20&%20engineering.%20A,%20Structural%20materials%20:%20properties,%20microstructure%20and%20processing&rft.au=Lepist%C3%B6,%20T.K.&rft.date=1991-01-20&rft.volume=131&rft.issue=2&rft.spage=171&rft.epage=176&rft.pages=171-176&rft.issn=0921-5093&rft.eissn=1873-4936&rft_id=info:doi/10.1016/0921-5093(91)90393-2&rft_dat=%3Cproquest_cross%3E25439705%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=25439705&rft_id=info:pmid/&rft_els_id=0921509391903932&rfr_iscdi=true