A study on using expanded perlite with hydroxyapatite: Reinforced bio-composites
People are exposed to different kinds of diseases or various accidents in life. Hydroxyapatite (HA) has been widely employed for bone treatment applications. In this study, HA was extracted from sheep bones. Bio-composites were doped with 1, 5, and 10 wt.% of expanded perlite and 5 wt.% of ZrO2–MgO-...
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| Veröffentlicht in: | Proceedings of the Institution of Mechanical Engineers. Part H, Journal of engineering in medicine Journal of engineering in medicine, 2021-05, Vol.235 (5), p.574-582 |
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| container_title | Proceedings of the Institution of Mechanical Engineers. Part H, Journal of engineering in medicine |
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| creator | Karip, Erdoğan Muratoğlu, Mehtap |
| description | People are exposed to different kinds of diseases or various accidents in life. Hydroxyapatite (HA) has been widely employed for bone treatment applications. In this study, HA was extracted from sheep bones. Bio-composites were doped with 1, 5, and 10 wt.% of expanded perlite and 5 wt.% of ZrO2–MgO-P2O5. The bio-composites were prepared by the cold isostatic pressing method (250 MPa) and sintered at 900°C for 1 h. In order to evaluate the characteristics of the bio-composites, microhardness, density, X-ray diffraction (XRD), Fourier transform infra-red spectroscopy (FT-IR), scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS) analyses were carried out on them. Additionally, the specimens whose characteristics were determined were kept in synthetic body fluid (SBF), and their in vitro behavior was examined. As a result, it was observed that microhardness increased as both the weight and the grain size of the expanded perlite were increased. Calcium silicate, tri-calcium phosphate, and hydroxyapatite were observed in the XRD analysis of all samples, and the formation of apatite structures was increased by addition of ZrO2–MgO–P2O5. |
| doi_str_mv | 10.1177/0954411921996565 |
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Hydroxyapatite (HA) has been widely employed for bone treatment applications. In this study, HA was extracted from sheep bones. Bio-composites were doped with 1, 5, and 10 wt.% of expanded perlite and 5 wt.% of ZrO2–MgO-P2O5. The bio-composites were prepared by the cold isostatic pressing method (250 MPa) and sintered at 900°C for 1 h. In order to evaluate the characteristics of the bio-composites, microhardness, density, X-ray diffraction (XRD), Fourier transform infra-red spectroscopy (FT-IR), scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS) analyses were carried out on them. Additionally, the specimens whose characteristics were determined were kept in synthetic body fluid (SBF), and their in vitro behavior was examined. As a result, it was observed that microhardness increased as both the weight and the grain size of the expanded perlite were increased. Calcium silicate, tri-calcium phosphate, and hydroxyapatite were observed in the XRD analysis of all samples, and the formation of apatite structures was increased by addition of ZrO2–MgO–P2O5.</description><identifier>ISSN: 0954-4119</identifier><identifier>EISSN: 2041-3033</identifier><identifier>DOI: 10.1177/0954411921996565</identifier><identifier>PMID: 33594926</identifier><language>eng</language><publisher>London, England: SAGE Publications</publisher><subject>Apatite ; Biomedical materials ; Body fluids ; Bones ; Calcium phosphates ; Calcium silicates ; Cold isostatic pressing ; Cold pressing ; Composite materials ; Fourier analysis ; Fourier transforms ; Grain size ; Hydroxyapatite ; Infrared spectroscopy ; Magnesium oxide ; Microhardness ; Perlite ; Phosphorus pentoxide ; Scanning electron microscopy ; Sheep ; Spectroscopy ; Spectrum analysis ; X-ray diffraction ; Zirconium dioxide</subject><ispartof>Proceedings of the Institution of Mechanical Engineers. 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Part H, Journal of engineering in medicine</title><addtitle>Proc Inst Mech Eng H</addtitle><description>People are exposed to different kinds of diseases or various accidents in life. Hydroxyapatite (HA) has been widely employed for bone treatment applications. In this study, HA was extracted from sheep bones. Bio-composites were doped with 1, 5, and 10 wt.% of expanded perlite and 5 wt.% of ZrO2–MgO-P2O5. The bio-composites were prepared by the cold isostatic pressing method (250 MPa) and sintered at 900°C for 1 h. In order to evaluate the characteristics of the bio-composites, microhardness, density, X-ray diffraction (XRD), Fourier transform infra-red spectroscopy (FT-IR), scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS) analyses were carried out on them. Additionally, the specimens whose characteristics were determined were kept in synthetic body fluid (SBF), and their in vitro behavior was examined. As a result, it was observed that microhardness increased as both the weight and the grain size of the expanded perlite were increased. Calcium silicate, tri-calcium phosphate, and hydroxyapatite were observed in the XRD analysis of all samples, and the formation of apatite structures was increased by addition of ZrO2–MgO–P2O5.</description><subject>Apatite</subject><subject>Biomedical materials</subject><subject>Body fluids</subject><subject>Bones</subject><subject>Calcium phosphates</subject><subject>Calcium silicates</subject><subject>Cold isostatic pressing</subject><subject>Cold pressing</subject><subject>Composite materials</subject><subject>Fourier analysis</subject><subject>Fourier transforms</subject><subject>Grain size</subject><subject>Hydroxyapatite</subject><subject>Infrared spectroscopy</subject><subject>Magnesium oxide</subject><subject>Microhardness</subject><subject>Perlite</subject><subject>Phosphorus pentoxide</subject><subject>Scanning electron microscopy</subject><subject>Sheep</subject><subject>Spectroscopy</subject><subject>Spectrum analysis</subject><subject>X-ray diffraction</subject><subject>Zirconium dioxide</subject><issn>0954-4119</issn><issn>2041-3033</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNp1kM1LAzEQxYMotlbvnmTBi5fVyccmjbdS_AJBET0v2STbbmk3a7KL3f_elFaFgnMZmPebN8ND6BzDNcZC3IDMGMNYEiwlz3h2gIYEGE4pUHqIhhs53egDdBLCAgAwBn6MBpRmkknCh-h1koS2M33i6qQLVT1L7LpRtbEmaaxfVq1Nvqp2nsx74926V41q4-w2ebNVXTqvI1dULtVu1bgQlXCKjkq1DPZs10fo4_7uffqYPr88PE0nz6mmPGvTArBlZMyoNcwoJghRWtDClFmBQatCWCksVlhungYTq9BaMKGAlBIIpyN0tfVtvPvsbGjzVRW0XS5VbV0XcsIkcOAiIxG93EMXrvN1_C4nGeaCjMdjHCnYUtq7ELwt88ZXK-X7HEO-STvfTzuuXOyMu2Jlze_CT7wRSLdAUDP7d_Vfw2-Ceoaz</recordid><startdate>202105</startdate><enddate>202105</enddate><creator>Karip, Erdoğan</creator><creator>Muratoğlu, Mehtap</creator><general>SAGE Publications</general><general>SAGE PUBLICATIONS, INC</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QF</scope><scope>7QO</scope><scope>7QQ</scope><scope>7SC</scope><scope>7SE</scope><scope>7SP</scope><scope>7SR</scope><scope>7TA</scope><scope>7TB</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>F28</scope><scope>FR3</scope><scope>H8D</scope><scope>H8G</scope><scope>JG9</scope><scope>JQ2</scope><scope>K9.</scope><scope>KR7</scope><scope>L7M</scope><scope>L~C</scope><scope>L~D</scope><scope>P64</scope><scope>7X8</scope><orcidid>https://orcid.org/0000-0002-2679-1360</orcidid></search><sort><creationdate>202105</creationdate><title>A study on using expanded perlite with hydroxyapatite: Reinforced bio-composites</title><author>Karip, Erdoğan ; 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Part H, Journal of engineering in medicine</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Karip, Erdoğan</au><au>Muratoğlu, Mehtap</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A study on using expanded perlite with hydroxyapatite: Reinforced bio-composites</atitle><jtitle>Proceedings of the Institution of Mechanical Engineers. Part H, Journal of engineering in medicine</jtitle><addtitle>Proc Inst Mech Eng H</addtitle><date>2021-05</date><risdate>2021</risdate><volume>235</volume><issue>5</issue><spage>574</spage><epage>582</epage><pages>574-582</pages><issn>0954-4119</issn><eissn>2041-3033</eissn><abstract>People are exposed to different kinds of diseases or various accidents in life. Hydroxyapatite (HA) has been widely employed for bone treatment applications. In this study, HA was extracted from sheep bones. Bio-composites were doped with 1, 5, and 10 wt.% of expanded perlite and 5 wt.% of ZrO2–MgO-P2O5. The bio-composites were prepared by the cold isostatic pressing method (250 MPa) and sintered at 900°C for 1 h. In order to evaluate the characteristics of the bio-composites, microhardness, density, X-ray diffraction (XRD), Fourier transform infra-red spectroscopy (FT-IR), scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS) analyses were carried out on them. Additionally, the specimens whose characteristics were determined were kept in synthetic body fluid (SBF), and their in vitro behavior was examined. As a result, it was observed that microhardness increased as both the weight and the grain size of the expanded perlite were increased. 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| ispartof | Proceedings of the Institution of Mechanical Engineers. Part H, Journal of engineering in medicine, 2021-05, Vol.235 (5), p.574-582 |
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| source | SAGE Complete A-Z List |
| subjects | Apatite Biomedical materials Body fluids Bones Calcium phosphates Calcium silicates Cold isostatic pressing Cold pressing Composite materials Fourier analysis Fourier transforms Grain size Hydroxyapatite Infrared spectroscopy Magnesium oxide Microhardness Perlite Phosphorus pentoxide Scanning electron microscopy Sheep Spectroscopy Spectrum analysis X-ray diffraction Zirconium dioxide |
| title | A study on using expanded perlite with hydroxyapatite: Reinforced bio-composites |
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