Low-temperature wet-chemical synthesis of amorphous indium sulfide powders

Low-temperature wet-chemical synthesis of amorphous indium sulfide powders

Reagent grade inorganic salts were used to synthesize amorphous indium sulfide powders at relatively low temperatures (⩽ 50° C). It was possible to prepare amorphous indium sulfide powders using the reaction between an acidified ( pH = 1.3) solution of indium chloride and sodium hydrosulfide (NaHS)....

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Veröffentlicht in:Materials letters 1987-09, Vol.5 (10), p.401-404
Hauptverfasser: Kumta, P.N., Phule, P.P., Risbud, S.H.
Format: Artikel
Sprache:eng
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Aerosols
Chemistry
Colloidal gels. Colloidal sols
Colloidal state and disperse state
Emulsions. Microemulsions. Foams
Exact sciences and technology
General and physical chemistry
Powders
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container_title Materials letters
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creator Kumta, P.N.
Phule, P.P.
Risbud, S.H.
description Reagent grade inorganic salts were used to synthesize amorphous indium sulfide powders at relatively low temperatures (⩽ 50° C). It was possible to prepare amorphous indium sulfide powders using the reaction between an acidified ( pH = 1.3) solution of indium chloride and sodium hydrosulfide (NaHS). The indium sulfide powders prepared by this process give a glass transition at 330°C and a crystallization exotherm on heating at 390°C in a DSC. Results of characterization of the amorphous and heattreated indium sulfide powders using electron microscopy (SEM, TEM), electron beam microprobe (EMPA) and X-ray diffraction (XRD) are presented.
doi_str_mv 10.1016/0167-577X(87)90049-8
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subjects Aerosols
Chemistry
Colloidal gels. Colloidal sols
Colloidal state and disperse state
Emulsions. Microemulsions. Foams
Exact sciences and technology
General and physical chemistry
Powders
title Low-temperature wet-chemical synthesis of amorphous indium sulfide powders
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