Effects of the ratio of silane to 10-methacryloyloxydecyl dihydrogenphosphate (MDP) in primer on bonding performance of silica-based and zirconia ceramics
The purpose of the study was to evaluate the effects of the ratio of different concentrations of silane to 1 wt% 10-methacryloyloxydecyl dihydrogenphosphate (MDP) in primer on the performance and durability of bonding to silica-based and zirconia ceramics. Phosphoric acid–treated lithium–disilicate...
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| Veröffentlicht in: | Journal of the mechanical behavior of biomedical materials 2020-12, Vol.112, p.104026-104026, Article 104026 |
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| creator | Koko, Minkhant Takagaki, Tomohiro Abdou, Ahmed Inokoshi, Masanao Ikeda, Masaomi Wada, Takahiro Uo, Motohiro Nikaido, Toru Tagami, Junji |
| description | The purpose of the study was to evaluate the effects of the ratio of different concentrations of silane to 1 wt% 10-methacryloyloxydecyl dihydrogenphosphate (MDP) in primer on the performance and durability of bonding to silica-based and zirconia ceramics.
Phosphoric acid–treated lithium–disilicate (LD) and alumina-blasted zirconia specimens were assigned to five groups according to surface chemical treatment with different concentrations of γ-methacryloxypropyltrimethoxysilane (γ-MPTS) to 1 wt% MDP containing primer as follows: S0) without γ-MPTS; S1) 1 wt% γ-MPTS; S2) 2 wt% γ-MPTS; S5) 5 wt% γ-MPTS and S10) 10 wt% γ-MPTS. After priming, stainless-steel rods were bonded to the specimens with PanaviaV5 cement. Tensile bond strength (TBS) test was evaluated after 24-h (TC0) or 5000 thermocycling (TC5K). The wettability of primer-treated surfaces was measured using contact angle measurements. Surface elemental composition of zirconia was determined with X-ray photoelectron spectroscopy (XPS). The TBS data were analyzed using Weibull analysis. Contact angle data were analyzed by three-way analysis of variance (α = 0.05).
Before thermocycling, S5 (34.3 ± 4.5 MPa) showed the highest TBS compared to S1 (27.8 ± 5.2 MPa) and S2 (29.7 ± 4.8 MPa), and insignificant difference with S10 (30.6 ± 6.2 MPa) in LD. For zirconia there was no significant difference in all silane containing primers with S0 (p > 0.05). Thermocycling decreased TBS for all experimental groups among both ceramics (p |
| doi_str_mv | 10.1016/j.jmbbm.2020.104026 |
| format | Article |
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Phosphoric acid–treated lithium–disilicate (LD) and alumina-blasted zirconia specimens were assigned to five groups according to surface chemical treatment with different concentrations of γ-methacryloxypropyltrimethoxysilane (γ-MPTS) to 1 wt% MDP containing primer as follows: S0) without γ-MPTS; S1) 1 wt% γ-MPTS; S2) 2 wt% γ-MPTS; S5) 5 wt% γ-MPTS and S10) 10 wt% γ-MPTS. After priming, stainless-steel rods were bonded to the specimens with PanaviaV5 cement. Tensile bond strength (TBS) test was evaluated after 24-h (TC0) or 5000 thermocycling (TC5K). The wettability of primer-treated surfaces was measured using contact angle measurements. Surface elemental composition of zirconia was determined with X-ray photoelectron spectroscopy (XPS). The TBS data were analyzed using Weibull analysis. Contact angle data were analyzed by three-way analysis of variance (α = 0.05).
Before thermocycling, S5 (34.3 ± 4.5 MPa) showed the highest TBS compared to S1 (27.8 ± 5.2 MPa) and S2 (29.7 ± 4.8 MPa), and insignificant difference with S10 (30.6 ± 6.2 MPa) in LD. For zirconia there was no significant difference in all silane containing primers with S0 (p > 0.05). Thermocycling decreased TBS for all experimental groups among both ceramics (p < 0.05). Contact angles increased in S5 and S10 for both LD and zirconia ceramics. XPS analysis revealed that phosphorous peak of MDP was detected after priming. Additionally, silica peak of γ-MPTS coexist with MDP in S5 on zirconia surface.
The bond strength of lithium-disilicate ceramics was improved with 5% γ-MPTS in MDP primer. Moreover, increasing percentage of γ-MPTS by more than 5% has not improved the bond strength, conversely, it can alter the long-term durability of the bonded ceramic. MDP primers alone are best suited for efficient bonding of resin cement with zirconia ceramic.
[Display omitted]
•Experimental primers can influence the bond strength and durability.•The effective silane-MDP ratio was ceramic materials–dependent.•Thermocycling decreased the tensile bond strength of all experimental primers.</description><identifier>ISSN: 1751-6161</identifier><identifier>EISSN: 1878-0180</identifier><identifier>DOI: 10.1016/j.jmbbm.2020.104026</identifier><identifier>PMID: 32841834</identifier><language>eng</language><publisher>AMSTERDAM: Elsevier Ltd</publisher><subject>Ceramics ; Dental Bonding ; Engineering ; Engineering, Biomedical ; Lithium–disilicate ; Materials Science ; Materials Science, Biomaterials ; Materials Testing ; MDP ; Resin Cements ; Science & Technology ; Shear Strength ; Silane ; Silanes ; Silicon Dioxide ; Surface Properties ; Technology ; Tensile bond strength ; X-ray photoelectron spectroscopy ; Zirconia ; Zirconium</subject><ispartof>Journal of the mechanical behavior of biomedical materials, 2020-12, Vol.112, p.104026-104026, Article 104026</ispartof><rights>2020 Elsevier Ltd</rights><rights>Copyright © 2020 Elsevier Ltd. All rights reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>true</woscitedreferencessubscribed><woscitedreferencescount>30</woscitedreferencescount><woscitedreferencesoriginalsourcerecordid>wos000587642000003</woscitedreferencesoriginalsourcerecordid><citedby>FETCH-LOGICAL-c425t-f3e7f1c3923126822c05883ac589570dbd0ac82ba2ca68a22a371fb5ab995e753</citedby><cites>FETCH-LOGICAL-c425t-f3e7f1c3923126822c05883ac589570dbd0ac82ba2ca68a22a371fb5ab995e753</cites><orcidid>0000-0002-4830-4594 ; 0000-0001-8833-3907 ; 0000-0003-4253-9189</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.jmbbm.2020.104026$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>315,781,785,3551,27929,27930,28253,46000</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/32841834$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Koko, Minkhant</creatorcontrib><creatorcontrib>Takagaki, Tomohiro</creatorcontrib><creatorcontrib>Abdou, Ahmed</creatorcontrib><creatorcontrib>Inokoshi, Masanao</creatorcontrib><creatorcontrib>Ikeda, Masaomi</creatorcontrib><creatorcontrib>Wada, Takahiro</creatorcontrib><creatorcontrib>Uo, Motohiro</creatorcontrib><creatorcontrib>Nikaido, Toru</creatorcontrib><creatorcontrib>Tagami, Junji</creatorcontrib><title>Effects of the ratio of silane to 10-methacryloyloxydecyl dihydrogenphosphate (MDP) in primer on bonding performance of silica-based and zirconia ceramics</title><title>Journal of the mechanical behavior of biomedical materials</title><addtitle>J MECH BEHAV BIOMED</addtitle><addtitle>J Mech Behav Biomed Mater</addtitle><description>The purpose of the study was to evaluate the effects of the ratio of different concentrations of silane to 1 wt% 10-methacryloyloxydecyl dihydrogenphosphate (MDP) in primer on the performance and durability of bonding to silica-based and zirconia ceramics.
Phosphoric acid–treated lithium–disilicate (LD) and alumina-blasted zirconia specimens were assigned to five groups according to surface chemical treatment with different concentrations of γ-methacryloxypropyltrimethoxysilane (γ-MPTS) to 1 wt% MDP containing primer as follows: S0) without γ-MPTS; S1) 1 wt% γ-MPTS; S2) 2 wt% γ-MPTS; S5) 5 wt% γ-MPTS and S10) 10 wt% γ-MPTS. After priming, stainless-steel rods were bonded to the specimens with PanaviaV5 cement. Tensile bond strength (TBS) test was evaluated after 24-h (TC0) or 5000 thermocycling (TC5K). The wettability of primer-treated surfaces was measured using contact angle measurements. Surface elemental composition of zirconia was determined with X-ray photoelectron spectroscopy (XPS). The TBS data were analyzed using Weibull analysis. Contact angle data were analyzed by three-way analysis of variance (α = 0.05).
Before thermocycling, S5 (34.3 ± 4.5 MPa) showed the highest TBS compared to S1 (27.8 ± 5.2 MPa) and S2 (29.7 ± 4.8 MPa), and insignificant difference with S10 (30.6 ± 6.2 MPa) in LD. For zirconia there was no significant difference in all silane containing primers with S0 (p > 0.05). Thermocycling decreased TBS for all experimental groups among both ceramics (p < 0.05). Contact angles increased in S5 and S10 for both LD and zirconia ceramics. XPS analysis revealed that phosphorous peak of MDP was detected after priming. Additionally, silica peak of γ-MPTS coexist with MDP in S5 on zirconia surface.
The bond strength of lithium-disilicate ceramics was improved with 5% γ-MPTS in MDP primer. Moreover, increasing percentage of γ-MPTS by more than 5% has not improved the bond strength, conversely, it can alter the long-term durability of the bonded ceramic. MDP primers alone are best suited for efficient bonding of resin cement with zirconia ceramic.
[Display omitted]
•Experimental primers can influence the bond strength and durability.•The effective silane-MDP ratio was ceramic materials–dependent.•Thermocycling decreased the tensile bond strength of all experimental primers.</description><subject>Ceramics</subject><subject>Dental Bonding</subject><subject>Engineering</subject><subject>Engineering, Biomedical</subject><subject>Lithium–disilicate</subject><subject>Materials Science</subject><subject>Materials Science, Biomaterials</subject><subject>Materials Testing</subject><subject>MDP</subject><subject>Resin Cements</subject><subject>Science & Technology</subject><subject>Shear Strength</subject><subject>Silane</subject><subject>Silanes</subject><subject>Silicon Dioxide</subject><subject>Surface Properties</subject><subject>Technology</subject><subject>Tensile bond strength</subject><subject>X-ray photoelectron spectroscopy</subject><subject>Zirconia</subject><subject>Zirconium</subject><issn>1751-6161</issn><issn>1878-0180</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><sourceid>AOWDO</sourceid><sourceid>EIF</sourceid><recordid>eNqNksmO1DAURSMEopuGL0BCXjZCKTxkcBYsWkUzSI1gAWvLw0vHpcQOtgsIn8LX4pCilwjLkged-6z7roviKcE7gknz8rA7TEpNO4rpelNh2twrzglveYkJx_fzvq1J2ZCGnBWPYjxg3GDM-cPijFFeEc6q8-LXdd-DThH5HqUBUJDJ-vUQ7SgdoOQRweUEaZA6LKPP88diQC8jMnZYTPC34ObBx3mQCdDlh9efniPr0BzsBAF5h5R3xrpbNEPofZik03Cqb7UslYxgkHQG_bRBe2cl0hDkZHV8XDzo5RjhyWm9KL68uf68f1fefHz7fn91U-qK1qnsGbQ90ayjjNCGU6pxzTmTuuZd3WKjDJaaUyWplg2XlErWkl7VUnVdDW3NLorLre4c_NcjxCQmGzWMq39_jIJWrK1ww5suo2xDdfAxBujF6lOGRRAs1lDEQfwJRayhiC2UrHp2euCoJjB3mr8pZODFBnwH5fuoLeQm3WEYZ0NtU1G8DpZp_v_03qY1Ubf3R5ey9NUmhdzPbxaCOMmNDfkXCOPtP538BpZuwO8</recordid><startdate>202012</startdate><enddate>202012</enddate><creator>Koko, Minkhant</creator><creator>Takagaki, Tomohiro</creator><creator>Abdou, Ahmed</creator><creator>Inokoshi, Masanao</creator><creator>Ikeda, Masaomi</creator><creator>Wada, Takahiro</creator><creator>Uo, Motohiro</creator><creator>Nikaido, Toru</creator><creator>Tagami, Junji</creator><general>Elsevier Ltd</general><general>Elsevier</general><scope>AOWDO</scope><scope>BLEPL</scope><scope>DTL</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><orcidid>https://orcid.org/0000-0002-4830-4594</orcidid><orcidid>https://orcid.org/0000-0001-8833-3907</orcidid><orcidid>https://orcid.org/0000-0003-4253-9189</orcidid></search><sort><creationdate>202012</creationdate><title>Effects of the ratio of silane to 10-methacryloyloxydecyl dihydrogenphosphate (MDP) in primer on bonding performance of silica-based and zirconia ceramics</title><author>Koko, Minkhant ; Takagaki, Tomohiro ; Abdou, Ahmed ; Inokoshi, Masanao ; Ikeda, Masaomi ; Wada, Takahiro ; Uo, Motohiro ; Nikaido, Toru ; Tagami, Junji</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c425t-f3e7f1c3923126822c05883ac589570dbd0ac82ba2ca68a22a371fb5ab995e753</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Ceramics</topic><topic>Dental Bonding</topic><topic>Engineering</topic><topic>Engineering, Biomedical</topic><topic>Lithium–disilicate</topic><topic>Materials Science</topic><topic>Materials Science, Biomaterials</topic><topic>Materials Testing</topic><topic>MDP</topic><topic>Resin Cements</topic><topic>Science & Technology</topic><topic>Shear Strength</topic><topic>Silane</topic><topic>Silanes</topic><topic>Silicon Dioxide</topic><topic>Surface Properties</topic><topic>Technology</topic><topic>Tensile bond strength</topic><topic>X-ray photoelectron spectroscopy</topic><topic>Zirconia</topic><topic>Zirconium</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Koko, Minkhant</creatorcontrib><creatorcontrib>Takagaki, Tomohiro</creatorcontrib><creatorcontrib>Abdou, Ahmed</creatorcontrib><creatorcontrib>Inokoshi, Masanao</creatorcontrib><creatorcontrib>Ikeda, Masaomi</creatorcontrib><creatorcontrib>Wada, Takahiro</creatorcontrib><creatorcontrib>Uo, Motohiro</creatorcontrib><creatorcontrib>Nikaido, Toru</creatorcontrib><creatorcontrib>Tagami, Junji</creatorcontrib><collection>Web of Science - Science Citation Index Expanded - 2020</collection><collection>Web of Science Core Collection</collection><collection>Science Citation Index Expanded</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of the mechanical behavior of biomedical materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Koko, Minkhant</au><au>Takagaki, Tomohiro</au><au>Abdou, Ahmed</au><au>Inokoshi, Masanao</au><au>Ikeda, Masaomi</au><au>Wada, Takahiro</au><au>Uo, Motohiro</au><au>Nikaido, Toru</au><au>Tagami, Junji</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Effects of the ratio of silane to 10-methacryloyloxydecyl dihydrogenphosphate (MDP) in primer on bonding performance of silica-based and zirconia ceramics</atitle><jtitle>Journal of the mechanical behavior of biomedical materials</jtitle><stitle>J MECH BEHAV BIOMED</stitle><addtitle>J Mech Behav Biomed Mater</addtitle><date>2020-12</date><risdate>2020</risdate><volume>112</volume><spage>104026</spage><epage>104026</epage><pages>104026-104026</pages><artnum>104026</artnum><issn>1751-6161</issn><eissn>1878-0180</eissn><abstract>The purpose of the study was to evaluate the effects of the ratio of different concentrations of silane to 1 wt% 10-methacryloyloxydecyl dihydrogenphosphate (MDP) in primer on the performance and durability of bonding to silica-based and zirconia ceramics.
Phosphoric acid–treated lithium–disilicate (LD) and alumina-blasted zirconia specimens were assigned to five groups according to surface chemical treatment with different concentrations of γ-methacryloxypropyltrimethoxysilane (γ-MPTS) to 1 wt% MDP containing primer as follows: S0) without γ-MPTS; S1) 1 wt% γ-MPTS; S2) 2 wt% γ-MPTS; S5) 5 wt% γ-MPTS and S10) 10 wt% γ-MPTS. After priming, stainless-steel rods were bonded to the specimens with PanaviaV5 cement. Tensile bond strength (TBS) test was evaluated after 24-h (TC0) or 5000 thermocycling (TC5K). The wettability of primer-treated surfaces was measured using contact angle measurements. Surface elemental composition of zirconia was determined with X-ray photoelectron spectroscopy (XPS). The TBS data were analyzed using Weibull analysis. Contact angle data were analyzed by three-way analysis of variance (α = 0.05).
Before thermocycling, S5 (34.3 ± 4.5 MPa) showed the highest TBS compared to S1 (27.8 ± 5.2 MPa) and S2 (29.7 ± 4.8 MPa), and insignificant difference with S10 (30.6 ± 6.2 MPa) in LD. For zirconia there was no significant difference in all silane containing primers with S0 (p > 0.05). Thermocycling decreased TBS for all experimental groups among both ceramics (p < 0.05). Contact angles increased in S5 and S10 for both LD and zirconia ceramics. XPS analysis revealed that phosphorous peak of MDP was detected after priming. Additionally, silica peak of γ-MPTS coexist with MDP in S5 on zirconia surface.
The bond strength of lithium-disilicate ceramics was improved with 5% γ-MPTS in MDP primer. Moreover, increasing percentage of γ-MPTS by more than 5% has not improved the bond strength, conversely, it can alter the long-term durability of the bonded ceramic. MDP primers alone are best suited for efficient bonding of resin cement with zirconia ceramic.
[Display omitted]
•Experimental primers can influence the bond strength and durability.•The effective silane-MDP ratio was ceramic materials–dependent.•Thermocycling decreased the tensile bond strength of all experimental primers.</abstract><cop>AMSTERDAM</cop><pub>Elsevier Ltd</pub><pmid>32841834</pmid><doi>10.1016/j.jmbbm.2020.104026</doi><tpages>8</tpages><orcidid>https://orcid.org/0000-0002-4830-4594</orcidid><orcidid>https://orcid.org/0000-0001-8833-3907</orcidid><orcidid>https://orcid.org/0000-0003-4253-9189</orcidid></addata></record> |
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| subjects | Ceramics Dental Bonding Engineering Engineering, Biomedical Lithium–disilicate Materials Science Materials Science, Biomaterials Materials Testing MDP Resin Cements Science & Technology Shear Strength Silane Silanes Silicon Dioxide Surface Properties Technology Tensile bond strength X-ray photoelectron spectroscopy Zirconia Zirconium |
| title | Effects of the ratio of silane to 10-methacryloyloxydecyl dihydrogenphosphate (MDP) in primer on bonding performance of silica-based and zirconia ceramics |
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