Novel eco-friendly electrospun nanomagnetic zinc oxide hybridized PVA/alginate/chitosan nanofibers for enhanced phenol decontamination
In the current study, poly(vinyl alcohol)/alginate/chitosan (PVA/Alg/CS) composite nanofiber was immobilized with six different ratios of nanomagnetic zinc oxide (M-ZnO) (0 wt%, 0.2 wt%, 0.4 wt%, 0.6 wt%, 0.8 wt%, and 1 wt%) via the electrospinning technique. The various fabricated composite (M-6) n...
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| Veröffentlicht in: | Environmental science and pollution research international 2020-12, Vol.27 (34), p.43077-43092 |
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| creator | Elkady, Marwa Salama, Eslam Amer, Wael A. Ebeid, El-Zeiny M. Ayad, Mohamad M. Shokry, Hassan |
| description | In the current study, poly(vinyl alcohol)/alginate/chitosan (PVA/Alg/CS) composite nanofiber was immobilized with six different ratios of nanomagnetic zinc oxide (M-ZnO) (0 wt%, 0.2 wt%, 0.4 wt%, 0.6 wt%, 0.8 wt%, and 1 wt%) via the electrospinning technique. The various fabricated composite (M-6) nanofibers were characterized using Fourier transform infrared (FTIR), X-ray diffractometer (XRD), vibrating sample magnetometer (VSM), scanning electron microscope (SEM), atomic force microscope (AFM), thermogravimetric analysis (TGA), mechanical testing machine, and optical contact angle measurement. The fabricated composite nanofibers were applied for the adsorption of phenol from aqueous solutions. The 1.0 wt% M-ZnO/PVA/Alg/CS composite nanofibers were selected as the best phenol adsorbent with removal percentage of 84.22%. The influence of different processing parameter such as contact time, composite nanofiber dosage, pH, initial pollutant concentration, and temperature were examined. Increasing nanofiber dosage and the solution temperature was found to enhance the phenol adsorption onto the prepared nanocomposites. The maximum percentage of phenol removal was achieved at 84.22% after 90 min. Meanwhile, the maximum monolayer adsorption capacity (at pH = 5.0) was estimated to be 10.03 mg g
−1
at 25 °C. Kinetic, isotherm, and thermodynamic studies were designated to proof the endothermic, spontaneous, and thermodynamically nature of the phenol adsorption process. These outcomes indicate the effectiveness of the fabricated M-ZnO/PVA/Alg/CS nanofibers as adsorbent materials for phenol from aqueous solutions. |
| doi_str_mv | 10.1007/s11356-020-10247-8 |
| format | Article |
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−1
at 25 °C. Kinetic, isotherm, and thermodynamic studies were designated to proof the endothermic, spontaneous, and thermodynamically nature of the phenol adsorption process. These outcomes indicate the effectiveness of the fabricated M-ZnO/PVA/Alg/CS nanofibers as adsorbent materials for phenol from aqueous solutions.</description><identifier>ISSN: 0944-1344</identifier><identifier>EISSN: 1614-7499</identifier><identifier>DOI: 10.1007/s11356-020-10247-8</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Adsorbents ; Adsorption ; Alginates ; Alginic acid ; Aquatic Pollution ; Aqueous solutions ; Atmospheric Protection/Air Quality Control/Air Pollution ; Atomic force microscopes ; Atomic force microscopy ; Chitosan ; Contact angle ; Decontamination ; Dosage ; Earth and Environmental Science ; Ecotoxicology ; Environment ; Environmental Chemistry ; Environmental Health ; Environmental science ; Fourier analysis ; Fourier transforms ; Mechanical properties ; Mechanical tests ; Nanocomposites ; Nanofibers ; pH effects ; Phenols ; Pollutants ; Polyvinyl alcohol ; Process parameters ; Research Article ; Scanning electron microscopy ; Thermogravimetric analysis ; Waste Water Technology ; Water Management ; Water Pollution Control ; Zinc oxide ; Zinc oxides</subject><ispartof>Environmental science and pollution research international, 2020-12, Vol.27 (34), p.43077-43092</ispartof><rights>Springer-Verlag GmbH Germany, part of Springer Nature 2020</rights><rights>Springer-Verlag GmbH Germany, part of Springer Nature 2020.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c389t-55d5c618f2dd540a889cda33989218ef8e0e945b88286c9d7d11660ef1b564453</citedby><cites>FETCH-LOGICAL-c389t-55d5c618f2dd540a889cda33989218ef8e0e945b88286c9d7d11660ef1b564453</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11356-020-10247-8$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11356-020-10247-8$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Elkady, Marwa</creatorcontrib><creatorcontrib>Salama, Eslam</creatorcontrib><creatorcontrib>Amer, Wael A.</creatorcontrib><creatorcontrib>Ebeid, El-Zeiny M.</creatorcontrib><creatorcontrib>Ayad, Mohamad M.</creatorcontrib><creatorcontrib>Shokry, Hassan</creatorcontrib><title>Novel eco-friendly electrospun nanomagnetic zinc oxide hybridized PVA/alginate/chitosan nanofibers for enhanced phenol decontamination</title><title>Environmental science and pollution research international</title><addtitle>Environ Sci Pollut Res</addtitle><description>In the current study, poly(vinyl alcohol)/alginate/chitosan (PVA/Alg/CS) composite nanofiber was immobilized with six different ratios of nanomagnetic zinc oxide (M-ZnO) (0 wt%, 0.2 wt%, 0.4 wt%, 0.6 wt%, 0.8 wt%, and 1 wt%) via the electrospinning technique. The various fabricated composite (M-6) nanofibers were characterized using Fourier transform infrared (FTIR), X-ray diffractometer (XRD), vibrating sample magnetometer (VSM), scanning electron microscope (SEM), atomic force microscope (AFM), thermogravimetric analysis (TGA), mechanical testing machine, and optical contact angle measurement. The fabricated composite nanofibers were applied for the adsorption of phenol from aqueous solutions. The 1.0 wt% M-ZnO/PVA/Alg/CS composite nanofibers were selected as the best phenol adsorbent with removal percentage of 84.22%. The influence of different processing parameter such as contact time, composite nanofiber dosage, pH, initial pollutant concentration, and temperature were examined. Increasing nanofiber dosage and the solution temperature was found to enhance the phenol adsorption onto the prepared nanocomposites. The maximum percentage of phenol removal was achieved at 84.22% after 90 min. Meanwhile, the maximum monolayer adsorption capacity (at pH = 5.0) was estimated to be 10.03 mg g
−1
at 25 °C. Kinetic, isotherm, and thermodynamic studies were designated to proof the endothermic, spontaneous, and thermodynamically nature of the phenol adsorption process. These outcomes indicate the effectiveness of the fabricated M-ZnO/PVA/Alg/CS nanofibers as adsorbent materials for phenol from aqueous solutions.</description><subject>Adsorbents</subject><subject>Adsorption</subject><subject>Alginates</subject><subject>Alginic acid</subject><subject>Aquatic Pollution</subject><subject>Aqueous solutions</subject><subject>Atmospheric Protection/Air Quality Control/Air Pollution</subject><subject>Atomic force microscopes</subject><subject>Atomic force microscopy</subject><subject>Chitosan</subject><subject>Contact angle</subject><subject>Decontamination</subject><subject>Dosage</subject><subject>Earth and Environmental Science</subject><subject>Ecotoxicology</subject><subject>Environment</subject><subject>Environmental Chemistry</subject><subject>Environmental Health</subject><subject>Environmental science</subject><subject>Fourier analysis</subject><subject>Fourier transforms</subject><subject>Mechanical properties</subject><subject>Mechanical tests</subject><subject>Nanocomposites</subject><subject>Nanofibers</subject><subject>pH effects</subject><subject>Phenols</subject><subject>Pollutants</subject><subject>Polyvinyl alcohol</subject><subject>Process parameters</subject><subject>Research Article</subject><subject>Scanning electron microscopy</subject><subject>Thermogravimetric analysis</subject><subject>Waste Water Technology</subject><subject>Water Management</subject><subject>Water Pollution Control</subject><subject>Zinc oxide</subject><subject>Zinc 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decontamination</atitle><jtitle>Environmental science and pollution research international</jtitle><stitle>Environ Sci Pollut Res</stitle><date>2020-12-01</date><risdate>2020</risdate><volume>27</volume><issue>34</issue><spage>43077</spage><epage>43092</epage><pages>43077-43092</pages><issn>0944-1344</issn><eissn>1614-7499</eissn><abstract>In the current study, poly(vinyl alcohol)/alginate/chitosan (PVA/Alg/CS) composite nanofiber was immobilized with six different ratios of nanomagnetic zinc oxide (M-ZnO) (0 wt%, 0.2 wt%, 0.4 wt%, 0.6 wt%, 0.8 wt%, and 1 wt%) via the electrospinning technique. The various fabricated composite (M-6) nanofibers were characterized using Fourier transform infrared (FTIR), X-ray diffractometer (XRD), vibrating sample magnetometer (VSM), scanning electron microscope (SEM), atomic force microscope (AFM), thermogravimetric analysis (TGA), mechanical testing machine, and optical contact angle measurement. The fabricated composite nanofibers were applied for the adsorption of phenol from aqueous solutions. The 1.0 wt% M-ZnO/PVA/Alg/CS composite nanofibers were selected as the best phenol adsorbent with removal percentage of 84.22%. The influence of different processing parameter such as contact time, composite nanofiber dosage, pH, initial pollutant concentration, and temperature were examined. Increasing nanofiber dosage and the solution temperature was found to enhance the phenol adsorption onto the prepared nanocomposites. The maximum percentage of phenol removal was achieved at 84.22% after 90 min. Meanwhile, the maximum monolayer adsorption capacity (at pH = 5.0) was estimated to be 10.03 mg g
−1
at 25 °C. Kinetic, isotherm, and thermodynamic studies were designated to proof the endothermic, spontaneous, and thermodynamically nature of the phenol adsorption process. These outcomes indicate the effectiveness of the fabricated M-ZnO/PVA/Alg/CS nanofibers as adsorbent materials for phenol from aqueous solutions.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><doi>10.1007/s11356-020-10247-8</doi><tpages>16</tpages></addata></record> |
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| subjects | Adsorbents Adsorption Alginates Alginic acid Aquatic Pollution Aqueous solutions Atmospheric Protection/Air Quality Control/Air Pollution Atomic force microscopes Atomic force microscopy Chitosan Contact angle Decontamination Dosage Earth and Environmental Science Ecotoxicology Environment Environmental Chemistry Environmental Health Environmental science Fourier analysis Fourier transforms Mechanical properties Mechanical tests Nanocomposites Nanofibers pH effects Phenols Pollutants Polyvinyl alcohol Process parameters Research Article Scanning electron microscopy Thermogravimetric analysis Waste Water Technology Water Management Water Pollution Control Zinc oxide Zinc oxides |
| title | Novel eco-friendly electrospun nanomagnetic zinc oxide hybridized PVA/alginate/chitosan nanofibers for enhanced phenol decontamination |
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