Preparation, structural, microstructural, mechanical and cytotoxic characterization of as-cast Ti-25Ta-Zr alloys
Titanium alloys have been widely used as biomaterials, especially for orthopedic prostheses and dental implants, but these materials have Young's modulus almost three times greater than human cortical bones. Because of this, new alloys are being produced for the propose of decreasing Young'...
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| Veröffentlicht in: | Journal of materials science. Materials in medicine 2020-02, Vol.31 (2), p.19-19, Article 19 |
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| creator | Kuroda, Pedro Akira Bazaglia de Freitas Quadros, Fernanda Sousa, Karolyne dos Santos Jorge Donato, Tatiani Ayako Goto de Araújo, Raul Oliveira Grandini, Carlos Roberto |
| description | Titanium alloys have been widely used as biomaterials, especially for orthopedic prostheses and dental implants, but these materials have Young's modulus almost three times greater than human cortical bones. Because of this, new alloys are being produced for the propose of decreasing Young's modulus to achieve a more balanced mechanical compatibility with the bone. In this paper, it is reported the development of Ti-25Ta alloys as a base material, in which was introduced zirconium, with concentration varying between 0 and 40 wt%, with the aim of biomedical applications. The alloys were prepared in an arc-melting furnace. The microstructural analysis was performed by x-ray diffraction as well as optical and scanning electron microscopy. Selected mechanical properties were analyzed by microhardness and Young’s modulus measurements, and cytotoxicity analysis by indirect test. X-ray measurements revealed the presence of α″ phase in the alloy without zirconium; α″ + β phases for alloys with 10, 20, and 30 wt% of zirconium, and β phase only for the alloy with 40 wt% of zirconium. These results were corroborated by the microscopy results. The hardness of the alloy was higher than that of cp-Ti due to the actions of zirconium and tantalum as hardening agents. The Young’s modulus decreases with high levels of zirconium due to the stabilization of the β phase. The cytotoxicity test showed that the extracts of studied alloys are not cytotoxic for osteoblast cells in short periods of culture. |
| doi_str_mv | 10.1007/s10856-019-6350-7 |
| format | Article |
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Because of this, new alloys are being produced for the propose of decreasing Young's modulus to achieve a more balanced mechanical compatibility with the bone. In this paper, it is reported the development of Ti-25Ta alloys as a base material, in which was introduced zirconium, with concentration varying between 0 and 40 wt%, with the aim of biomedical applications. The alloys were prepared in an arc-melting furnace. The microstructural analysis was performed by x-ray diffraction as well as optical and scanning electron microscopy. Selected mechanical properties were analyzed by microhardness and Young’s modulus measurements, and cytotoxicity analysis by indirect test. X-ray measurements revealed the presence of α″ phase in the alloy without zirconium; α″ + β phases for alloys with 10, 20, and 30 wt% of zirconium, and β phase only for the alloy with 40 wt% of zirconium. These results were corroborated by the microscopy results. The hardness of the alloy was higher than that of cp-Ti due to the actions of zirconium and tantalum as hardening agents. The Young’s modulus decreases with high levels of zirconium due to the stabilization of the β phase. The cytotoxicity test showed that the extracts of studied alloys are not cytotoxic for osteoblast cells in short periods of culture.</description><identifier>ISSN: 0957-4530</identifier><identifier>EISSN: 1573-4838</identifier><identifier>DOI: 10.1007/s10856-019-6350-7</identifier><identifier>PMID: 31965338</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Alloy development ; Alloys ; Beta phase ; Biocompatibility ; Biomaterials ; Biomaterials Synthesis and Characterization ; Biomedical Engineering and Bioengineering ; Biomedical materials ; Bones ; Cell culture ; Ceramics ; Chemistry and Materials Science ; Composites ; Cytotoxicity ; Dental implants ; Dental materials ; Dental prosthetics ; Glass ; Materials Science ; Mechanical properties ; Melting furnaces ; Microhardness ; Microscopy ; Microstructural analysis ; Modulus of elasticity ; Natural Materials ; Optical properties ; Orthopedics ; Polymer Sciences ; Prostheses ; Regenerative Medicine/Tissue Engineering ; Scanning electron microscopy ; Surfaces and Interfaces ; Surgical implants ; Tantalum ; Thin Films ; Titanium ; Titanium alloys ; Titanium base alloys ; Toxicity testing ; X-ray diffraction ; Zirconium ; Zirconium base alloys</subject><ispartof>Journal of materials science. Materials in medicine, 2020-02, Vol.31 (2), p.19-19, Article 19</ispartof><rights>Springer Science+Business Media, LLC, part of Springer Nature 2020</rights><rights>Journal of Materials Science: Materials in Medicine is a copyright of Springer, (2020). All Rights Reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c372t-f3d85f6d1c88bf3cfd021ca54882f92fcd1db5485cf6262fb8b668144d60aa513</citedby><cites>FETCH-LOGICAL-c372t-f3d85f6d1c88bf3cfd021ca54882f92fcd1db5485cf6262fb8b668144d60aa513</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10856-019-6350-7$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10856-019-6350-7$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27903,27904,41467,42536,51298</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/31965338$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Kuroda, Pedro Akira Bazaglia</creatorcontrib><creatorcontrib>de Freitas Quadros, Fernanda</creatorcontrib><creatorcontrib>Sousa, Karolyne dos Santos Jorge</creatorcontrib><creatorcontrib>Donato, Tatiani Ayako Goto</creatorcontrib><creatorcontrib>de Araújo, Raul Oliveira</creatorcontrib><creatorcontrib>Grandini, Carlos Roberto</creatorcontrib><title>Preparation, structural, microstructural, mechanical and cytotoxic characterization of as-cast Ti-25Ta-Zr alloys</title><title>Journal of materials science. Materials in medicine</title><addtitle>J Mater Sci: Mater Med</addtitle><addtitle>J Mater Sci Mater Med</addtitle><description>Titanium alloys have been widely used as biomaterials, especially for orthopedic prostheses and dental implants, but these materials have Young's modulus almost three times greater than human cortical bones. Because of this, new alloys are being produced for the propose of decreasing Young's modulus to achieve a more balanced mechanical compatibility with the bone. In this paper, it is reported the development of Ti-25Ta alloys as a base material, in which was introduced zirconium, with concentration varying between 0 and 40 wt%, with the aim of biomedical applications. The alloys were prepared in an arc-melting furnace. The microstructural analysis was performed by x-ray diffraction as well as optical and scanning electron microscopy. Selected mechanical properties were analyzed by microhardness and Young’s modulus measurements, and cytotoxicity analysis by indirect test. X-ray measurements revealed the presence of α″ phase in the alloy without zirconium; α″ + β phases for alloys with 10, 20, and 30 wt% of zirconium, and β phase only for the alloy with 40 wt% of zirconium. These results were corroborated by the microscopy results. The hardness of the alloy was higher than that of cp-Ti due to the actions of zirconium and tantalum as hardening agents. The Young’s modulus decreases with high levels of zirconium due to the stabilization of the β phase. The cytotoxicity test showed that the extracts of studied alloys are not cytotoxic for osteoblast cells in short periods of culture.</description><subject>Alloy development</subject><subject>Alloys</subject><subject>Beta phase</subject><subject>Biocompatibility</subject><subject>Biomaterials</subject><subject>Biomaterials Synthesis and Characterization</subject><subject>Biomedical Engineering and Bioengineering</subject><subject>Biomedical materials</subject><subject>Bones</subject><subject>Cell culture</subject><subject>Ceramics</subject><subject>Chemistry and Materials Science</subject><subject>Composites</subject><subject>Cytotoxicity</subject><subject>Dental implants</subject><subject>Dental materials</subject><subject>Dental prosthetics</subject><subject>Glass</subject><subject>Materials Science</subject><subject>Mechanical properties</subject><subject>Melting furnaces</subject><subject>Microhardness</subject><subject>Microscopy</subject><subject>Microstructural 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Materials in medicine</jtitle><stitle>J Mater Sci: Mater Med</stitle><addtitle>J Mater Sci Mater Med</addtitle><date>2020-02-01</date><risdate>2020</risdate><volume>31</volume><issue>2</issue><spage>19</spage><epage>19</epage><pages>19-19</pages><artnum>19</artnum><issn>0957-4530</issn><eissn>1573-4838</eissn><abstract>Titanium alloys have been widely used as biomaterials, especially for orthopedic prostheses and dental implants, but these materials have Young's modulus almost three times greater than human cortical bones. Because of this, new alloys are being produced for the propose of decreasing Young's modulus to achieve a more balanced mechanical compatibility with the bone. In this paper, it is reported the development of Ti-25Ta alloys as a base material, in which was introduced zirconium, with concentration varying between 0 and 40 wt%, with the aim of biomedical applications. The alloys were prepared in an arc-melting furnace. The microstructural analysis was performed by x-ray diffraction as well as optical and scanning electron microscopy. Selected mechanical properties were analyzed by microhardness and Young’s modulus measurements, and cytotoxicity analysis by indirect test. X-ray measurements revealed the presence of α″ phase in the alloy without zirconium; α″ + β phases for alloys with 10, 20, and 30 wt% of zirconium, and β phase only for the alloy with 40 wt% of zirconium. These results were corroborated by the microscopy results. The hardness of the alloy was higher than that of cp-Ti due to the actions of zirconium and tantalum as hardening agents. The Young’s modulus decreases with high levels of zirconium due to the stabilization of the β phase. The cytotoxicity test showed that the extracts of studied alloys are not cytotoxic for osteoblast cells in short periods of culture.</abstract><cop>New York</cop><pub>Springer US</pub><pmid>31965338</pmid><doi>10.1007/s10856-019-6350-7</doi><tpages>1</tpages></addata></record> |
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| source | Springer Nature - Complete Springer Journals |
| subjects | Alloy development Alloys Beta phase Biocompatibility Biomaterials Biomaterials Synthesis and Characterization Biomedical Engineering and Bioengineering Biomedical materials Bones Cell culture Ceramics Chemistry and Materials Science Composites Cytotoxicity Dental implants Dental materials Dental prosthetics Glass Materials Science Mechanical properties Melting furnaces Microhardness Microscopy Microstructural analysis Modulus of elasticity Natural Materials Optical properties Orthopedics Polymer Sciences Prostheses Regenerative Medicine/Tissue Engineering Scanning electron microscopy Surfaces and Interfaces Surgical implants Tantalum Thin Films Titanium Titanium alloys Titanium base alloys Toxicity testing X-ray diffraction Zirconium Zirconium base alloys |
| title | Preparation, structural, microstructural, mechanical and cytotoxic characterization of as-cast Ti-25Ta-Zr alloys |
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