Sensitive quantitative analysis of phosphorylated primary metabolites using selective metal oxide enrichment and GC- and IC- MS/MS

In this study, we present a novel selective cleanup/enrichment method based on metal oxide solid phase extraction combined with quantitative gas chromatography-tandem mass spectrometry and ion exchange chromatography-tandem mass spectrometry for the analysis of phosphorylated metabolites in yeast ce...

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Veröffentlicht in:	Talanta (Oxford) 2019-12, Vol.205, p.120147-120147, Article 120147
Hauptverfasser:	Si-Hung, Le, Troyer, Christina, Causon, Tim, Hann, Stephan
Format:	Artikel
Sprache:	eng
Schlagworte:	Gas Chromatography-Mass Spectrometry - methods Ion Exchange Limit of Detection Mass spectrometry Metabolomics Metabolomics - methods Metabolomics - standards Metals - chemistry Oxides - chemistry Phosphorylation Pichia - chemistry Quantification Reference Standards Sample preparation Solid Phase Extraction Sugar phosphate Tandem Mass Spectrometry - methods
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