Comparison of three‐phase hollow fiber liquid‐phase microextraction based on reverse micelle with conventional two‐phase hollow fiber liquid‐phase microextraction and their applications for analysis of cinnamic acids in traditional Chinese medicines
A novel three‐phase hollow fiber liquid‐phase microextraction was developed based on reverse micelle as extraction solvent and acceptor phase, and compared with conventional two‐phase hollow fiber liquid‐phase microextraction. Both procedures were used in the extraction and concentration of four cin...
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| Veröffentlicht in: | Journal of separation science 2019-09, Vol.42 (18), p.2977-2984 |
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| creator | Liu, Zhao‐chan Zhang, Shu‐mei Wang, Run‐qin Chen, Xuan Hu, Shuang Bai, Xiao‐hong |
| description | A novel three‐phase hollow fiber liquid‐phase microextraction was developed based on reverse micelle as extraction solvent and acceptor phase, and compared with conventional two‐phase hollow fiber liquid‐phase microextraction. Both procedures were used in the extraction and concentration of four cinnamic acids (caffeic acid, p‐hydroxycinnamic acid, ferulic acid, and cinnamic acid) in traditional Chinese medicines prior to high‐performance liquid chromatography analysis. Parameters affecting the two procedures were investigated and optimized to obtain the optimum enrichment factors. The mechanism of the developed procedure was explored and elucidated by comparison with conventional two‐phase hollow fiber liquid‐phase microextraction. Under the optimized conditions, the analytes’ enrichment factors were between 50 and 118 for the proposed procedure, and 31–96 for conventional two‐phase mode. Satisfactory linear ranges (r2 ≥ 0.99), detection limits (0.1–0.6 ng/mL), precisions ( |
| doi_str_mv | 10.1002/jssc.201900472 |
| format | Article |
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Both procedures were used in the extraction and concentration of four cinnamic acids (caffeic acid, p‐hydroxycinnamic acid, ferulic acid, and cinnamic acid) in traditional Chinese medicines prior to high‐performance liquid chromatography analysis. Parameters affecting the two procedures were investigated and optimized to obtain the optimum enrichment factors. The mechanism of the developed procedure was explored and elucidated by comparison with conventional two‐phase hollow fiber liquid‐phase microextraction. Under the optimized conditions, the analytes’ enrichment factors were between 50 and 118 for the proposed procedure, and 31–96 for conventional two‐phase mode. Satisfactory linear ranges (r2 ≥ 0.99), detection limits (0.1–0.6 ng/mL), precisions (<9.2%), and accuracies (recoveries: 80–123.1%) were observed for the two procedures. The results showed that the enrichment capacity of the proposed procedure for the cinnamic acids is better than that of conventional two‐phase procedure, and both are eco‐friendly, simple, and effective for the enrichment and detection of cinnamic acids in traditional Chinese medicines.</description><identifier>ISSN: 1615-9306</identifier><identifier>EISSN: 1615-9314</identifier><identifier>DOI: 10.1002/jssc.201900472</identifier><identifier>PMID: 31273922</identifier><language>eng</language><publisher>Germany: Wiley Subscription Services, Inc</publisher><subject>Acids ; Cinnamates - analysis ; Cinnamic acid ; cinnamic acids ; Drugs, Chinese Herbal - analysis ; Enrichment ; Ferulic acid ; high performance liquid chromatography ; hollow fiber liquid‐phase microextraction ; Hydroxycinnamic acid ; Liquid chromatography ; Liquid Phase Microextraction ; Medicine, Chinese Traditional ; Micelles ; Molecular Structure ; reverse micelle ; Reverse micelles ; Traditional Chinese medicine ; traditional Chinese medicines</subject><ispartof>Journal of separation science, 2019-09, Vol.42 (18), p.2977-2984</ispartof><rights>2019 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim</rights><rights>2019 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c4051-b499e0e5e4a75f42b37f866b79a768459ec12981f436705583e59bc040c774443</citedby><cites>FETCH-LOGICAL-c4051-b499e0e5e4a75f42b37f866b79a768459ec12981f436705583e59bc040c774443</cites><orcidid>0000-0002-0784-3786 ; 0000-0002-8276-4586 ; 0000-0001-5287-6002</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fjssc.201900472$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fjssc.201900472$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,780,784,1416,27923,27924,45573,45574</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/31273922$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Liu, Zhao‐chan</creatorcontrib><creatorcontrib>Zhang, Shu‐mei</creatorcontrib><creatorcontrib>Wang, Run‐qin</creatorcontrib><creatorcontrib>Chen, Xuan</creatorcontrib><creatorcontrib>Hu, Shuang</creatorcontrib><creatorcontrib>Bai, Xiao‐hong</creatorcontrib><title>Comparison of three‐phase hollow fiber liquid‐phase microextraction based on reverse micelle with conventional two‐phase hollow fiber liquid‐phase microextraction and their applications for analysis of cinnamic acids in traditional Chinese medicines</title><title>Journal of separation science</title><addtitle>J Sep Sci</addtitle><description>A novel three‐phase hollow fiber liquid‐phase microextraction was developed based on reverse micelle as extraction solvent and acceptor phase, and compared with conventional two‐phase hollow fiber liquid‐phase microextraction. Both procedures were used in the extraction and concentration of four cinnamic acids (caffeic acid, p‐hydroxycinnamic acid, ferulic acid, and cinnamic acid) in traditional Chinese medicines prior to high‐performance liquid chromatography analysis. Parameters affecting the two procedures were investigated and optimized to obtain the optimum enrichment factors. The mechanism of the developed procedure was explored and elucidated by comparison with conventional two‐phase hollow fiber liquid‐phase microextraction. Under the optimized conditions, the analytes’ enrichment factors were between 50 and 118 for the proposed procedure, and 31–96 for conventional two‐phase mode. Satisfactory linear ranges (r2 ≥ 0.99), detection limits (0.1–0.6 ng/mL), precisions (<9.2%), and accuracies (recoveries: 80–123.1%) were observed for the two procedures. The results showed that the enrichment capacity of the proposed procedure for the cinnamic acids is better than that of conventional two‐phase procedure, and both are eco‐friendly, simple, and effective for the enrichment and detection of cinnamic acids in traditional Chinese medicines.</description><subject>Acids</subject><subject>Cinnamates - analysis</subject><subject>Cinnamic acid</subject><subject>cinnamic acids</subject><subject>Drugs, Chinese Herbal - analysis</subject><subject>Enrichment</subject><subject>Ferulic acid</subject><subject>high performance liquid chromatography</subject><subject>hollow fiber liquid‐phase microextraction</subject><subject>Hydroxycinnamic acid</subject><subject>Liquid chromatography</subject><subject>Liquid Phase Microextraction</subject><subject>Medicine, Chinese Traditional</subject><subject>Micelles</subject><subject>Molecular Structure</subject><subject>reverse micelle</subject><subject>Reverse micelles</subject><subject>Traditional Chinese medicine</subject><subject>traditional Chinese medicines</subject><issn>1615-9306</issn><issn>1615-9314</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqdkruO1DAUhrNoEXuBlhJZoqGZwdc4LlHEVStRLNSR45woZ5SJs3ays9PtI-wz8iQ4mmEKGiQqHx1_5z8X_Vn2mtE1o5S_38To1pwyQ6nU_Fl2yXKmVkYweX6KaX6RXcW4oZTpwtAX2YVgXAvD-eXZWem3ow0Y_UB8S6YuAPx6fBo7G4F0vu_9jrRYQyA93s3YnP626IKHhylYN2EqrlOyISkIcA_hAEDfA9nh1BHnh3sYFtD2ZNr5_2phhyYNCBiIHccenV2ykbQ-JZLuPmJcdnA4DDbVEuuwiQQHkhQaPDYvOxxgEYcG3RK-zJ63to_w6vheZz8_ffxRflndfP_8tfxws3KSKraqpTFAQYG0WrWS10K3RZ7X2lidF1IZcIybgrVS5JoqVQhQpnZUUqe1lFJcZ-8OumPwdzPEqdpiXE5kB_BzrDhXgmsjRZHQt3-hGz-HNP1CGVHQXDGRqPWBSleKMUBbjQG3NuwrRqvFHNVijupkjlTw5ig712n9E_7HDQmQB2CHPez_IVd9u70tc8WZ-A32Mc94</recordid><startdate>201909</startdate><enddate>201909</enddate><creator>Liu, Zhao‐chan</creator><creator>Zhang, Shu‐mei</creator><creator>Wang, Run‐qin</creator><creator>Chen, Xuan</creator><creator>Hu, Shuang</creator><creator>Bai, Xiao‐hong</creator><general>Wiley Subscription Services, Inc</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope><scope>7X8</scope><orcidid>https://orcid.org/0000-0002-0784-3786</orcidid><orcidid>https://orcid.org/0000-0002-8276-4586</orcidid><orcidid>https://orcid.org/0000-0001-5287-6002</orcidid></search><sort><creationdate>201909</creationdate><title>Comparison of three‐phase hollow fiber liquid‐phase microextraction based on reverse micelle with conventional two‐phase hollow fiber liquid‐phase microextraction and their applications for analysis of cinnamic acids in traditional Chinese medicines</title><author>Liu, Zhao‐chan ; Zhang, Shu‐mei ; Wang, Run‐qin ; Chen, Xuan ; Hu, Shuang ; Bai, Xiao‐hong</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4051-b499e0e5e4a75f42b37f866b79a768459ec12981f436705583e59bc040c774443</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>Acids</topic><topic>Cinnamates - analysis</topic><topic>Cinnamic acid</topic><topic>cinnamic acids</topic><topic>Drugs, Chinese Herbal - analysis</topic><topic>Enrichment</topic><topic>Ferulic acid</topic><topic>high performance liquid chromatography</topic><topic>hollow fiber liquid‐phase microextraction</topic><topic>Hydroxycinnamic acid</topic><topic>Liquid chromatography</topic><topic>Liquid Phase Microextraction</topic><topic>Medicine, Chinese Traditional</topic><topic>Micelles</topic><topic>Molecular Structure</topic><topic>reverse micelle</topic><topic>Reverse micelles</topic><topic>Traditional Chinese medicine</topic><topic>traditional Chinese medicines</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Liu, Zhao‐chan</creatorcontrib><creatorcontrib>Zhang, Shu‐mei</creatorcontrib><creatorcontrib>Wang, Run‐qin</creatorcontrib><creatorcontrib>Chen, Xuan</creatorcontrib><creatorcontrib>Hu, Shuang</creatorcontrib><creatorcontrib>Bai, Xiao‐hong</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of separation science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Liu, Zhao‐chan</au><au>Zhang, Shu‐mei</au><au>Wang, Run‐qin</au><au>Chen, Xuan</au><au>Hu, Shuang</au><au>Bai, Xiao‐hong</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Comparison of three‐phase hollow fiber liquid‐phase microextraction based on reverse micelle with conventional two‐phase hollow fiber liquid‐phase microextraction and their applications for analysis of cinnamic acids in traditional Chinese medicines</atitle><jtitle>Journal of separation science</jtitle><addtitle>J Sep Sci</addtitle><date>2019-09</date><risdate>2019</risdate><volume>42</volume><issue>18</issue><spage>2977</spage><epage>2984</epage><pages>2977-2984</pages><issn>1615-9306</issn><eissn>1615-9314</eissn><abstract>A novel three‐phase hollow fiber liquid‐phase microextraction was developed based on reverse micelle as extraction solvent and acceptor phase, and compared with conventional two‐phase hollow fiber liquid‐phase microextraction. Both procedures were used in the extraction and concentration of four cinnamic acids (caffeic acid, p‐hydroxycinnamic acid, ferulic acid, and cinnamic acid) in traditional Chinese medicines prior to high‐performance liquid chromatography analysis. Parameters affecting the two procedures were investigated and optimized to obtain the optimum enrichment factors. The mechanism of the developed procedure was explored and elucidated by comparison with conventional two‐phase hollow fiber liquid‐phase microextraction. Under the optimized conditions, the analytes’ enrichment factors were between 50 and 118 for the proposed procedure, and 31–96 for conventional two‐phase mode. Satisfactory linear ranges (r2 ≥ 0.99), detection limits (0.1–0.6 ng/mL), precisions (<9.2%), and accuracies (recoveries: 80–123.1%) were observed for the two procedures. The results showed that the enrichment capacity of the proposed procedure for the cinnamic acids is better than that of conventional two‐phase procedure, and both are eco‐friendly, simple, and effective for the enrichment and detection of cinnamic acids in traditional Chinese medicines.</abstract><cop>Germany</cop><pub>Wiley Subscription Services, Inc</pub><pmid>31273922</pmid><doi>10.1002/jssc.201900472</doi><tpages>8</tpages><orcidid>https://orcid.org/0000-0002-0784-3786</orcidid><orcidid>https://orcid.org/0000-0002-8276-4586</orcidid><orcidid>https://orcid.org/0000-0001-5287-6002</orcidid></addata></record> |
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| subjects | Acids Cinnamates - analysis Cinnamic acid cinnamic acids Drugs, Chinese Herbal - analysis Enrichment Ferulic acid high performance liquid chromatography hollow fiber liquid‐phase microextraction Hydroxycinnamic acid Liquid chromatography Liquid Phase Microextraction Medicine, Chinese Traditional Micelles Molecular Structure reverse micelle Reverse micelles Traditional Chinese medicine traditional Chinese medicines |
| title | Comparison of three‐phase hollow fiber liquid‐phase microextraction based on reverse micelle with conventional two‐phase hollow fiber liquid‐phase microextraction and their applications for analysis of cinnamic acids in traditional Chinese medicines |
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