Adsorption capacity of heavy metal ions using sultone-modified magnetic activated carbon as a bio-adsorbent

A novel magnetic bio-adsorbent has been prepared by the loading of Fe3O4 NPs and immobilization of 1,4-butane sultone on the surface of activated carbon. The activated carbon was synthesized from pistachio shell as a carbon material of biogenic, bio-resources and its use is cost effective. Structure...

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Veröffentlicht in:Materials Science & Engineering C 2019-08, Vol.101, p.42-52
Hauptverfasser: Nejadshafiee, Vajihe, Islami, Mohammad Reza
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description A novel magnetic bio-adsorbent has been prepared by the loading of Fe3O4 NPs and immobilization of 1,4-butane sultone on the surface of activated carbon. The activated carbon was synthesized from pistachio shell as a carbon material of biogenic, bio-resources and its use is cost effective. Structure, morphology and magnetic property of the prepared adsorbent were studied by transmission electron microscopy (TEM), vibrating sample magnetometer (VSM), Fourier transform infrared spectroscopy (FT-IR), and thermal gravimetric analysis (TGA). The capacity of the adsorbent for removing heavy metals ions Pb(II), As(III) and Cd(II) was studied using Langmuir adsorption isotherm under ultrasound-assisted condition. The maximum adsorption capacities of Pb(II), As(III) and Cd(II) were found to be 147.05, 151.51 and 119.04 mg g−1, respectively. In addition to high adsorption capacity, this adsorbent shows advantages such as green synthesis, low cast, recyclability, and easy separation. So this nanocomposite can be a suitable absorbent for removal of heavy metal ions from aqueous solutions. Meanwhile, the use of ultrasound radiation is an effective and rapid uptake technology for separating of heavy metal ions from aqueous solutions. [Display omitted] •A novel magnetic bio-adsorbent for removal of heavy metal ions from aqueous•Synthesis of Fe3O4 NPs@AC@C4H8SO3H with high adsorption capacity•Easy separation of the bio-adsorbent from the reaction medium by an external magnet
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The activated carbon was synthesized from pistachio shell as a carbon material of biogenic, bio-resources and its use is cost effective. Structure, morphology and magnetic property of the prepared adsorbent were studied by transmission electron microscopy (TEM), vibrating sample magnetometer (VSM), Fourier transform infrared spectroscopy (FT-IR), and thermal gravimetric analysis (TGA). The capacity of the adsorbent for removing heavy metals ions Pb(II), As(III) and Cd(II) was studied using Langmuir adsorption isotherm under ultrasound-assisted condition. The maximum adsorption capacities of Pb(II), As(III) and Cd(II) were found to be 147.05, 151.51 and 119.04 mg g−1, respectively. In addition to high adsorption capacity, this adsorbent shows advantages such as green synthesis, low cast, recyclability, and easy separation. So this nanocomposite can be a suitable absorbent for removal of heavy metal ions from aqueous solutions. 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The activated carbon was synthesized from pistachio shell as a carbon material of biogenic, bio-resources and its use is cost effective. Structure, morphology and magnetic property of the prepared adsorbent were studied by transmission electron microscopy (TEM), vibrating sample magnetometer (VSM), Fourier transform infrared spectroscopy (FT-IR), and thermal gravimetric analysis (TGA). The capacity of the adsorbent for removing heavy metals ions Pb(II), As(III) and Cd(II) was studied using Langmuir adsorption isotherm under ultrasound-assisted condition. The maximum adsorption capacities of Pb(II), As(III) and Cd(II) were found to be 147.05, 151.51 and 119.04 mg g−1, respectively. In addition to high adsorption capacity, this adsorbent shows advantages such as green synthesis, low cast, recyclability, and easy separation. So this nanocomposite can be a suitable absorbent for removal of heavy metal ions from aqueous solutions. 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Meanwhile, the use of ultrasound radiation is an effective and rapid uptake technology for separating of heavy metal ions from aqueous solutions. [Display omitted] •A novel magnetic bio-adsorbent for removal of heavy metal ions from aqueous•Synthesis of Fe3O4 NPs@AC@C4H8SO3H with high adsorption capacity•Easy separation of the bio-adsorbent from the reaction medium by an external magnet</abstract><cop>Netherlands</cop><pub>Elsevier B.V</pub><pmid>31029336</pmid><doi>10.1016/j.msec.2019.03.081</doi><tpages>11</tpages></addata></record>
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subjects Activated carbon
Adsorbents
Adsorption
Adsorption capacity
Aqueous solutions
Butane
Cadmium
Carbon
Charcoal - chemistry
Fe3O4 NPs@AC@SO3H
Fourier transforms
Gravimetric analysis
Heavy metals
Hydrogen-Ion Concentration
Immobilization
Infrared analysis
Infrared spectroscopy
Ions
Iron oxides
Kinetics
Lead
Magnetic properties
Magnetics
Materials science
Metal ions
Metals, Heavy - analysis
Morphology
Nanocomposites
Nanoparticles - chemistry
Nanoparticles - ultrastructure
Naphthalenesulfonates - chemistry
Particle Size
Radiation
Recyclability
Spectroscopy, Fourier Transform Infrared
Thermal analysis
Thermodynamics
Thermogravimetry
Time Factors
Transmission electron microscopy
Ultrasonic imaging
Ultrasound
X-Ray Diffraction
title Adsorption capacity of heavy metal ions using sultone-modified magnetic activated carbon as a bio-adsorbent
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