Versatile photoacoustic spectrometer based on a mid-infrared pulsed optical parametric oscillator
We demonstrate the usefulness of a nanosecond-pulsed single-mode mid-infrared (MIR) optical parametric oscillator (OPO) for photoacoustic (PA) spectroscopic measurements. The maximum wavelength ranges for the signal and idler are 1.4 μm to 1.7 μm and 2.8 μm to 4.6 μm, respectively, with a MIR output...
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Veröffentlicht in: | Applied optics (2004) 2019-01, Vol.58 (2), p.250-256 |
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creator | Lamard, Laurent Balslev-Harder, David Peremans, Andre Petersen, Jan C Lassen, Mikael |
description | We demonstrate the usefulness of a nanosecond-pulsed single-mode mid-infrared (MIR) optical parametric oscillator (OPO) for photoacoustic (PA) spectroscopic measurements. The maximum wavelength ranges for the signal and idler are 1.4 μm to 1.7 μm and 2.8 μm to 4.6 μm, respectively, with a MIR output power of up to 500 mW, making the OPO useful for different spectroscopic PA trace-gas measurements targeting the major market opportunity of environmental monitoring and breath gas analysis. We perform spectroscopic measurements of methane (CH
), nitrogen dioxide (NO
), and ammonia (NH
) in the 2.8 μm to 3.7 μm wavelength region. The measurements were conducted with a constant flow rate of 300 mL/min, thus demonstrating the suitability of the gas sensor for real-time trace-gas measurements. The acquired spectra are compared with data from the HITRAN database, and good agreement is found, demonstrating a resolution bandwidth of 1.5 cm
. An Allan deviation analysis shows that the detection limit for methane at optimum integration time for the PA sensor is 8 ppbV (nmol/mol) at 105 s of integration time, corresponding to a normalized noise equivalent absorption coefficient of 2.9×10
W cm
Hz
. |
doi_str_mv | 10.1364/AO.58.000250 |
format | Article |
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), nitrogen dioxide (NO
), and ammonia (NH
) in the 2.8 μm to 3.7 μm wavelength region. The measurements were conducted with a constant flow rate of 300 mL/min, thus demonstrating the suitability of the gas sensor for real-time trace-gas measurements. The acquired spectra are compared with data from the HITRAN database, and good agreement is found, demonstrating a resolution bandwidth of 1.5 cm
. An Allan deviation analysis shows that the detection limit for methane at optimum integration time for the PA sensor is 8 ppbV (nmol/mol) at 105 s of integration time, corresponding to a normalized noise equivalent absorption coefficient of 2.9×10
W cm
Hz
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), nitrogen dioxide (NO
), and ammonia (NH
) in the 2.8 μm to 3.7 μm wavelength region. The measurements were conducted with a constant flow rate of 300 mL/min, thus demonstrating the suitability of the gas sensor for real-time trace-gas measurements. The acquired spectra are compared with data from the HITRAN database, and good agreement is found, demonstrating a resolution bandwidth of 1.5 cm
. An Allan deviation analysis shows that the detection limit for methane at optimum integration time for the PA sensor is 8 ppbV (nmol/mol) at 105 s of integration time, corresponding to a normalized noise equivalent absorption coefficient of 2.9×10
W cm
Hz
.</description><subject>Absorptivity</subject><subject>Ammonia</subject><subject>Environmental monitoring</subject><subject>Flow velocity</subject><subject>Gas analysis</subject><subject>Gas sensors</subject><subject>Methane</subject><subject>Nitrogen dioxide</subject><subject>Optical Parametric Oscillators</subject><subject>Parametric amplifiers</subject><subject>Spectroscopic analysis</subject><issn>1559-128X</issn><issn>2155-3165</issn><issn>1539-4522</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><recordid>eNpdkD1PxDAMhiME4o6DjRlVYmGgRz7qtB1PJ76kk24BxBalqSN6apuStAP_nsABA15s2c9r2S8h54wumZDZzWq7hGJJKeVAD8icM4BUMAmHZB7LMmW8eJ2RkxB2lArIyvyYzASVGQjK5kS_oA96bFpMhjc3Om3cFMbGJGFAM3rX4Yg-qXTAOnF9opOuqdOmt1772Bmm9nswRIVuk0F7HQU-yl0wTdvq0flTcmR1xM5-8oI8390-rR_Szfb-cb3apEawckzRCpRZLnPkmQUDEgsAXtU1ZDyG0CBsLpFZC7m0GYK1oqw0ZkaWrMJKLMjVfu_g3fuEYVRdEwzGI3qMPynO8lKUBUgZ0ct_6M5Nvo_XRUoWRcG4KCN1vaeMdyF4tGrwTaf9h2JUfVmvVlsFhdpbH_GLn6VT1WH9B_96LT4BCr5_ng</recordid><startdate>20190110</startdate><enddate>20190110</enddate><creator>Lamard, Laurent</creator><creator>Balslev-Harder, David</creator><creator>Peremans, Andre</creator><creator>Petersen, Jan C</creator><creator>Lassen, Mikael</creator><general>Optical Society of America</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SP</scope><scope>7U5</scope><scope>8FD</scope><scope>H8D</scope><scope>L7M</scope><scope>7X8</scope></search><sort><creationdate>20190110</creationdate><title>Versatile photoacoustic spectrometer based on a mid-infrared pulsed optical parametric oscillator</title><author>Lamard, Laurent ; Balslev-Harder, David ; Peremans, Andre ; Petersen, Jan C ; Lassen, Mikael</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c319t-ef3e64767e24f5c56e8552bdd5422223a53f76e1ff576f4e5ff39bae4c691beb3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>Absorptivity</topic><topic>Ammonia</topic><topic>Environmental monitoring</topic><topic>Flow velocity</topic><topic>Gas analysis</topic><topic>Gas sensors</topic><topic>Methane</topic><topic>Nitrogen dioxide</topic><topic>Optical Parametric Oscillators</topic><topic>Parametric amplifiers</topic><topic>Spectroscopic analysis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Lamard, Laurent</creatorcontrib><creatorcontrib>Balslev-Harder, David</creatorcontrib><creatorcontrib>Peremans, Andre</creatorcontrib><creatorcontrib>Petersen, Jan C</creatorcontrib><creatorcontrib>Lassen, Mikael</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>Electronics & Communications Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Aerospace Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>MEDLINE - Academic</collection><jtitle>Applied optics (2004)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Lamard, Laurent</au><au>Balslev-Harder, David</au><au>Peremans, Andre</au><au>Petersen, Jan C</au><au>Lassen, Mikael</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Versatile photoacoustic spectrometer based on a mid-infrared pulsed optical parametric oscillator</atitle><jtitle>Applied optics (2004)</jtitle><addtitle>Appl Opt</addtitle><date>2019-01-10</date><risdate>2019</risdate><volume>58</volume><issue>2</issue><spage>250</spage><epage>256</epage><pages>250-256</pages><issn>1559-128X</issn><eissn>2155-3165</eissn><eissn>1539-4522</eissn><abstract>We demonstrate the usefulness of a nanosecond-pulsed single-mode mid-infrared (MIR) optical parametric oscillator (OPO) for photoacoustic (PA) spectroscopic measurements. The maximum wavelength ranges for the signal and idler are 1.4 μm to 1.7 μm and 2.8 μm to 4.6 μm, respectively, with a MIR output power of up to 500 mW, making the OPO useful for different spectroscopic PA trace-gas measurements targeting the major market opportunity of environmental monitoring and breath gas analysis. We perform spectroscopic measurements of methane (CH
), nitrogen dioxide (NO
), and ammonia (NH
) in the 2.8 μm to 3.7 μm wavelength region. The measurements were conducted with a constant flow rate of 300 mL/min, thus demonstrating the suitability of the gas sensor for real-time trace-gas measurements. The acquired spectra are compared with data from the HITRAN database, and good agreement is found, demonstrating a resolution bandwidth of 1.5 cm
. An Allan deviation analysis shows that the detection limit for methane at optimum integration time for the PA sensor is 8 ppbV (nmol/mol) at 105 s of integration time, corresponding to a normalized noise equivalent absorption coefficient of 2.9×10
W cm
Hz
.</abstract><cop>United States</cop><pub>Optical Society of America</pub><pmid>30645301</pmid><doi>10.1364/AO.58.000250</doi><tpages>7</tpages></addata></record> |
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source | Alma/SFX Local Collection; Optica Publishing Group Journals |
subjects | Absorptivity Ammonia Environmental monitoring Flow velocity Gas analysis Gas sensors Methane Nitrogen dioxide Optical Parametric Oscillators Parametric amplifiers Spectroscopic analysis |
title | Versatile photoacoustic spectrometer based on a mid-infrared pulsed optical parametric oscillator |
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